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1.发明授权公开(公告)号：US06716792B2
公开(公告)日：2004-04-06
申请号：US09881214
申请日：2001-06-15
申请人： Kuniaki Okamoto , Mutsumi Sato , Atsunori Sano
发明人： Kuniaki Okamoto , Mutsumi Sato , Atsunori Sano
IPC分类号： B01J2026
CPC分类号： C08F8/42 , B01J23/466 , B01J31/06 , B01J31/1625 , C08K2201/013
摘要： The present invention relates to {circle around (1)} a metal oxide or metallic Lewis acid composition comprising the metal oxide or the metallic Lewis acid carried on a cross-linked polymer compound, {circle around (2)} a metal compound composition comprising the metal compound carried on a cross-linked product of a polymer compound containing a cross-linkable condensing functional group and/or a polymer containing a polymerizable double bond formed by a condensation reaction, {circle around (3)} a method for producing a metal compound composition comprising the metal compound carried on a cross-linked polymer compound, which comprises mixing a non-cross-linked polymer compound containing a cross-linkable condensing functional group and/or a polymer compound containing a polymerizable double bond formed by a condensation reaction with a metal compound, and then cross-linking the polymer compound, {circle around (4)} a carrier for carrying a metal compound comprising a 1st polymer compound containing a cross-linkable condensing functional group and/or a 2nd polymer compound containing a polymerizable double bond formed by a condensation reaction as a non-cross-linked polymer compound and {circle around (5)} a method for improving solvent resistance, heat resistance and durability of a metal compound comprising mixing a non-cross-linked polymer compound containing a cross-linkable condensing functional group and/or a polymer compound containing a polymerizable double bond formed by a condensation reaction with a metal compound, and then cross-linking said polymer compounds.
摘要翻译： 本发明涉及{围绕（1个金属氧化物或金属路易斯酸组合物，其包含金属氧化物或交联聚合物化合物上携带的金属路易斯酸，{圆周（2为包含载有金属化合物的金属化合物组合物 在含有可交联缩合官能团的高分子化合物和/或含有通过缩合反应形成的可聚合双键的聚合物的交联产物上，{圆周（3）制备包含该金属的金属化合物组合物的方法 在交联聚合物化合物上携带的化合物，其包括将含有可交联缩合官能团的非交联聚合物化合物和/或含有通过缩合反应形成的可聚合双键的高分子化合物与金属化合物混合， 然后交联高分子化合物{圆周（4是用于承载包含第1聚合物化合物的金属化合物的载体） 制备可交联的缩合官能团和/或含有通过缩合反应形成的可聚合双键的第二聚合物化合物作为非交联聚合物化合物和{圆周（5）一种提高耐溶剂性，耐热性和 金属化合物的耐久性包括将含有可交联缩合官能团的非交联聚合物化合物和/或含有通过缩合反应形成的可聚合双键的高分子化合物与金属化合物混合，然后将所述 聚合物化合物。
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公开(公告)号：US5516919A
公开(公告)日：1996-05-14
申请号：US423988
申请日：1995-04-18
申请人： Atsunori Sano , Kuniaki Okamoto , Jun Ebashi
发明人： Atsunori Sano , Kuniaki Okamoto , Jun Ebashi
IPC分类号： C07F9/655 , C07D307/62
CPC分类号： C07F9/65515
摘要： Metal salts or substitutted or non-substituted ammonium salts of ascorbic acid derivatives can be produced in high yield by treating an acidic aqueous solution containing ascorbic acid-2-phosphate or ascorbic acid-2-sulfate with a porous adsorbent such as activated carbon, followed by treating the adsorbent with a basic aqueous solution containing e.g. a metal salt of an organic acid or substituted or non-substituted ammonium salt ion to elute the desired salt of ascorbic acid derivative.
摘要翻译： 通过用多孔吸附剂如活性炭处理含有抗坏血酸-2-磷酸或抗坏血酸-2-硫酸的酸性水溶液，可以高收率地生产抗坏血酸衍生物的金属盐或取代或未取代的铵盐，随后 通过用含有例如的碱性水溶液处理吸附剂 有机酸的金属盐或取代或未取代的铵盐离子洗脱所需的抗坏血酸衍生物盐。
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公开(公告)号：US06566572B2
公开(公告)日：2003-05-20
申请号：US09788550
申请日：2001-02-21
申请人： Kuniaki Okamoto , Tomimasa Kurita , Atsunori Sano
发明人： Kuniaki Okamoto , Tomimasa Kurita , Atsunori Sano
IPC分类号： C07C128
摘要： 9,10-Diphenylanthracene, which can be produced applicably for industrial use in one or two process steps by subjecting a 9,10-dihalogenoanthracene and a metal or half-metal phenyl compound to a cross-coupling reaction.
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4.发明授权公开(公告)号：US09190695B2
公开(公告)日：2015-11-17
申请号：US13814291
申请日：2011-08-02
IPC分类号： H01M10/056 , H01M10/0567 , H01M10/0566 , H01M10/052 , H01M10/0525 , H01M10/0569
CPC分类号： H01M10/056 , H01M10/052 , H01M10/0525 , H01M10/0566 , H01M10/0567 , H01M10/0569 , H01M2300/0025 , Y02T10/7011
摘要： The present invention provides a non-aqueous electrolytic solution including a methylenebissulfonate derivative and improving initial irreversible capacity and other characteristics of a battery such as cycle characteristics, electric capacity, and storage characteristics; a method for producing thereof; and a battery using the electrolytic solution. The non-aqueous electrolytic solution includes: (1) a non-aqueous solvent comprising a cyclic carbonate ester, a straight chained carbonate ester, and/or a cyclic carboxylic acid ester, (2) a lithium salt which may be dissolved in the non-aqueous solvent, as an electrolyte salt, and (3) a methylenebissulfonate derivative of formula [I]: The method includes steps of dissolving a lithium salt in a non-aqueous solvent, and then dissolving the methylenebissulfonate derivative. The non-aqueous electrolytic solution battery includes (i) the non-aqueous electrolytic solution above, (ii) a negative electrode, (iii) a positive electrode, and (iv) a separator.
摘要翻译： 本发明提供一种包含亚甲基双磺酸酯衍生物的非水电解液，提高循环特性，电容量，储存特性等电池的初始不可逆容量等特性。 其制造方法; 和使用电解液的电池。 非水电解液包括：（1）包含环状碳酸酯，直链状碳酸酯和/或环状羧酸酯的非水溶剂，（2）可溶于非水溶液的锂盐， - 水溶剂作为电解质盐，和（3）式[I]的亚甲基双磺酸酯衍生物：该方法包括将锂盐溶解在非水溶剂中，然后溶解亚甲基双磺酸酯衍生物的步骤。 非水电解液电池包括（i）上述非水电解液，（ii）负极，（iii）正极和（iv）隔膜。
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公开(公告)号：US08742136B2
公开(公告)日：2014-06-03
申请号：US12304409
申请日：2007-06-14
IPC分类号： C07D327/00
CPC分类号： C07D327/00 , C07D327/06
摘要： It is an object of the present invention to provide a commercially advantageous method for producing a cyclic disulfonic acid ester with high yield, the present invention discloses a method for producing a cyclic disulfonic acid ester represented by the general formula (3), which comprises reacting a silver alkanedisulfonate represented by the general formula (1) with a dihaloalkane represented by the general formula (2) in a nonpolar solvent. Wherein X1 and X2 are each independently a chlorine atom, a bromine atom or an iodine atom; and Y and Z are each independently a substituted or unsubstituted alkylene chain which may have a heteroatom in the chain.
摘要翻译： 本发明的目的是提供一种以高收率生产环状二磺酸酯的商业上有利的方法，本发明公开了一种由通式（3）表示的环状二磺酸酯的制备方法，该方法包括使通式 由通式（1）表示的烷撑二磺酸烷基酯与通式（2）表示的二卤代烷烃在非极性溶剂中反应。 其中X1和X2各自独立地为氯原子，溴原子或碘原子; 并且Y和Z各自独立地是在链中可以具有杂原子的取代或未取代的亚烷基链。
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公开(公告)号：US08673963B2
公开(公告)日：2014-03-18
申请号：US13388405
申请日：2010-08-03
IPC分类号： A61K31/381 , C07D327/10
CPC分类号： C07D327/04 , C07D327/10
摘要： The present invention is directed to provide an efficient production method which is capable of not only obtaining a cyclic sulfonic acid ester (sultone) at low cost and in high yield, but also the sulfonic acid ester (sultone) stably even in a commercial scale. The present invention relates to a method for producing hydroxysultone comprising a first step where a diol having a specified structure and a thionyl halide are reacted to obtain a cyclic sulfite having a specified structure, and a second step where the cyclic sulfite is reacted with water or/and alcohol; a method for producing an unsaturated sultone having a specified structure comprising a third step where a hydroxylsultone having a specified structure is reacted with an acid halide or an acid anhydride to obtain an intermediate, subsequently the intermediate is treated with a base; as well as a cyclic sulfite having a specified structure.
摘要翻译： 本发明的目的在于提供一种能够以低成本，高收率地获得环状磺酸酯（磺内酯），而且能够以工业规模稳定地获得磺酸酯（磺内酯）的有效的制造方法。 本发明涉及一种生产羟基培养基的方法，包括第一步骤，其中具有特定结构的二醇和亚硫酰卤反应得到具有特定结构的环状亚硫酸盐，第二步是将环状亚硫酸盐与水或 /和酒精; 一种具有特定结构的不饱和磺内酯的制造方法，其特征在于，具有将具有规定结构的羟基磺内酯与酰卤或酸酐反应得到中间体的第3工序，接着用碱处理中间体; 以及具有特定结构的环状亚硫酸盐。
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公开(公告)号：US20120157680A1
公开(公告)日：2012-06-21
申请号：US13393144
申请日：2010-08-30
IPC分类号： C07C309/04 , C07D213/20 , C07D295/037 , C07D403/06 , C07D295/088 , C07D233/58 , C07D401/06
CPC分类号： C07C309/20 , C07D213/06 , C07D213/20 , C07D213/68 , C07D233/58 , C07D295/04 , C07D295/08
摘要： PROBLEM:Providing a novel ionic liquid, which is low-cost, environment-friendly, and has low viscosity and melting point.MEANS FOR SOLVING THE PROBLEM:The present invention is the invention of the ionic liquid represented by the general formula [1]: {wherein, R1 to R3 and n pieces of R4 each independently represent hydrogen atom or alkyl group having 1 to 4 carbon atoms, R5 to R7 each independently represent alkyl group, aralkyl group, or aryl group, R8 represents alkyl group, aralkyl group, aryl group, or the one represented by the general formula [2]: (wherein T represents alkylene chain having 1 to 8 carbon atoms, n represents 1 or 2, and R1 to R7 are the same as the above-described), X represents nitrogen atom or phosphorus atom, n represents 1 or 2. When n is 1, R3 and R4 are bound and may form cyclohexene ring together with the adjacent carbon atoms. In addition, when X is nitrogen atom, R5 to R7 or R5 to R6 may form hetero ring with nitrogen atom binding thereto}.
摘要翻译： 问题：提供低成本，环保的低粘度和熔点的新型离子液体。 解决问题的手段：本发明是由通式[1]表示的离子液体的发明：{其中，R 1〜R 3和n个R 4各自独立地表示氢原子或碳原子数1〜4的烷基 R 5至R 7各自独立地表示烷基，芳烷基或芳基，R 8表示烷基，芳烷基，芳基或由通式[2]表示的基团：（其中T表示亚烷基链，具有1〜8个 碳原子，n表示1或2，并且R 1至R 7与上述相同），X表示氮原子或磷原子，n表示1或2.当n为1时，R 3和R 4结合并形成 环己烯环与相邻的碳原子一起环。 此外，当X是氮原子时，R 5至R 7或R 5至R 6可以与与其结合的氮原子形成杂环}。
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8.发明申请公开(公告)号：US20120130107A1
公开(公告)日：2012-05-24
申请号：US13387887
申请日：2010-08-05
IPC分类号： C07C309/73 , C07C303/32
CPC分类号： C07D213/127 , C07C309/73 , C07D213/06 , C07D233/64 , H01M10/052 , H01M10/0567
摘要： Object To provide a method for producing a bis-quaternary ammonium salt efficiently and a novel synthetic intermediate thereof.Solution The present invention relates to a method for producing a bis-quaternary ammonium salt represented by a general formula [3] which comprises reacting a disulfonic acid ester represented by a general formula [1] (in the formula, definitions of two R1's and T are as described in claim 1) with a tertiary amine represented by a general formula [2] (in the formula, definitions of R3 to R5 are as described in claim 1), and a disulfonic acid ester represented by a general formula [1′] (in the formula, two R16's represent independently a halogen atom or a C1-C3 fluoroalkyl group, and two m's represent independently an integer of 1 to 5).
摘要翻译： 本发明提供一种双季铵盐生产方法及其新型合成中间体。 溶液本发明涉及由通式[3]表示的双季铵盐的制备方法，其包括使由通式[1]表示的二磺酸酯（式中，R 2和R 2的定义相同） 如通式[2]所示的叔胺（在该式中，R3至R5的定义如权利要求1所述）和由通式[1'表示的二磺酸酯如通式 （式中，两个R 16独立地表示卤素原子或C1-C3氟代烷基，2m独立地表示1〜5的整数）。
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公开(公告)号：US20080058200A1
公开(公告)日：2008-03-06
申请号：US10590206
申请日：2005-03-07
申请人： Shu Kobayashi , Kuniaki Okamoto , Ryo Akiyama , Keiji Ohno , Yoshio Inagaki
发明人： Shu Kobayashi , Kuniaki Okamoto , Ryo Akiyama , Keiji Ohno , Yoshio Inagaki
IPC分类号： B01J31/06
CPC分类号： C07C67/31 , B01J31/069 , B01J31/165 , B01J2231/4261 , B01J2231/643 , B01J2531/824 , B01J2531/827 , B01J2531/828 , C07C17/14 , C07C45/68 , C07C49/796 , C07C67/343 , C08F212/08 , C08F212/14 , C07C22/04 , C07C69/732 , C07C69/618
摘要： The objective is to present compositions obtained by supporting by polymers micro clusters of transition metals and the like that are useful as catalysts in various reactions and, once used, are readily recovered and reused.A polymer-supported metal cluster composition is obtained by supporting a transition metal by a cross-linked polymer, and the polymer-supported cluster composition is characterized by the cross-linked polymer obtained by cross-linking of a cross-linkable polymer containing a hydrophilic side chain and a hydrophobic side chain group having a cross-linkable functional group. This polymer-supported metal cluster composition is, for example, preferably formed by first forming a micelle composed of the metal clusters supported by the cross-linkable polymer in a suitable solution and subsequently subjecting the cross-linkable polymer to a cross-linking reaction. The composition is useful as a catalyst and the like in hydrogenation reactions, dehydrogenation reactions, allylic substitution reactions, oxidation reactions, coupling reactions and carbonylation reactions.
摘要翻译： 目的是提供通过聚合物支撑的组合物，所述过渡金属等的微簇等可用作各种反应中的催化剂，并且一旦使用，就容易回收和重复使用。 聚合物负载的金属簇组合物通过用交联聚合物负载过渡金属而获得，聚合物负载的簇组合物的特征在于通过交联含有亲水性的交联聚合物而获得的交联聚合物 侧链和具有可交联官能团的疏水侧链基团。 该聚合物负载的金属簇组合物例如优选通过首先在合适的溶液中形成由可交联聚合物负载的金属簇构成的胶束，然后使可交联聚合物进行交联反应而形成。 该组合物可用作氢化反应，脱氢反应，烯丙基取代反应，氧化反应，偶联反应和羰基化反应中的催化剂等。
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公开(公告)号：US09263767B2
公开(公告)日：2016-02-16
申请号：US14235370
申请日：2012-07-26
IPC分类号： H01M6/16 , H01M10/0567 , H01M10/0568 , H01M10/0569 , H01M10/054
CPC分类号： H01M10/0567 , H01M10/054 , H01M10/0568 , H01M10/0569 , H01M2300/0025
摘要： It is an object of the present invention to provide an electrochemical device having an electrolytic solution having high current density and high oxidation resistance, as well as high safety, where dissolution and deposition of magnesium progress repeatedly and stably.The present invention relates to the electrolytic solution for an electrochemical device comprising (1) the supporting electrolyte composed of a magnesium salt and (2) at least one or more kinds of the compound represented by the following general formula [2], as well as the electrochemical device comprising said electrolytic solution, a positive electrode, a negative electrode and a separator.
摘要翻译： 本发明的目的是提供一种具有高电流密度和高抗氧化性的电解液以及高安全性的电化学装置，其中镁的溶解和沉积反复稳定地进行。 本发明涉及一种电化学装置用电解液，其特征在于，包括：（1）由镁盐构成的支持电解质和（2）至少一种以上由下述通式[2]表示的化合物，以及 包括所述电解液的电化学装置，正极，负极和隔板。
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