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公开(公告)号：US08735492B2
公开(公告)日：2014-05-27
申请号：US13392814
申请日：2010-08-25
IPC分类号： C08F2/24
CPC分类号： C08F214/18 , C08F2/22 , C08F14/24 , C08F214/22 , C08F2220/286 , C08F2/24 , C08F2/26
摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound (1) represented by the formula: CH2═CR1—R2—O-(AO)p—X (in the formula, R1 is hydrogen or an alkyl group; R2 is an alkylene group having two or more carbon atoms; AO is a linear or branched oxyalkylene group having 2 to 4 carbon atoms; p is a positive integer; X is H or SO3Y wherein Y is NH4 or an alkaline metal; and AO may be the same or different and may form two or more blocks if there is more than one AO.)
摘要翻译： 本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。 含氟聚合物的制造方法包括在由式：CH 2 = CR 1 -R 2 -O-（AO）p -X（式1）表示的化合物（1）的存在下包含至少一种氟烯烃的单体的水分散聚合 R1是氢或烷基; R2是具有两个或更多个碳原子的亚烷基; AO是具有2至4个碳原子的直链或支链氧化烯基; p是正整数; X是H或SO 3 Y，其中Y是 NH 4或碱金属;并且AO可以相同或不同，如果存在多于一个AO，则可以形成两个或更多个嵌段）。
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公开(公告)号：US20120157621A1
公开(公告)日：2012-06-21
申请号：US13392814
申请日：2010-08-25
IPC分类号： C08K5/1535 , C08F2/22 , C08L27/20 , C08L27/18 , C08L27/12 , C08L27/14 , C08K5/42 , C08L27/16
CPC分类号： C08F214/18 , C08F2/22 , C08F14/24 , C08F214/22 , C08F2220/286 , C08F2/24 , C08F2/26
摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound (1) represented by the formula: CH2═CR1—R2—O-(AO)p—X (in the formula, R1 is hydrogen or an alkyl group; R2 is an alkylene group having two or more carbon atoms; AO is a linear or branched oxyalkylene group having 2 to 4 carbon atoms; p is a positive integer; X is H or SO3Y wherein Y is NH4 or an alkaline metal; and AO may be the same or different and may form two or more blocks if there is more than one AO.)
摘要翻译： 本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。 含氟聚合物的制造方法包括在由式：CH 2 = CR 1 -R 2 -O-（AO）p -X（式1）表示的化合物（1）的存在下包含至少一种氟烯烃的单体的水分散聚合 R1是氢或烷基; R2是具有两个或更多个碳原子的亚烷基; AO是具有2至4个碳原子的直链或支链氧化烯基; p是正整数; X是H或SO 3 Y，其中Y是 NH 4或碱金属;并且AO可以相同或不同，如果存在多于一个AO，则可以形成两个或更多个嵌段）。
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3.发明授权Method for producing aqueous dispersion of fluorine-containing seed polymer particles and aqueous coating composition and coated article thereof 有权含氟种子聚合物颗粒和水性涂料组合物的水性分散体及其涂布制品的制备方法公开(公告)号：US08993679B2
公开(公告)日：2015-03-31
申请号：US13255742
申请日：2010-03-11
IPC分类号： C08F2/24 , C08F214/00 , C09D5/02 , C09D127/12 , C09D129/10 , C08F214/18 , C08F14/18 , C09D127/16
CPC分类号： C08F214/18 , C08F14/18 , C08F214/186 , C09D5/02 , C09D127/12 , C09D127/16 , C08F2/16
摘要： There is provided a method for producing an aqueous dispersion of fluorine-containing seed polymer (B) particles, comprising a step for preparing an aqueous dispersion of fluorine-containing polymer (A) particles by polymerizing monomer comprising at least one fluoroolefin in an aqueous dispersion in the presence of a compound (1) represented by the formula: CH2═CHCH2—O—R, wherein R is a hydrocarbon group which may have an oxygen atom, a nitrogen atom and/or a polar group, and (II) a step for seed-polymerizing ethylenically unsaturated monomer with the fluorine-containing polymer (A) particles in the aqueous dispersion of the fluorine-containing polymer (A) particles. The production method is the method for producing an aqueous dispersion of fluorine-containing seed polymer particles and assures a low foamability and gives an excellent gloss of an obtained coating film and excellent adhesion to a substrate when the fluorine-containing seed polymer particles are used as a coating film forming component of a coating composition.
摘要翻译： 提供了一种制备含氟种子聚合物（B）颗粒的水性分散体的方法，包括通过在水分散体中聚合包含至少一种氟烯烃的单体来制备含氟聚合物（A）颗粒的水分散体的步骤 在由式：CH 2 = CHCH 2 -O-R表示的化合物（1）的存在下，其中R是可具有氧原子，氮原子和/或极性基团的烃基，和（II） 在含氟聚合物（A）颗粒的水分散体中与含氟聚合物（A）颗粒进行种子聚合烯键式不饱和单体的步骤。 制造方法是含氟种子聚合物粒子的水性分散体的制造方法，当使用含氟种子聚合物粒子时，可确保低发泡性，得到的涂膜的光泽度优异，对基材的粘附性优异 涂料组合物的涂膜形成组分。
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公开(公告)号：US08952115B2
公开(公告)日：2015-02-10
申请号：US13392733
申请日：2010-08-25
IPC分类号： C08F14/18
CPC分类号： C08F214/18 , C08F14/18 , C08F14/22 , C08F14/24 , C08F14/26 , C08F214/227 , C08F214/287 , C08F2/16 , C08F2/24 , C08F2/22
摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound represented by the formula: CH2═CHCH2—O—(C═O)CHXCH2COO(CH2)nCH3 (in the formula, X is H or SO3Y wherein Y is NH4 or an alkaline metal; and n is an integer of 0 to 19.)
摘要翻译： 本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。 含氟聚合物的制造方法包括在由式：CH 2 = CHCH 2 -O-（C = O）CHXCH 2 COO（CH 2）n CH 3表示的化合物存在下，包含至少一种氟烯烃的单体的水分散聚合（式中， X是H或SO 3 Y，其中Y是NH 4或碱金属; n是0至19的整数。）
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公开(公告)号：US20120157646A1
公开(公告)日：2012-06-21
申请号：US13392733
申请日：2010-08-25
IPC分类号： C08F2/16 , C08F214/28 , C08F2/24 , C08F214/26
CPC分类号： C08F214/18 , C08F14/18 , C08F14/22 , C08F14/24 , C08F14/26 , C08F214/227 , C08F214/287 , C08F2/16 , C08F2/24 , C08F2/22
摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound represented by the formula: CH2═CHCH2—O—(C═O)CHXCH2COO(CH2)nCH3 (in the formula, X is H or SO3Y wherein Y is NH4 or an alkaline metal; and n is an integer of 0 to 19.)
摘要翻译： 本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。 含氟聚合物的制造方法包括在由式：CH 2 = CHCH 2 -O-（C = O）CHXCH 2 COO（CH 2）n CH 3表示的化合物存在下，包含至少一种氟烯烃的单体的水分散聚合（式中， X是H或SO 3 Y，其中Y是NH 4或碱金属; n是0至19的整数。）
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6.发明申请公开(公告)号：US20120004367A1
公开(公告)日：2012-01-05
申请号：US13255742
申请日：2010-03-11
IPC分类号： C09D127/18
CPC分类号： C08F214/18 , C08F14/18 , C08F214/186 , C09D5/02 , C09D127/12 , C09D127/16 , C08F2/16
摘要： There is provided a method for producing an aqueous dispersion of fluorine-containing seed polymer (B) particles, comprising a step for preparing an aqueous dispersion of fluorine-containing polymer (A) particles by polymerizing monomer comprising at least one fluoroolefin in an aqueous dispersion in the presence of a compound (1) represented by the formula: CH2═CHCH2—O—R, wherein R is a hydrocarbon group which may have an oxygen atom, a nitrogen atom and/or a polar group, and (II) a step for seed-polymerizing ethylenically unsaturated monomer with the fluorine-containing polymer (A) particles in the aqueous dispersion of the fluorine-containing polymer (A) particles. The production method is the method for producing an aqueous dispersion of fluorine-containing seed polymer particles and assures a low foamability and gives an excellent gloss of an obtained coating film and excellent adhesion to a substrate when the fluorine-containing seed polymer particles are used as a coating film forming component of a coating composition.
摘要翻译： 提供了一种制备含氟种子聚合物（B）颗粒的水性分散体的方法，包括通过在水分散体中聚合包含至少一种氟烯烃的单体来制备含氟聚合物（A）颗粒的水分散体的步骤 在由式：CH 2 = CHCH 2 -O-R表示的化合物（1）的存在下，其中R是可具有氧原子，氮原子和/或极性基团的烃基，和（II） 在含氟聚合物（A）颗粒的水分散体中与含氟聚合物（A）颗粒进行种子聚合烯键式不饱和单体的步骤。 制造方法是含氟种子聚合物粒子的水性分散体的制造方法，当使用含氟种子聚合物粒子时，可确保低发泡性，得到的涂膜的光泽度优异，对基材的粘附性优异 涂料组合物的涂膜形成组分。
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