METHOD FOR PRODUCING NITRIDE SINGLE CRYSTAL AND AUTOCLAVE FOR USE IN THE METHOD
    3.
    发明申请
    METHOD FOR PRODUCING NITRIDE SINGLE CRYSTAL AND AUTOCLAVE FOR USE IN THE METHOD 审中-公开
    用于生产氮化物单晶和自动化的方法用于该方法

    公开(公告)号:US20140205840A1

    公开(公告)日:2014-07-24

    申请号:US14128474

    申请日:2011-06-23

    IPC分类号: C30B7/10 C01B21/06 C30B29/40

    摘要: There is provided a novel method for producing a nitride single crystal with both a rapid crystal growth rate and high crystal quality, as well as a novel autoclave that can be used in the method. The invention provides a method for producing a Ga-containing nitride single crystal by an ammonothermal method, comprising introducing at least a starting material, an acidic mineralizer and ammonia into an autoclave, and then growing a Ga-containing nitride single crystal under conditions wherein the temperature (T1) at the single crystal growth site is 600° C. to 850° C., the temperature (T1) at the single crystal growth site and the temperature (T2) at the starting material feeder site are in the relationship T1>T2, and the pressure in the autoclave is 40 MPa to 250 MPa, as well as an autoclave that can be used in the method.

    摘要翻译: 提供了一种用于生产具有快速晶体生长速率和高晶体质量的氮化物单晶的新颖方法,以及可用于该方法的新型高压釜。 本发明提供了一种通过氨热法制备含Ga氮化物单晶的方法,包括将至少一种起始材料,酸性矿化剂和氨引入高压釜中,然后在其中使含Ga的氮化物单晶生长 单晶生长部位的温度(T1)为600℃〜850℃,单晶生长部位的温度(T1)和原料供给部位的温度(T2)为T1> T2,高压釜中的压力为40MPa〜250MPa,以及可用于该方法的高压釜。