Crystallized pellet/liquid separator
    1.
    发明申请
    Crystallized pellet/liquid separator 有权
    结晶丸/液分离器

    公开(公告)号:US20070062872A1

    公开(公告)日:2007-03-22

    申请号:US11501606

    申请日:2006-08-09

    IPC分类号: B01D61/00

    摘要: A process and apparatus which reduces the fines in a liquid discharge stream and/or increases the dryness of a solids discharge stream while under a pressure equal to or greater than the vapor pressure of the liquid. There is provided a process for separating particles such as polyethylene terephthalate or polyethylene naphthalate from a liquid in a slurry comprising: a. feeding a slurry comprising solid particles and a liquid into a within a separation zone maintained at a pressure equal to or greater than the vapor pressure of the liquid; b. contacting the slurry in the separation zone with a porous filter, optionally a microfilter, nanofilter, reverse osmosis filter, or ultrafilter, and separating liquid from the particles, wherein the liquid flows through the filter into an outer annulus defined as a space between the wall of the separation device and the filter, and said porous filter optionally having a terminal point beyond which the separated liquid does not pass from the outer annulus back through the filter; c. accumulating no liquid in the outer annulus or accumulating liquid in the outer annulus at a level below or in front of the terminal point, and continuously discharging the separated liquid from the outer annulus through a liquid outlet; d. decoupling the particles from the separation zone through the solids outlet to a low pressure below the vapor pressure of the liquid at the liquid temperature within the separation zone while maintaining a pressure on the particles prior to decoupling at or above the vapor pressure of the liquid within the separation zone.

    摘要翻译: 一种在液体排出流中减少细粉和/或在等于或大于液体的蒸气压的压力下增加固体排出流的干度的方法和装置。 提供了一种用于从浆液中的液体分离颗粒如聚对苯二甲酸乙二醇酯或聚萘二甲酸乙二醇酯的方法,包括:a。 将包含固体颗粒和液体的浆料进料到保持在等于或大于液体的蒸气压的压力的分离区内; b。 使分离区中的浆料与多孔过滤器,任选的微过滤器,纳米过滤器,反渗透过滤器或超滤器接触,并将液体从颗粒中分离,其中液体流过过滤器,形成外壁,其被定义为壁之间的空间 分离装置和过滤器,并且所述多孔过滤器任选地具有终点,超过该终点,分离的液体不从外环通过过滤器; C。 在外环形空间中没有液体或在外环空中积聚液体在终点下方或前方的水平,并且通过液体出口连续排出来自外环的分离的液体; d。 在分离区内的液体温度下将来自分离区的颗粒通过固体出口分离成低于液体蒸气压的低压,同时在等于或高于液体的蒸汽压力的去耦之前保持颗粒上的压力, 分离区。

    PROCESS FOR REMOVAL OF IMPURITIES FROM MOTHER LIQUOR IN THE SYNTHESIS OF CARBOXYLIC ACID USING PRESSURE FILTRATION
    3.
    发明申请
    PROCESS FOR REMOVAL OF IMPURITIES FROM MOTHER LIQUOR IN THE SYNTHESIS OF CARBOXYLIC ACID USING PRESSURE FILTRATION 有权
    使用压力过滤合成羧酸的方法从母液中除去污染物

    公开(公告)号:US20070284317A1

    公开(公告)日:2007-12-13

    申请号:US11842469

    申请日:2007-08-21

    IPC分类号: B01D37/04 B01D33/06 B01D35/18

    摘要: A process is disclosed that relates to the recovery of a metal catalyst from an oxidizer purge stream produced in the synthesis of carboxylic acid, typically terephthalic. More particularly, the process involves recovery of a metal catalyst from an oxidizer purge stream through the use of a pressure filter, the combining of water with a mother liquor to recover the metal catalyst and then subjecting an aqueous mixture so formed to a single stage extraction with an extraction solvent to produce an extract stream comprising organic impurities and a raffinate stream comprising the metal catalyst.

    摘要翻译: 公开了一种涉及从合成羧酸(通常为对苯二甲酸)中产生的氧化剂清除流回收金属催化剂的方法。 更具体地说,该方法包括通过使用压滤器从氧化剂吹扫流中回收金属催化剂,将水与母液混合以回收金属催化剂,然后将如此形成的含水混合物进行单段萃取 与提取溶剂一起产生包含有机杂质的萃取物流和包含金属催化剂的萃余液流。

    Process for production of a dried carboxylic acid cake suitable for use in polyester production
    8.
    发明申请
    Process for production of a dried carboxylic acid cake suitable for use in polyester production 有权
    生产适用于聚酯生产的干燥羧酸饼的方法

    公开(公告)号:US20050159616A1

    公开(公告)日:2005-07-21

    申请号:US10758676

    申请日:2004-01-15

    IPC分类号: C07C51/47 C07C51/48 C07C51/42

    CPC分类号: C07C51/47 C07C51/48 C07C63/26

    摘要: The present invention relates to a process by which a dried carboxylic acid cake is obtained from a slurry or cake carboxylic acid product through the use of at least one counter current wash. More specifically, the present invention relates to a process by which a dried terephthalic acid cake suitable as a starting material for polyester or co-polyester production is obtained from a slurry or cake terephthalic acid product through the use of at least one counter current wash.

    摘要翻译: 本发明涉及通过使用至少一种逆流洗涤从浆料或蛋糕羧酸产物获得干燥的羧酸饼的方法。 更具体地,本发明涉及通过使用至少一种逆流洗涤从浆液或饼对苯二甲酸产物获得适合作为聚酯或共聚酯生产原料的干燥的对苯二甲酸饼。

    Esterification of an exchange solvent enriched composition
    9.
    发明申请
    Esterification of an exchange solvent enriched composition 审中-公开
    交换溶剂富集组合物的酯化

    公开(公告)号:US20060264664A1

    公开(公告)日:2006-11-23

    申请号:US11365439

    申请日:2006-03-01

    IPC分类号: C07C51/42

    CPC分类号: C07C67/08 C07C69/82

    摘要: A process is provided for producing an enriched carboxylic acid compositions produced by contacting composition comprising a carboxylic acid with an enrichment feed in an enrichment zone to form an enriched carboxylic acid composition. This invention also relates to a process and the resulting compositions for removing catalyst from a carboxylic acid composition to produce a post catalyst removal composition.

    摘要翻译: 提供了一种制备富集的羧酸组合物的方法,该组合物包含羧酸与富集进料在富集区中接触以形成富集的羧酸组合物。 本发明还涉及从羧酸组合物中除去催化剂以产生后催化剂去除组合物的方法和所得组合物。