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    PREPARATION OF HIGH-QUALITY OXO PROCESS ALCOHOLS FROM INCONSTANT RAW MATERIAL SOURCES
    9.
    发明申请
    PREPARATION OF HIGH-QUALITY OXO PROCESS ALCOHOLS FROM INCONSTANT RAW MATERIAL SOURCES 有权
    从不合理原料来源制备高品质氧气工艺酒精

    公开(公告)号：US20150336861A1

    公开(公告)日：2015-11-26

    申请号：US14717183

    申请日：2015-05-20

    申请人： Frank GEILEN ,  Katrin Marie DYBALLA ,  Dieter HESS ,  Stephan PEITZ ,  Robert FRANKE ,  Dirk FRIDAG ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Guido STOCHNIOL

    发明人： Frank GEILEN ,  Katrin Marie DYBALLA ,  Dieter HESS ,  Stephan PEITZ ,  Robert FRANKE ,  Dirk FRIDAG ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Guido STOCHNIOL

    IPC分类号： C07C29/14 ,  C07C69/80 ,  C08K5/12 ,  C07C67/08

    CPC分类号： C07C29/14 ,  B01J31/185 ,  B01J31/1885 ,  C07C2/24 ,  C07C29/141 ,  C07C45/50 ,  C07C67/08 ,  C07C69/80 ,  C07C2523/755 ,  C08K5/12 ,  C07C11/02 ,  C07C47/02 ,  C07C31/125

    摘要： The preparation of high-quality oxo process alcohols from inconstant raw material sources is the technically demanding problem which is addressed by a process for continuously preparing an alcohol mixture, in which an input mixture which contains an olefin and has a composition that changes over time is subjected to an oligomerization to obtain an oligomerizate and at least a portion of the olefin oligomers present in the oligomerizate are hydroformylated with carbon monoxide and hydrogen in a hydroformylation in the presence of a homogeneous catalyst system to give aldehydes, at least some of which are converted to the alcohol mixture by subsequent hydrogenation. The process provides a constant plasticizer quality to be produced over a long production period and, optionally, a higher throughput with the same product quality. This is achieved a) by control of the temperature and/or the conversion of the oligomerization as a function of the current composition of the oligomerizate; and b) by control of the composition of the catalyst system and/or of the pressure of the hydroformylation as a function of the current composition of the aldehydes.

    摘要翻译： 从不定原料来源制备高品质氧化工艺醇是技术上要求苛刻的问题，其通过连续制备醇混合物的方法来解决，其中含有烯烃并且具有随时间变化的组成的输入混合物是 进行低聚以获得低聚物，并且在均相催化剂体系的存在下，在加氢甲酰化中，将低聚物中存在的烯烃低聚物的至少一部分与一氧化碳和氢气加氢甲酰化，得到醛，其中至少一些转化为 通过随后的氢化到醇混合物。 该方法提供了在长的生产周期内生产的恒定的增塑剂质量，并且可选地具有相同产品质量的较高产量。 这是通过控制低聚物的温度和/或转化作为当前低聚物组成的函数来实现的; 和b）通过控制催化剂体系的组成和/或加氢甲酰基化的压力作为醛的当前组成的函数。