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    Fluorine-containing graft copolymer and toner using the same
    4.
    发明授权
    Fluorine-containing graft copolymer and toner using the same 失效
    含氟接枝共聚物和使用其的调色剂

    公开(公告)号：US5328794A

    公开(公告)日：1994-07-12

    申请号：US031952

    申请日：1993-03-16

    申请人： Tsubuko Kazuo ,  Shinichi Kuramoto ,  Kazuhiko Umemura ,  Toshihiko Takahashi ,  Hidemi Uematsu

    发明人： Tsubuko Kazuo ,  Shinichi Kuramoto ,  Kazuhiko Umemura ,  Toshihiko Takahashi ,  Hidemi Uematsu

    IPC分类号： C08F291/00 ,  G03G9/087 ,  G03G9/08 ,  C08F265/04

    CPC分类号： G03G9/08791 ,  C08F291/00 ,  G03G9/08728 ,  G03G9/08786

    摘要： A fluorine-containing graft copolymer prepared by a step (i) of polymerizing a monomer having formula (I) and an unsaturated carboxylic acid or a monomer having a glycidyl group to obtain a copolymer, ##STR1## wherein R represents --H or --CH.sub.3 group; and A represents --COOC.sub.n H.sub.2n+1 or OC.sub.n H.sub.2n+1, in which n is an integer of 6 to 20; a step (ii) of esterifying the resulting copolymer by using a monomer having a glycidyl group in the case where a constituting monomer of the above copolymer is an unsaturated carboxylic acid, or by using an unsaturated carboxylic acid in the case where a constituting monomer of the above copolymer is a monomer having a glycidyl group; and a step (iii) of graft-polymerizing a monomer comprising at least fluoroalkyl acrylate or fluoroalkyl methacrylate on the above esterified copolymer. In addition, a toner comprising a coloring agent and a resin component which comprises the above-mentioned fluorine-containing graft copolymer is disclosed.

    摘要翻译： 通过聚合具有式（I）的单体和不饱和羧酸或具有缩水甘油基的单体的步骤（i）制备的含氟接枝共聚物以获得共聚物; A表示-COOC n H 2n + 1或OC n H 2n + 1，其中n为6至20的整数; 在上述共聚物的构成单体为不饱和羧酸的情况下使用具有缩水甘油基的单体或通过使用不饱和羧酸在所得共聚物的构成单体的情况下酯化所得共聚物的工序（ii） 上述共聚物是具有缩水甘油基的单体; 和在上述酯化共聚物上至少含有丙烯酸氟代烷基酯或甲基丙烯酸氟烷基酯的单体的接枝聚合步骤（iii）。 此外，公开了包含着色剂和包含上述含氟接枝共聚物的树脂组分的调色剂。

    Liquid developer for electrostatic electrophotography
    5.
    发明授权
    Liquid developer for electrostatic electrophotography 失效
    静电电子照相用液体显影剂

    公开(公告)号：US5759733A

    公开(公告)日：1998-06-02

    申请号：US821314

    申请日：1992-01-13

    申请人： Kazuo Tsubuko ,  Shinichi Kuramoto ,  Toshiki Nanya ,  Kazuhiko Umemura ,  Kayoko Nagai

    发明人： Kazuo Tsubuko ,  Shinichi Kuramoto ,  Toshiki Nanya ,  Kazuhiko Umemura ,  Kayoko Nagai

    IPC分类号： G03G9/13 ,  G03G9/135

    CPC分类号： G03G9/131

    摘要： A liquid developer for use in electrophotography is disclosed, which comprises (i) a toner comprising as the main toner components a colorant, a resin, and a polyolefin resin having an acid value of from 5 to 50 and a melt viscosity at 200.degree. C. of from 100 to 15,000 cps, and (ii) a carrier liquid in which the toner is dispersed. The polyolefin resin and the colorant in the liquid developer may constitute an integral flushing colorant which is prepared by subjecting the resin and the colorant to flushing processing.

    摘要翻译： 公开了一种用于电子照相术的液体显影剂，其包括（i）包含作为主要调色剂组分的着色剂，树脂和酸值为5至50的聚烯烃树脂和200℃下的熔体粘度的调色剂 100至15,000cps，和（ii）其中调色剂分散的载体液体。 液体显影剂中的聚烯烃树脂和着色剂可以构成通过使树脂和着色剂进行冲洗加工而制备的整体冲洗着色剂。

    Toner for electrophotography
    6.
    发明授权
    Toner for electrophotography 失效
    电子照相用碳粉

    公开(公告)号：US5026621A

    公开(公告)日：1991-06-25

    申请号：US351025

    申请日：1989-05-12

    申请人： Kazuo Tsubuko ,  Shinichi Kuramoto ,  Kazuhiko Umemura ,  Makoto Ohkawara

    发明人： Kazuo Tsubuko ,  Shinichi Kuramoto ,  Kazuhiko Umemura ,  Makoto Ohkawara

    IPC分类号： G03G9/087 ,  G03G9/09 ,  G03G9/13

    CPC分类号： G03G9/08788 ,  G03G9/08728

    摘要： A toner for electrophotography is disclosed, which comprises as the main components a coloring component and a binder resin which is a block copolymer comprising a functional segment (A) consisting of at least one of a fluoralkyl acryl ester block unit or a fluoralkyl methacryl ester block unit, and a compatible segment (B) consisting of a fluorine-free vinyl or olefin monomer block unit.

    摘要翻译： 公开了用于电子照相的调色剂，其包含作为主要组分的着色组分和粘合剂树脂，其是包含由氟烷基丙烯酸酯嵌段单元或氟代烷基甲基丙烯酸酯嵌段中的至少一种组成的官能区段（A）的嵌段共聚物 单元和由无氟乙烯基或烯烃单体嵌段单元组成的相容片段（B）。

    Liquid developer for developing electrostatic image and image forming method
    8.
    发明授权
    Liquid developer for developing electrostatic image and image forming method 失效
    用于显影静电图像和图像形成方法的液体显影剂

    公开(公告)号：US06447973B1

    公开(公告)日：2002-09-10

    申请号：US09644266

    申请日：2000-08-23

    申请人： Tsuyoshi Asami ,  Kazuo Tsubuko ,  Aiko Ishikawa ,  Akihiro Koseki ,  Takeo Kudoh ,  Kazuhiko Umemura

    发明人： Tsuyoshi Asami ,  Kazuo Tsubuko ,  Aiko Ishikawa ,  Akihiro Koseki ,  Takeo Kudoh ,  Kazuhiko Umemura

    IPC分类号： G03G900

    CPC分类号： G03G9/135 ,  G03G9/125 ,  G03G9/131 ,  G03G9/132

    摘要： A liquid developer containing a carrier liquid containing silicone oil, and toner particles dispersed in the carrier liquid and each containing a coloring agent and a resin, the resin contains at least one member selected from the group consisting of the following resins (a)-(g): (a): rosin polymers having a softening point of 50-190° C., a glass transition point of 10-170° C. and a molecular weight of 2,000-40,000 and obtained by reacting (a1) a rosin glycidyl ester, (a2) dicarboxylic acid or dicarboxylic anhydride, (a3) at least one crosslinking agent selected from the group consisting of polyfunctional epoxy compounds, tri- or more polybasic acids or anhydrides thereof tri- or more polyhydric alcohols, and (a4) a dihydric alcohol; (b): vinyl polymers having a ratio of the weight average molecular weight to the number average molecular weight of greater than 4; (c): olefin resins having a melt index of 2.5-700; (d): polyolefins or polyolefin copolymers having an acid value of 0.5-80 and a melt viscosity of 50-20,000 mpa·s at 200° C.; (e): polymers obtained by crosslinking carboxyl group-containing vinyl polymers with an amine; (f): vinyl polymers having at least 0.005% by weight of a crosslinking monomer based on a total monomer; and (g): silicone copolymers, silicone rubber or silicone-modified resins. A liquid developer containing a carrier liquid containing silicone oil, toner particles each containing a coloring agent and a resin, and an erucamide compound.

    摘要翻译： 含有含有硅油的载体液体的液体显影剂和分散在载体液体中并分别含有着色剂和树脂的调色剂颗粒，所述树脂含有选自以下树脂中的至少一种：（a） - （ g）:( a）：软化点为50-190℃，玻璃化转变温度为10-170℃，分子量为2,000-40,000的松香聚合物，通过使（a1）松香缩水甘油基 酯，（a2）二羧酸或二羧酸酐，（a3）至少一种交联剂，其选自多官能环氧化合物，三元以上多元酸或其酸酐三元以上多元醇，和（a4）a 二元醇;（b）：重均分子量与数均分子量之比大于4的乙烯基聚合物;（c）：熔体指数为2.5-700的烯烃树脂;（d）：聚烯烃或 酸值为0.5-80的聚烯烃共聚物和a （e）：通过使含羧基的乙烯基聚合物与胺交联而获得的聚合物;（f）：具有至少0.005重量％的交联单体的乙烯基聚合物 基于总单体; 和（g）：硅氧烷共聚物，硅橡胶或硅氧烷改性树脂。 含有含有硅油的载体液体，各自含有着色剂和树脂的调色剂颗粒和芥酸酰胺化合物的液体显影剂。