利索-全球专利检索

  1. 登录
  2. 注册

搜索结果

19 条记录 (耗时 0.017 秒)

    Regenerator of acid reaction lubricant residues
    1.
    发明授权
    Regenerator of acid reaction lubricant residues 有权
    酸反应润滑剂残渣再生剂

    公开(公告)号：US06479439B1

    公开(公告)日：2002-11-12

    申请号：US09509696

    申请日：2000-11-06

    申请人： Klaus-Dieter Nittel ,  Uwe Rau ,  Norbert Schwinke-Kruse

    发明人： Klaus-Dieter Nittel ,  Uwe Rau ,  Norbert Schwinke-Kruse

    IPC分类号： C10G7100

    CPC分类号： C10M175/02 ,  B01D17/00 ,  B01D17/0217 ,  B01D21/262

    摘要： The invention relates to a method for regenerating reaction lubricant residues containing acid organic lubricants refused and processed during cold forming and multivalent metal ions and phosphate ions, wherein said reaction lubricant residues undergo the following procedural steps: a) precipitating metal ions from the metal organic compounds by adding phosphoric acid and/or acid phosphoric acid esters; b) dissolving water-soluble impurities by adding water; c) separating the solids from the lubricant components and from the aqueous phases that are incompatible with the oily lubricant components, and whereby d) acid phosphoric acid esters for adjusting the free acid at a value of less than 10 points and for adjusting a total acidity point value of less than 70 is adjusted at a free acid. total acidity ratio having a value in the range of 0.15 to 0.5. The separation indicated in step c) preferably occurs by means of a centrifuge at 2,000 to 3,000 g, especially at 8,000 to 15,000 g.

    摘要翻译： 本发明涉及一种用于再生含有在冷成型期间拒绝和加工的酸性有机润滑剂和多价金属离子和磷酸根离子的反应润滑剂残留物的方法，其中所述反应润滑剂残余物经历以下程序步骤：a）从金属有机化合物沉淀金属离子 通过加入磷酸和/或酸式磷酸酯; b）通过加水溶解水溶性杂质; c）将固体与润滑剂组分和与油性润滑剂组分不相容的水相分离，并且由此d）用于调节游离酸的值小于10分的酸性磷酸酯和用于调节总酸度 小于70的点值在游离酸下调节。 总酸度比的值在0.15〜0.5的范围内。 步骤c）中所示的分离优选通过2,000至3,000g，特别是8,000至15,000g的离心机进行。

    Lubricant for metal forming
    3.
    发明授权
    Lubricant for metal forming 有权
    用于金属成型的润滑剂

    公开(公告)号：US06034041A

    公开(公告)日：2000-03-07

    申请号：US137804

    申请日：1998-08-20

    申请人： Klaus-Dieter Nittel ,  Norbert Schwinke-Kruse ,  Gunter Hesse

    发明人： Klaus-Dieter Nittel ,  Norbert Schwinke-Kruse ,  Gunter Hesse

    IPC分类号： C10M173/02 ,  C10M157/00

    CPC分类号： C10M173/02 ,  C10M2201/02 ,  C10M2201/041 ,  C10M2201/042 ,  C10M2201/066 ,  C10M2201/085 ,  C10M2201/087 ,  C10M2205/022 ,  C10M2205/04 ,  C10M2205/14 ,  C10M2209/084 ,  C10M2209/104 ,  C10M2209/108 ,  C10M2219/044 ,  C10N2220/02 ,  C10N2240/402 ,  C10N2240/403 ,  C10N2240/404 ,  C10N2240/405 ,  C10N2240/406 ,  C10N2240/407 ,  C10N2240/408 ,  C10N2240/409 ,  C10N2250/02

    摘要： Disclosed is a solid or aqueous lubricant concentrate used for the cold forming of metals, which, with reference to the solids content, including a) 20 to 50 parts by weight polyethylene with a softening point above 120.degree. C. and a particle size int he range between 0.1 and 50 .mu.m; b) 20 to 8 parts by weight polyacrylate with a molecular weight of 4,500 to 10,000 and c) 2 to 8 parts by weight styrene/acrylic acid copolymer with a molecular weight of 150,000 to 250,000 and a glass transition temperature of 45 to 55.degree. C., where, under the conditions of use, the acrylic acid component of the polymers in accordance with items b) and c) is predominantly present as salt of one or more inorganic cations, and the softening points of the individuals polymers are distributed over the temperature range defined by the limiting values of ambient temperature and 200.degree. C. The lubricant concentrate may contain homo-or copolymers or acrylic acid or the esters thereof with graded molecular weights as well as surfacant. Also disclosed is a method for facilitating the cold forming, where, by means of the lubricant concentrate, a lubricant film is applied on the workpiece from a dispersion having solids content of 5 to 25 wt-%.

    摘要翻译： 公开了用于冷成型金属的固体或水性润滑剂浓缩物，其相对于固体含量，包括a）20至50重量份的软化点高于120℃的聚乙烯和其粒径 范围在0.1到50微米之间; b）20至8重量份的分子量为4,500至10,000的聚丙烯酸酯和c）2至8重量份的苯乙烯/丙烯酸共聚物，分子量为150,000至250,000，玻璃化转变温度为45至55℃ 其中，在使用条件下，根据项目b）和c）的聚合物的丙烯酸组分主要作为一种或多种无机阳离子的盐存在，并且个体聚合物的软化点分布在 温度范围由环境温度和200℃的限制值限定。润滑剂浓缩物可以含有均匀或共聚物或具有分级分子量和表面活性剂的丙烯酸或其酯。 还公开了一种促进冷成型的方法，其中通过润滑剂浓缩物，将润滑剂膜从具有5至25重量％的固体含量的分散体施加在工件上。

    Preparation of workpieces for cold forming
    5.
    发明授权
    Preparation of workpieces for cold forming 失效
    冷成型工件的制备

    公开(公告)号：US06482273B1

    公开(公告)日：2002-11-19

    申请号：US09787043

    申请日：2001-04-06

    申请人： Klaus-Dieter Nittel ,  Uwe Rau

    发明人： Klaus-Dieter Nittel ,  Uwe Rau

    IPC分类号： C23C2200

    CPC分类号： C23C22/78

    摘要： The invention relates to a method for preparing workpieces suitable for phosphatizing for chipless cold forming by acid pickling, rinsing, drying and treatment with acid reaction lubricants containing phosphate ions. According to said method the workpieces are rinsed before drying with a solution which contains lactic acid, has a pH below 3 and preferably a temperature of between 60 and 80° C. Preferred embodiments of the invention consist of rinsing the workpieces with a solution which in addition contains phosphoric acid, has a lactic acid concentration of between 1 and 50 g/l and a weight ratio of lactic acid to phosphoric acid of between 1:9 and 9:1.

    摘要翻译： 本发明涉及一种适用于通过酸洗，漂洗，干燥和含有磷酸根离子的酸反应润滑剂进行处理的用于无酸冷成型的工件的制备方法。 根据所述方法，在用含有乳酸的溶液干燥之前将工件漂洗，pH低于3，优选温度在60至80℃之间。本发明的优选实施方案包括用溶液冲洗工件， 添加含有磷酸，乳酸浓度为1〜50g / l，乳酸与磷酸的重量比为1：9〜9：1。

    Concentrate for the electroless deposition of copper coatings on iron and iron alloy surfaces
    6.
    发明授权
    Concentrate for the electroless deposition of copper coatings on iron and iron alloy surfaces 失效
    集中在铁和铁合金表面上的铜涂层的无电沉积

    公开(公告)号：US5776231A

    公开(公告)日：1998-07-07

    申请号：US802029

    申请日：1997-02-18

    申请人： Klaus-Dieter Nittel ,  Karl-Heinz Nuss

    发明人： Klaus-Dieter Nittel ,  Karl-Heinz Nuss

    IPC分类号： C23C18/38 ,  B22F7/00

    CPC分类号： C23C18/38

    摘要： Disclosed is a process for the electroless deposition of a copper coating on an iron or iron alloy surface wherein the workpiece surface is contacted with a solution which contains hydrogen ions, 5 to 30 g/l Cu as well as 0.2 to 5 g/l Mg and preferably copper and magnesium with a weight ratio of Cu:Mg of (35 to 5):1 for a treatment time of 3 sec to 15 min at a temperature of the solution of 20.degree. to 65.degree. C. The invention also comprises a solid concentrate for preparing and replenishing the solution for carrying out the process, which consists of at least 85 wt-% CuSO.sub.4.5H.sub.2 O and MgSO.sub.4 (anhydrous) with a weight ratio of (35 to 5):1, and preferably contains in addition a maximum of 10 wt-% polyglycol and a maximum of 5 wt-% sodium chloride.

    摘要翻译： 公开了一种在铁或铁合金表面上无电沉积铜涂层的方法，其中工件表面与含有氢离子的溶液接触，5至30g / l的Cu以及0.2至5g / l的Mg 优选铜和镁的重量比为（35〜5）：1，在20〜65℃的温度下处理时间为3秒〜15分钟。本发明还包括 用于制备和补充用于进行该方法的溶液的固体浓缩物，其由至少85重量％的重量比为（35至5）：1的CuSO 4·5H 2 O和MgSO 4（无水）组成，并且优选还包含 最多10重量％的聚乙二醇和最多5重量％的氯化钠。

    Process for the electroless deposition of copper coatings on iron and iron alloy surfaces
    10.
    发明授权
    Process for the electroless deposition of copper coatings on iron and iron alloy surfaces 失效
    铜涂层在铁和铁合金表面上的无电沉积工艺

    公开(公告)号：US06261644B1

    公开(公告)日：2001-07-17

    申请号：US08554288

    申请日：1995-11-06

    申请人： Klaus-Dieter Nittel ,  Karl-Heinz Nuss

    发明人： Klaus-Dieter Nittel ,  Karl-Heinz Nuss

    IPC分类号： B05D118

    CPC分类号： C23C18/38

    摘要： Disclosed is a process for the electroless deposition of a copper coating on an iron or iron alloy surface wherein the workpiece surface is contacted with a solution which contains hydrogen ions, 5 to 30 g/l Cu as well as 0.2 to 5 g/l Mg and preferably copper and magnesium with a weight ratio of Cu:Mg of (35 to 5):1 for a treatment time of 3 sec to 15 min at a temperature of the solution of 20 to 65° C.

    摘要翻译： 公开了一种在铁或铁合金表面上无电沉积铜涂层的方法，其中工件表面与含有氢离子的溶液接触，5至30g / l的Cu以及0.2至5g / l的Mg 优选Cu:Mg为（35〜5）：1的铜和镁，在20〜65℃的溶液温度下处理时间为3秒〜15分钟。