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64 条记录 (耗时 0.016 秒)

    Method for producing fluorine-containing polymer
    2.
    发明授权
    Method for producing fluorine-containing polymer 有权
    含氟聚合物的制造方法

    公开(公告)号：US08952115B2

    公开(公告)日：2015-02-10

    申请号：US13392733

    申请日：2010-08-25

    申请人： Katsuhiko Imoto ,  Shumi Nishii ,  Yoshinari Fukuhara

    发明人： Katsuhiko Imoto ,  Shumi Nishii ,  Yoshinari Fukuhara

    IPC分类号： C08F14/18

    CPC分类号： C08F214/18 ,  C08F14/18 ,  C08F14/22 ,  C08F14/24 ,  C08F14/26 ,  C08F214/227 ,  C08F214/287 ,  C08F2/16 ,  C08F2/24 ,  C08F2/22

    摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound represented by the formula: CH2═CHCH2—O—(C═O)CHXCH2COO(CH2)nCH3 (in the formula, X is H or SO3Y wherein Y is NH4 or an alkaline metal; and n is an integer of 0 to 19.)

    摘要翻译： 本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。 含氟聚合物的制造方法包括在由式：CH 2 = CHCH 2 -O-（C = O）CHXCH 2 COO（CH 2）n CH 3表示的化合物存在下，包含至少一种氟烯烃的单体的水分散聚合（式中， X是H或SO 3 Y，其中Y是NH 4或碱金属; n是0至19的整数。）

    METHOD FOR PRODUCING FLUORINE-CONTAINING POLYMER
    3.
    发明申请
    METHOD FOR PRODUCING FLUORINE-CONTAINING POLYMER 有权
    生产含氟聚合物的方法

    公开(公告)号：US20120157646A1

    公开(公告)日：2012-06-21

    申请号：US13392733

    申请日：2010-08-25

    申请人： Katsuhiko Imoto ,  Shumi Nishii ,  Yoshinari Fukuhara

    发明人： Katsuhiko Imoto ,  Shumi Nishii ,  Yoshinari Fukuhara

    IPC分类号： C08F2/16 ,  C08F214/28 ,  C08F2/24 ,  C08F214/26

    CPC分类号： C08F214/18 ,  C08F14/18 ,  C08F14/22 ,  C08F14/24 ,  C08F14/26 ,  C08F214/227 ,  C08F214/287 ,  C08F2/16 ,  C08F2/24 ,  C08F2/22

    摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound represented by the formula: CH2═CHCH2—O—(C═O)CHXCH2COO(CH2)nCH3 (in the formula, X is H or SO3Y wherein Y is NH4 or an alkaline metal; and n is an integer of 0 to 19.)

    摘要翻译： 本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。 含氟聚合物的制造方法包括在由式：CH 2 = CHCH 2 -O-（C = O）CHXCH 2 COO（CH 2）n CH 3表示的化合物存在下，包含至少一种氟烯烃的单体的水分散聚合（式中， X是H或SO 3 Y，其中Y是NH 4或碱金属; n是0至19的整数。）

    Process for production of fluorine-containing polymers and fluorine-containing polymers
    4.
    发明授权
    Process for production of fluorine-containing polymers and fluorine-containing polymers 有权
    含氟聚合物和含氟聚合物的制备方法

    公开(公告)号：US08080195B2

    公开(公告)日：2011-12-20

    申请号：US10579790

    申请日：2004-11-19

    申请人： Yoshiyuki Takase ,  Kenji Ishii ,  Shouji Fukuoka

    发明人： Yoshiyuki Takase ,  Kenji Ishii ,  Shouji Fukuoka

    IPC分类号： B27N3/08

    CPC分类号： C08F14/18 ,  C08F8/00 ,  C08F14/22 ,  C08F14/24 ,  C08F14/26 ,  C08F14/28 ,  C08F114/22 ,  C08F114/24 ,  Y10T428/3154

    摘要： A method of producing a fluoropolymer by which a melt-processable fluoropolymer (A) having a specific unstable terminal group or groups (P) is subjected to melt-kneading in a kneader having a stabilization treatment zone to thereby produce a fluoro-polymer (B) resulting from conversion of the specific unstable terminal group or groups (P) to —CF2H. The specific unstable terminal group or groups (P) include alkoxycarbonyl groups, fluoroalkoxycarbonyl groups and/or carboxyl group quaternary nitrogen compound salts, the melt-kneading is carried out in the absence or presence of an alkali metal element or alkaline earth metal element, the content of the alkali metal element or alkaline earth metal element is not greater than 2 ppm of the composition under melt-kneading, and the melt-kneading in the stabilization treatment zone is carried out in the presence of water. A fluoro-polymerised material is also disclosed.

    摘要翻译： 在具有稳定化处理区域的捏合机中对具有特定不稳定末端基团（P）的可熔融加工的含氟聚合物（A）进行熔融混炼的含氟聚合物的制造方法，由此制造氟聚合物 ）由特定的不稳定末端基团（P）转化为-CF 2 H而得到。 特定的不稳定末端基（P）包括烷氧基羰基，氟代烷氧基羰基和/或羧基季氮化合物盐，在不存在或不存在碱金属元素或碱土金属元素的情况下进行熔融混炼， 在熔融捏合下，碱金属元素或碱土金属元素的含量不超过组合物的2ppm，稳定化处理区的熔融捏合在水的存在下进行。 还公开了氟聚合材料。

    Process of polymerizing chloroetrifluoroethylene with alkyl hydroperoxide and metal metabisulfite
    6.
    发明授权
    Process of polymerizing chloroetrifluoroethylene with alkyl hydroperoxide and metal metabisulfite 失效
    用烷基氢过氧化物和偏亚硫酸氢钠聚合氯三氟乙烯的方法

    公开(公告)号：US5453477A

    公开(公告)日：1995-09-26

    申请号：US207973

    申请日：1994-03-07

    申请人： Bryce C. Oxenrider ,  Frank Mares ,  Mo-Shu Yang

    发明人： Bryce C. Oxenrider ,  Frank Mares ,  Mo-Shu Yang

    IPC分类号： C08F14/24 ,  C08F4/40

    CPC分类号： C08F14/24

    摘要： Process for the production of PCTFE homopolymer and/or copolymer resins by the use of an aqueous suspension system incorporating a redox initiator system which comprises t-butyl hydroperoxide and sodium metabisulfite to initiate the polymerization or copolymerization process. The process parameters may be controlled to provide a PCTFE homopolymer or copolymer resin having a desired target range of molecular weights. The process provides stable PCTFE polymer suspensions which exhibit a low tendency to coagulate and further exhibit good wettability of the homopolymer and copolymer particles, notably in the absence of soaps.

    摘要翻译： 通过使用包含叔丁基过氧化氢和偏亚硫酸氢钠的氧化还原引发剂体系的水性悬浮体系来制备PCTFE均聚物和/或共聚物树脂以引发聚合或共聚过程的方法。 可以控制工艺参数以提供具有期望的目标分子量范围的PCTFE均聚物或共聚物树脂。 该方法提供稳定的PCTFE聚合物悬浮液，其表现出低凝结倾向并且进一步显示均聚物和共聚物颗粒的良好润湿性，特别是在不存在皂的情况下。

    Polymerization of perhalocarbons with trifluorodichloropropionyl peroxide
    7.
    发明授权
    Polymerization of perhalocarbons with trifluorodichloropropionyl peroxide 失效
    用三氯二氯丙酰过氧化物对全卤代烃进行聚合

    公开(公告)号：US2705706A

    公开(公告)日：1955-04-05

    申请号：US22585051

    申请日：1951-05-11

    申请人： KELLOGG M W CO

    发明人： DITTMAN ALBERT L ,  WRIGHTSON JOHN M

    IPC分类号： C07C17/25 ,  C07C17/26 ,  C07C45/63 ,  C07C409/08 ,  C07C409/34 ,  C08F14/22 ,  C08F14/24

    CPC分类号： C07C17/25 ,  C07C17/263 ,  C07C45/63 ,  C08F14/22 ,  C08F14/24 ,  C07C22/08 ,  C07C47/14 ,  C08F2/02

    摘要： 723,445. Polymerization; perhalopolymers. KELLOGG CO., M. W. April 18, 1952 [May 11, 1951], No. 9792/52. Drawings to Specification. Class 2 (5). [Also in Group IV (b)] Liquid or solid perhalo-polymers are made by polymerizing, e.g. in a solvent or diluent, a perhalo-olefin alone or with another perhalo-olefin or with another halogen-containing organic monomer in the presence of a completely or partially chlorinated and/or fluorinated aliphatic acyl peroxide having at least 6 carbon atoms per molecule as catalyst, and optionally a chain-terminating agent which may be the solvent. The concentration of the catalyst is preferably maintained during the polymerization between 0.01 and 0.5 per cent of the olefin for solid polymers and between 0.5 to 10 per cent for liquid polymers. Perhalo-olefins and monomers mentioned are trifluorochloroethylene, tetrafluorethylene, perfluorobutadiene, difluorodichloroethylene, perfluoropropene, perfluoromonochloropropene, perfluorobutene, perfluoromonochlorobutene, diphenyldifluoroethylene, vinylidene fluoride, vinyl fluoride, vinyl chloride, vinylidene chloride, and perfluorostyrene. The catalyst may be trifluorodichloropropionyl, trichlorodifluoropropionyl, tetrafluorochloropropionyl, tetrachlorofluoropropionyl, perfluoropropionyl, perchloropropionyl, tetrachloropropionyl, tetrafluoropropionyl, fluoropropionyl, pentafluorodichlorobutyryl, pentachlorodifluoro-, butyryl, tetrafluorotrichlorobutyryl, tetrachlorotrifluorobutyryl, perfluorobutyryl, perchlorobutyryl, tetrachlorobutyryl, tetrafluorobutyryl, fluorobutyryl, septafluorodichlorovaleryl, pentafluorotetrachlorovaleryl, pentachlorotetrafluorovaleryl, perfluorovaleryl, perchlorovaleryl, tetrachlorovaleryl, tetrafluorovaleryl, or fluorovaleryl peroxide. Solvents and diluents mentioned are water, chloroform, hydrocarbon oils, carbon tetrachloride, bromotrichloromethane, trichlorotrifluoroethane, tetrachloroethane, and trichlorofluoromethane. Specification 694,164 is referred to.