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59 条记录 (耗时 0.018 秒)

    Process for making manganese (II) salt solutions containing ammonium salt
    1.
    发明授权
    Process for making manganese (II) salt solutions containing ammonium salt 失效
    制备含有铵盐的锰（II）盐溶液的方法

    公开(公告)号：US4600565A

    公开(公告)日：1986-07-15

    申请号：US708299

    申请日：1985-03-05

    申请人： Klaus Lehr ,  Bernhard Hofmann ,  Gero Heymer

    发明人： Klaus Lehr ,  Bernhard Hofmann ,  Gero Heymer

    IPC分类号： C01G45/00 ,  C22B47/00

    CPC分类号： C01G45/00 ,  C22B47/00

    摘要： Manganese(II)salt solutions containing ammonium salt are made by subjecting a manganese-containing compound to processing treatment with an ammonium salt solution. A boiling temperature of 57.degree.-68.degree. C. is established in the suspension to be subjected to the processing treatment, by application of a vacuum. The ammonium salt solution used contains 0.5-2.5 mol/l diammonium sulfate or 1.0-5.0 mol/l ammonium nitrate.

    摘要翻译： 含有铵盐的锰（II）盐溶液通过使含锰化合物用铵盐溶液进行处理来制备。 通过施加真空在待处理处理的悬浮液中建立沸点为57-68℃的温度。 使用的铵盐溶液含有0.5-2.5mol / l硫酸二铵或1.0-5.0mol / l硝酸铵。

    Process for removing nitrogen dioxide from off-gas
    2.
    发明授权
    Process for removing nitrogen dioxide from off-gas 失效
    从废气中除去二氧化氮的方法

    公开(公告)号：US4482527A

    公开(公告)日：1984-11-13

    申请号：US538130

    申请日：1983-10-03

    申请人： Klaus Lehr ,  Gero Heymer

    发明人： Klaus Lehr ,  Gero Heymer

    IPC分类号： B01D53/56 ,  C01B21/00 ,  B01J8/00

    CPC分类号： B01D53/56 ,  Y02C20/10

    摘要： The disclosure relates to a process for removing nitrogen dioxide from off-gas. To this end, the disclosure provides for the off-gas to be intimately contacted with a suspension consisting of red phosphorus and a liquid being inert with respect to red phosphorus, e.g. water.

    摘要翻译： 本公开涉及从废气中除去二氧化氮的方法。 为此，本公开内容提供废气与由红磷和相对于红磷惰性的液体组成的悬浮液紧密接触。 水。

    Process for making red phosphorus
    3.
    发明授权
    Process for making red phosphorus 失效
    制造红磷的工艺

    公开(公告)号：US4273752A

    公开(公告)日：1981-06-16

    申请号：US123106

    申请日：1980-02-20

    申请人： Klaus Lehr ,  Gero Heymer ,  Hans-Werner Stephan ,  Ursus Thummler

    发明人： Klaus Lehr ,  Gero Heymer ,  Hans-Werner Stephan ,  Ursus Thummler

    IPC分类号： B01J8/10 ,  B01J19/28 ,  B02C17/00 ,  C01B25/02 ,  C01B25/023 ,  C01B25/01 ,  C01B25/04

    CPC分类号： C01B25/023

    摘要： The invention relates to a process for making red phosphorus by subjecting molten yellow phosphorus to a thermal conversion reaction in a closed reaction zone. To this end, a hollow shaft-provided and closed ball mill is preheated to a reaction temperature within the range 280.degree. to 590.degree. C. Yellow phosphorus is continuously introduced into the ball mill through the hollow shaft in quantities per unit time which permit the reaction temperature prevailing inside the ball mill to be maintained without supply of heat from the outside. More particularly, decreasing quantities of yellow phosphorus are introduced per unit time at increasing temperature and increasing quantities of yellow phosphorus are introduced per unit time at decreasing temperature within the limits specified. Red phosphorus is allowed to cool inside the ball mill, water is poured over it and the whole is subjected to wet-grinding. An aqueous suspension of red phosphorus is finally removed from the ball mill.

    摘要翻译： 本发明涉及通过使熔融黄磷在封闭反应区中进行热转化反应来制备红磷的方法。 为此，空心轴提供和封闭的球磨机被预热到280℃至590℃的反应温度。黄磷通过空心轴以每单位时间的量连续地引入球磨机，这允许 球磨机内部的反应温度保持不受外界的热量的限制。 更特别地，在增加的温度下每单位时间引入黄磷的减少量，并且在规定的限度内在降低的温度下每单位时间引入增加量的黄磷。 使红磷在球磨机内冷却，将水倒在其上，整体进行湿磨。 最终从球磨机中除去红磷水悬浮液。

    Process for separating metals from aqueous solutions
    4.
    发明授权
    Process for separating metals from aqueous solutions 失效
    从水溶液中分离金属的工艺

    公开(公告)号：US4418043A

    公开(公告)日：1983-11-29

    申请号：US288667

    申请日：1981-07-30

    申请人： Klaus Lehr ,  Gero Heymer

    发明人： Klaus Lehr ,  Gero Heymer

    IPC分类号： C22B43/00 ,  C01G1/00 ,  C01G3/00 ,  C01G5/00 ,  C01G13/00 ,  C01G55/00 ,  C02F1/28 ,  C22B11/00 ,  C22B15/00 ,  C01G7/00

    CPC分类号： C02F1/288 ,  C02F1/281 ,  C22B11/04 ,  C22B3/24 ,  Y02P10/234 ,  Y10S210/912

    摘要： The invention relates to a process for separating seminoble metals or noble metals from aqueous solutions having compounds of these metals dissolved therein, by reaction with yellow phosphorus. More particularly the aqueous solutions are contacted with carrier material having a yellow phosphorus coating applied thereto.It is possible for the aqueous solutions to be conveyed through a zone having the yellow phosphorus-coated carrier material placed therein, and for them to be subsequently conveyed through a further zone having uncoated carrier material placed therein.

    摘要翻译： 本发明涉及通过与黄磷反应从其中溶解有这些金属的化合物的水溶液中分离出含半金属或贵金属的方法。 更具体地，水溶液与其上施加有黄磷涂层的载体材料接触。 水溶液可以通过其中放置有黄磷涂层的载体材料的区域输送，并且随后将其输送通过其中放置有未涂覆的载体材料的另一区域。

    Apparatus for making red phosphorus
    6.
    发明授权
    Apparatus for making red phosphorus 失效
    制备红磷的装置

    公开(公告)号：US4330504A

    公开(公告)日：1982-05-18

    申请号：US226468

    申请日：1981-01-19

    申请人： Klaus Lehr ,  Gero Heymer ,  Hans-Werner Stephan ,  Ursus Thummler

    发明人： Klaus Lehr ,  Gero Heymer ,  Hans-Werner Stephan ,  Ursus Thummler

    IPC分类号： B01J8/10 ,  B01J19/28 ,  B02C17/00 ,  C01B25/02 ,  C01B25/023

    CPC分类号： C01B25/023

    摘要： The invention relates to an apparatus for making red phosphorus by subjecting molten yellow phosphorus to a thermal conversion reaction in a closed reaction zone. To this end, a hollow shaft-provided and closed ball mill is preheated to a reaction temperature within the range 280.degree. to 590.degree. C. Yellow phosphorus is continuously introduced into the ball mill through the hollow shaft in quantities per unit time which permit the reaction temperature prevailing inside the ball mill to be maintained without supply of heat from the outside. More particularly, decreasing quantities of yellow phosphorous are introduced per unit time at increasing temperature and increasing quantities of yellow phosphorus are introduced per unit time at decreasing temperature within the limits specified. Red phosphorus is allowed to cool inside the ball mill, water is poured over it and the whole is subjected to wet-grinding. An aqueous suspension of red phosphorus is finally removed from the ball mill.

    摘要翻译： 本发明涉及一种通过使熔融黄磷在封闭反应区中进行热转化反应来制备红磷的装置。 为此，空心轴提供和封闭的球磨机被预热到280℃至590℃的反应温度。黄磷通过空心轴以每单位时间的量连续地引入球磨机，这允许 球磨机内部的反应温度保持不受外界的热量的限制。 更特别地，在增加的温度下每单位时间引入黄磷的量减少，并且在规定的限度内在逐渐降低的温度下每单位时间引入增加量的黄磷。 使红磷在球磨机内冷却，将水倒在其上，整体进行湿磨。 最终从球磨机中除去红磷水悬浮液。

    Process for making an alkali phosphate solution
    8.
    发明授权
    Process for making an alkali phosphate solution 失效
    碱式磷酸盐溶液的制备方法

    公开(公告)号：US4678650A

    公开(公告)日：1987-07-07

    申请号：US715167

    申请日：1985-03-22

    申请人： Reinhard Gradl ,  Gero Heymer

    发明人： Reinhard Gradl ,  Gero Heymer

    IPC分类号： C01B25/46 ,  C01B15/16

    CPC分类号： C01B25/46

    摘要： An aqueous alkali phosphate solution is made. An organic phase is countercurrently mixed with an aqueous phase, the two phases being used in a volume ratio larger than 1:1 and formed aqueous alkali phosphate solution is separated from the remaining organic phase. The two phases are mixed and reacted in a reaction zone comprised of a mixing and separating zone. The organic phase is continuously dispersed in the aqueous phase. A volume excess of aqueous phase is maintained in the mixing zone and the two phases are used in an overall quantity sufficient to provide a volume ratio of organic to aqueous phase of 4:6 to 2:8.

    摘要翻译： 制备磷酸碱水溶液。 有机相与水相逆流混合，两相以体积比大于1:1使用，形成的碱式磷酸碱水溶液与剩余的有机相分离。 将两相混合并在由混合和分离区组成的反应区中反应。 有机相连续分散在水相中。 在混合区中维持体积过量的水相，并且两相的使用量足以提供4:6至2:8的有机相与水相的体积比。