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公开(公告)号：US5739209A
公开(公告)日：1998-04-14
申请号：US797796
申请日：1997-02-07
CPC分类号： C08G59/5006 , C08G59/4042 , C08G59/50 , C08L63/00
摘要： Reductive alkylation of branched, short chain diamines, such as 2-methyl-1,5-pentanediamine, with certain aldehydes or ketones of moderate molecular weight, such as benzaldehyde or methyl isobutyl ketone, produces novel tri- and difunctional amines which are useful in curing epoxy resins to compositions having improved flexibility and enhanced resistance to moisture and chemicals. Particularly favorable results are achieved when this curative is combined in the epoxy formulation with low molecular weight acrylic copolymers added as flexibilizers. Further improvements are available by including in the recipe monofunctional epoxy or acrylic reactive diluents.
摘要翻译： 支链的短链二胺如2-甲基-1,5-戊二胺与某些中等分子量的醛或酮如苯甲醛或甲基异丁基酮的还原烷基化产生新的三官能和双官能胺，其可用于 将环氧树脂固化成具有改善的柔韧性和增强的抗潮湿和化学物质的组合物。 当将该固化剂与环氧树脂配方和作为增韧剂加入的低分子量丙烯酸共聚物结合时，可以获得特别有利的结果。 通过在配方中包括单官能环氧或丙烯酸反应性稀释剂可以进一步改进。
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公开(公告)号：US20100048833A1
公开(公告)日：2010-02-25
申请号：US12196606
申请日：2008-08-22
申请人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , RIchard V. C. Carr
发明人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , RIchard V. C. Carr
CPC分类号： C08G18/5024 , C08G18/3234 , C08G2150/50 , C09D175/02
摘要： Mixed polycycloaliphatic amines (MPCA) and alkylates thereof (MPCA alkylates), methods for making mixed polycycloaliphatic MPCA amines and MPCA alkylates thereof, as well as polymeric compositions, such as spray-applied polyurea coating compositions, comprising said mixed amines MPCA and MPCA alkylates thereof are described herein. In one embodiment, the polymeric composition comprises an isocyanate component, and a resin component comprising an organic compound having the following Formula I: where R1, R2 and R3 are each independently selected from a hydrogen atom, an alkyl group comprising from 1 to 20 carbon atoms, an aryl group comprising from 3 to 12 carbon atoms, an aralkyl group comprising from 3 to 12 carbon atoms and combinations thereof, provided that there is at least one alkyl group within Formula I, and X is a methylene bridged polycycloaliphatic amine (MPCA).
摘要翻译： 混合多环脂族胺（MPCA）及其烷基化物（MPCA烷基化物），制备混合多环脂肪族MPCA胺及其MPCA烷基化物的方法，以及聚合物组合物，例如喷雾施加的聚脲涂料组合物，其包含所述混合胺MPCA及其MPCA烷基化物 在此描述。 在一个实施方案中，聚合物组合物包含异氰酸酯组分和包含具有下式I的有机化合物的树脂组分：其中R 1，R 2和R 3各自独立地选自氢原子，含有1至20个碳的烷基 原子，包含3至12个碳原子的芳基，含有3至12个碳原子的芳烷基及其组合，条件是式I中至少有一个烷基，X是亚甲基桥连的聚环脂族胺（MPCA ）。
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公开(公告)号：US20100048832A1
公开(公告)日：2010-02-25
申请号：US12196535
申请日：2008-08-22
IPC分类号： C08G18/32 , C08L61/00 , C08L63/00 , C07C211/44
CPC分类号： C07C211/49 , C07C2601/14 , C08G18/10 , C08G59/5033 , C08L63/00 , C09D163/00 , C09D175/02 , C09J163/00 , C08G18/324 , C08G18/5024
摘要： Alkylated 4-aminobenzyl-4-aminocyclohexane curing agents that can be used, for example, in polyurea, polyurethane and urea/urethane hybrid elastomeric, epoxy resin, epoxy adhesive, epoxy composites and/or coating compositions and polymeric compositions comprising these curing agents are provided herein. In one embodiment, the curing agent comprises a compound having the following Formula I: wherein R1 and R2 are each independently a hydrogen, an alkyl group comprising from 1 to 20 carbon atoms, or combinations thereof. In another embodiment, a method of making the polymeric composition comprising the compound having the above Formula I is provided herein.
摘要翻译： 可用于例如聚脲，聚氨酯和尿素/聚氨酯混合弹性体，环氧树脂，环氧粘合剂，环氧复合材料和/或涂料组合物和包含这些固化剂的聚合物组合物中的烷基化4-氨基苄基-4-氨基环己烷固化剂是 本文提供。 在一个实施方案中，固化剂包含具有下式I的化合物：其中R 1和R 2各自独立地为氢，包含1至20个碳原子的烷基或其组合。 在另一个实施方案中，本文提供了制备包含具有上述式I的化合物的聚合物组合物的方法。
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公开(公告)号：US08759470B2
公开(公告)日：2014-06-24
申请号：US13216687
申请日：2011-08-24
申请人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , Richard V. C. Carr
发明人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , Richard V. C. Carr
IPC分类号： C08G18/32
CPC分类号： C08G18/5024 , C08G18/3234 , C08G2150/50 , C09D175/02
摘要： Mixed polycycloaliphatic amines (MPCA) and alkylates thereof (MPCA alkylates), methods for making mixed polycycloaliphatic MPCA amines and MPCA alkylates thereof, as well as polymeric compositions, such as spray-applied polyurea coating compositions, comprising said mixed amines MPCA and MPCA alkylates thereof are described herein. In one embodiment, the polymeric composition comprises an isocyanate component, and a resin component comprising an organic compound having the following Formula I: where R1, R2 and R3 are each independently selected from a hydrogen atom, an alkyl group comprising from 1 to 20 carbon atoms, an aryl group comprising from 3 to 12 carbon atoms, an aralkyl group comprising from 3 to 12 carbon atoms and combinations thereof, provided that there is at least one alkyl group within Formula I, and X is a methylene bridged polycycloaliphatic amine (MPCA).
摘要翻译： 混合多环脂族胺（MPCA）及其烷基化物（MPCA烷基化物），制备混合多环脂肪族MPCA胺及其MPCA烷基化物的方法，以及聚合物组合物，例如喷雾施加的聚脲涂料组合物，其包含所述混合胺MPCA及其MPCA烷基化物 在此描述。 在一个实施方案中，聚合物组合物包含异氰酸酯组分和包含具有下式I的有机化合物的树脂组分：其中R 1，R 2和R 3各自独立地选自氢原子，含有1至20个碳的烷基 原子，包含3至12个碳原子的芳基，含有3至12个碳原子的芳烷基及其组合，条件是式I中至少有一个烷基，X是亚甲基桥连的聚环脂族胺（MPCA ）。
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公开(公告)号：US08373287B2
公开(公告)日：2013-02-12
申请号：US13058688
申请日：2009-08-10
申请人： William Franklin Burgoyne, Jr. , Mark David Conner , Andrew Francis Nordquist , William Steven Collins
发明人： William Franklin Burgoyne, Jr. , Mark David Conner , Andrew Francis Nordquist , William Steven Collins
IPC分类号： H01L23/29
摘要： A polymeric composition comprising a first polymer chosen from a poly(arylene ether) polymer including polymer repeat units of the following structure: —(O—Ar1—O—Ar2—O—)m—(—O—Ar3—O—Ar4—O)n- where Ar1, Ar2, Ar3, and Ar4 are identical or different aryl radicals, m is 0 to 1, n is 1 m; a polysulfone, a polyimide, a poly(etherketone), a polyurea, a polyurethane, and combinations thereof and a second polymer comprising a per(phenylethynyl) arene polymer derivative. Cured films containing the polymer can exhibit at least one of the following properties: Tg from 160° C. to 180° C., a dielectric constant below 2.7 with frequency independence, and a maximum moisture absorption of less than 0.17 wt %. Accordingly, the polymer is especially useful, for example, in interlayer dielectrics and in die-attach adhesives.
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6.发明授权
公开(公告)号：US5698657A
公开(公告)日：1997-12-16
申请号：US510728
申请日：1995-08-03
CPC分类号： C08G59/4042 , C08G59/50 , C08G59/5006 , C08L63/00
摘要： Flexible epoxy resins are made by curing the epoxy with an amine curing agent in the presence of a low molecular weight acrylate copolymer made from a major amount of a lower aliphatic ester or amide of acrylic or methacrylic acid and a minor amount of an ethylenically unsaturated monomer having functionality reactive with functional groups present in the epoxy resin or its curing agent. The acrylate copolymer has a number average molecular weight in the range of 1000 to 6000, preferably 2000 to 3000, and a ratio of weight average to number average molecular weight in the range of 1 to 3.5. Copolymers of butylacrylate and acrylic acid or maleic anhydride are favored. Further advantages are realized by including in the cure formulation a monofunctional diluent reactive with the curative.
摘要翻译： 柔性环氧树脂通过在由主要量的丙烯酸或甲基丙烯酸的低级脂族酯或酰胺和少量烯属不饱和单体制备的低分子量丙烯酸酯共聚物的存在下，用胺固化剂固化环氧树脂 具有与存在于环氧树脂或其固化剂中的官能团反应的官能度。 丙烯酸酯共聚物的数均分子量为1000〜6000，优选为2000〜3000，重均分子量与数均分子量的比例为1〜3.5。 丙烯酸丁酯和丙烯酸或马来酸酐的共聚物是有利的。 通过在固化制剂中包含与治疗剂反应的单官能稀释剂来实现其它优点。
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公开(公告)号：US20110301318A1
公开(公告)日：2011-12-08
申请号：US13216687
申请日：2011-08-24
申请人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , RIchard V.C. Carr
发明人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , RIchard V.C. Carr
IPC分类号： C08G18/32
CPC分类号： C08G18/5024 , C08G18/3234 , C08G2150/50 , C09D175/02
摘要： Mixed polycycloaliphatic amines (MPCA) and alkylates thereof (MPCA alkylates), methods for making mixed polycycloaliphatic MPCA amines and MPCA alkylates thereof, as well as polymeric compositions, such as spray-applied polyurea coating compositions, comprising said mixed amines MPCA and MPCA alkylates thereof are described herein. In one embodiment, the polymeric composition comprises an isocyanate component, and a resin component comprising an organic compound having the following Formula I: where R1, R2 and R3 are each independently selected from a hydrogen atom, an alkyl group comprising from 1 to 20 carbon atoms, an aryl group comprising from 3 to 12 carbon atoms, an aralkyl group comprising from 3 to 12 carbon atoms and combinations thereof, provided that there is at least one alkyl group within Formula I, and X is a methylene bridged polycycloaliphatic amine (MPCA).
摘要翻译： 混合多环脂族胺（MPCA）及其烷基化物（MPCA烷基化物），制备混合多环脂肪族MPCA胺及其MPCA烷基化物的方法，以及聚合物组合物，例如喷雾施加的聚脲涂料组合物，其包含所述混合胺MPCA及其MPCA烷基化物 在此描述。 在一个实施方案中，聚合物组合物包含异氰酸酯组分和包含具有下式I的有机化合物的树脂组分：其中R 1，R 2和R 3各自独立地选自氢原子，含有1至20个碳的烷基 原子，包含3至12个碳原子的芳基，含有3至12个碳原子的芳烷基及其组合，条件是式I中至少有一个烷基，X是亚甲基桥连的聚环脂族胺（MPCA ）。
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8.发明申请公开(公告)号：US20110260343A1
公开(公告)日：2011-10-27
申请号：US13058688
申请日：2009-08-10
申请人： William Franklin Burgoyne, JR. , Mark David Conner , Andrew Francis Nordquist , William Steven Collins
发明人： William Franklin Burgoyne, JR. , Mark David Conner , Andrew Francis Nordquist , William Steven Collins
CPC分类号： C08G65/48 , C08G2261/3422 , C08L65/00 , C08L71/00 , C08L79/08 , H01L2924/0002 , C08L2666/22 , H01L2924/00
摘要： A polymeric composition comprising a first polymer chosen from a poly(arylene ether) polymer including polymer repeat units of the following structure: —(O—Ar1—O—Ar2—O—)m—(—O—Ar3—O—Ar4—O)n- where Ar1, Ar2, Ar3, and Ar4 are identical or different aryl radicals, m is 0 to 1, n is 1 m; a polysulfone, a polyimide, a poly(etherketone), a polyurea, a polyurethane, and combinations thereof and a second polymer comprising a per(phenylethynyl) arene polymer derivative. Cured films containing the polymer can exhibit at least one of the following properties: Tg from 160° C. to 180° C., a dielectric constant below 2.7 with frequency independence, and a maximum moisture absorption of less than 0.17 wt %. Accordingly, the polymer is especially useful, for example, in interlayer dielectrics and in die-attach adhesives.
摘要翻译： 一种聚合物组合物，其包含选自包含以下结构的聚合物重复单元的聚（亚芳基醚）聚合物的第一聚合物： - （O-Ar1-O-Ar2-O-）m - （ - O-Ar3-O-Ar4- 其中Ar 1，Ar 2，Ar 3和Ar 4为相同或不同的芳基，m为0至1，n为1; 聚砜，聚酰亚胺，聚（醚酮），聚脲，聚氨酯及其组合，以及包含全（苯基乙炔基）芳烃聚合物衍生物的第二聚合物。 含有该聚合物的固化膜可呈现以下特性中的至少一种：Tg为160℃至180℃，介电常数低于2.7，频率独立，最大吸湿率小于0.17重量％。 因此，聚合物特别适用于例如层间电介质和芯片附着粘合剂中。
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公开(公告)号：US08026318B2
公开(公告)日：2011-09-27
申请号：US12196606
申请日：2008-08-22
申请人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , Richard V. C. Carr
发明人： Mark David Conner , Gamini Ananda Vedage , Peter Andrew Lucas , Courtney Thompson Thurau , Richard V. C. Carr
CPC分类号： C08G18/5024 , C08G18/3234 , C08G2150/50 , C09D175/02
摘要： Mixed polycycloaliphatic amines (MPCA) and alkylates thereof (MPCA alkylates), methods for making mixed polycycloaliphatic MPCA amines and MPCA alkylates thereof, as well as polymeric compositions, such as spray-applied polyurea coating compositions, comprising said mixed amines MPCA and MPCA alkylates thereof are described herein. In one embodiment, the polymeric composition comprises an isocyanate component, and a resin component comprising an organic compound having the following Formula I: where R1, R2 and R3 are each independently selected from a hydrogen atom, an alkyl group comprising from 1 to 20 carbon atoms, an aryl group comprising from 3 to 12 carbon atoms, an aralkyl group comprising from 3 to 12 carbon atoms and combinations thereof, provided that there is at least one alkyl group within Formula I, and X is a methylene bridged polycycloaliphatic amine (MPCA).
摘要翻译： 混合多环脂族胺（MPCA）及其烷基化物（MPCA烷基化物），制备混合多环脂肪族MPCA胺及其MPCA烷基化物的方法，以及聚合物组合物，例如喷雾施加的聚脲涂料组合物，其包含所述混合胺MPCA及其MPCA烷基化物 在此描述。 在一个实施方案中，聚合物组合物包含异氰酸酯组分和包含具有下式I的有机化合物的树脂组分：其中R 1，R 2和R 3各自独立地选自氢原子，含有1至20个碳的烷基 原子，包含3至12个碳原子的芳基，含有3至12个碳原子的芳烷基及其组合，条件是式I中至少有一个烷基，X是亚甲基桥连的聚环脂族胺（MPCA ）。
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10.发明授权公开(公告)号：US08502401B2
公开(公告)日：2013-08-06
申请号：US13058688
申请日：2009-08-10
申请人： William Franklin Burgoyne, Jr. , Mark David Conner , Andrew Francis Nordquist , William Steven Collins
发明人： William Franklin Burgoyne, Jr. , Mark David Conner , Andrew Francis Nordquist , William Steven Collins
IPC分类号： H01L23/29
CPC分类号： C08G65/48 , C08G2261/3422 , C08L65/00 , C08L71/00 , C08L79/08 , H01L2924/0002 , C08L2666/22 , H01L2924/00
摘要： A polymeric composition comprising a first polymer chosen from a poly(arylene ether) polymer including polymer repeat units of the following structure: —(O—Ar1—O—Ar2—O—)m—(—O—Ar3—O—Ar4—O)n- where Ar1, Ar2, Ar3, and Ar4 are identical or different aryl radicals, m is 0 to 1, n is 1 m; a polysulfone, a polyimide, a poly(etherketone), a polyurea, a polyurethane, and combinations thereof and a second polymer comprising a per(phenylethynyl) arene polymer derivative. Cured films containing the polymer can exhibit at least one of the following properties: Tg from 160° C. to 180° C., a dielectric constant below 2.7 with frequency independence, and a maximum moisture absorption of less than 0.17 wt %. Accordingly, the polymer is especially useful, for example, in interlayer dielectrics and in die-attach adhesives.
摘要翻译： 一种聚合物组合物，其包含选自包含以下结构的聚合物重复单元的聚（亚芳基醚）聚合物的第一聚合物： - （O-Ar1-O-Ar2-O-）m - （ - O-Ar3-O-Ar4- 其中Ar 1，Ar 2，Ar 3和Ar 4为相同或不同的芳基，m为0至1，n为1; 聚砜，聚酰亚胺，聚（醚酮），聚脲，聚氨酯及其组合，以及包含全（苯基乙炔基）芳烃聚合物衍生物的第二聚合物。 含有该聚合物的固化膜可呈现以下特性中的至少一种：Tg为160℃至180℃，介电常数低于2.7，频率独立，最大吸湿率小于0.17重量％。 因此，聚合物特别适用于例如层间电介质和芯片附着粘合剂中。
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