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公开(公告)号：US20120083551A1
公开(公告)日：2012-04-05
申请号：US13020642
申请日：2011-02-03
申请人： Mark D. Soucek , Cynthia G. Templeman , Elif Alyamac , Hua Gu , Masahiko Ishii
发明人： Mark D. Soucek , Cynthia G. Templeman , Elif Alyamac , Hua Gu , Masahiko Ishii
IPC分类号： C09D163/00 , C08G63/91 , C08G59/14
CPC分类号： C08G59/1472 , C08G59/1488 , C08G59/5086 , C09D163/00
摘要： Telechelic resins with reactive end groups (e.g., epoxy phosphate and epoxy ester) were synthesized using bisphenol-A (BPA) epoxide. The bisphenol-A based epoxide and the telechelic resins were all modified with tetraethylorthosilicate (TEOS) oligomers to produce epoxide/polysilicate (organic/inorganic) hybrid systems. The modified epoxides were thermally cured with a melamine-formaldehyde resin, cast on steel substrates and salt spray analysis revealed that the inorganically modified epoxides provided improvement over unmodified epoxide resins with respect to both corrosion resistance and adhesion to steel substrates.
摘要翻译： 使用双酚A（BPA）环氧化物合成具有反应性端基（例如环氧磷酸酯和环氧酯）的亲风树脂。 双酚A基环氧化物和遥爪树脂都用原硅酸四乙酯（TEOS）低聚物进行了改性，以生产环氧/聚硅酸盐（有机/无机）混合体系。 改性的环氧化物用三聚氰胺 - 甲醛树脂热固化，铸造在钢基材上，盐雾分析表明，无机改性的环氧化物相对于耐腐蚀性和对钢基材的粘附性都提供了未改性环氧树脂的改进。
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公开(公告)号：US20120083568A1
公开(公告)日：2012-04-05
申请号：US13020600
申请日：2011-02-03
IPC分类号： C09D167/06
CPC分类号： C09D163/00 , Y10T428/31511 , Y10T428/3154 , Y10T428/31663 , Y10T428/31935
摘要： A series of low, medium, and high molecular weight copolymers containing methyl methacrylate, n-butyl acrylate. 2-hydroxyethyl methacrylate, and 2,2,2-trifluoroethyl methacrylate were synthesized by solution polymerization under monomer-starved conditions. The copolymers were crosslinked with a methylated melamine formaldehyde resin in order to obtain thermosetting acrylics. Lower wettability, higher oxygen permeability, and lower refractive index were observed for higher concentrations of fluorinated monomer in the copolymer composition and high number-average hydroxyl functionality of the high molecular weight copolymers increased the crosslink density of the acrylic films, thereby resulting in improved tensile strength and tensile modulus.
摘要翻译： 一系列含有甲基丙烯酸甲酯，丙烯酸正丁酯的低，中，高分子量共聚物。 甲基丙烯酸2-羟乙酯和甲基丙烯酸2,2,2-三氟乙酯在单体饥饿条件下通过溶液聚合合成。 共聚物与甲基化三聚氰胺甲醛树脂交联以获得热固性丙烯酸树脂。 对于较高浓度的氟化单体在共聚物组合物中观察到较低的润湿性，较高的透氧性和较低的折射率，并且高分子量共聚物的高数均羟基官能团增加了丙烯酸薄膜的交联密度，由此导致改进的拉伸强度 强度和拉伸模量。
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公开(公告)号：US08492001B2
公开(公告)日：2013-07-23
申请号：US13020595
申请日：2011-02-03
CPC分类号： C09D163/00 , Y10T428/31511 , Y10T428/3154 , Y10T428/31663 , Y10T428/31935
摘要： A self-stratifying coating composition is provided. The self-stratifying coating can include a base layer having a telechelic resin with reactive end groups and an alkoxide oligomer. In addition, a top layer having an acrylate and/or methacrylate such as a fluorinated acrylate, a fluorinated methacrylate, a fluorinated hydrocarbon copolymerized with an acrylate, a fluorinated hydrocarbon copolymerized with a methacrylate and combinations thereof, and a crosslinking agent can be included. In addition, the base layer and the top layer can have an interfacial surface tension therebetween that is within a range of about 15 to 60 mJ/cm2.
摘要翻译： 提供了一种自分层涂料组合物。 自分层涂层可以包括具有反应端基的遥爪树脂和烷氧基低聚物的基层。 此外，可以包括具有丙烯酸酯和/或甲基丙烯酸酯如氟化丙烯酸酯，氟化甲基丙烯酸酯，与丙烯酸酯共聚的氟化烃，与甲基丙烯酸酯共聚的氟化烃及其组合的顶层和交联剂。 此外，基层和顶层之间的界面表面张力可以在约15至60mJ / cm 2的范围内。
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公开(公告)号：US20120082854A1
公开(公告)日：2012-04-05
申请号：US13020595
申请日：2011-02-03
IPC分类号： B32B27/08
CPC分类号： C09D163/00 , Y10T428/31511 , Y10T428/3154 , Y10T428/31663 , Y10T428/31935
摘要： A self-stratifying coating composition is provided. The self-stratifying coating can include a base layer having a telechelic resin with reactive end groups and an alkoxide oligomer. In addition, a top layer having an acrylate and/or methacrylate such as a fluorinated acrylate, a fluorinated methacrylate, a fluorinated hydrocarbon copolymerized with an acrylate, a fluorinated hydrocarbon copolymerized with a methacrylate and combinations thereof, and a crosslinking agent can be included. In addition, the base layer and the top layer can have an interfacial surface tension therebetween that is within a range of about 15 to 60 mJ/cm2.
摘要翻译： 提供了一种自分层涂料组合物。 自分层涂层可以包括具有反应端基的遥爪树脂和烷氧基低聚物的基层。 此外，可以包括具有丙烯酸酯和/或甲基丙烯酸酯如氟化丙烯酸酯，氟化甲基丙烯酸酯，与丙烯酸酯共聚的氟化烃，与甲基丙烯酸酯共聚的氟化烃及其组合的顶层和交联剂。 此外，基层和顶层之间的界面表面张力可以在约15至60mJ / cm 2的范围内。
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公开(公告)号：US10067265B2
公开(公告)日：2018-09-04
申请号：US12902763
申请日：2010-10-12
CPC分类号： G02B1/005 , G02B1/10 , G02B5/0825 , G02B5/0833
摘要： In one embodiment, a semi-transparent reflector may include a multilayered photonic structure. The multilayered photonic structure includes a plurality of coating layers of high index dielectric material and a plurality of coating layers of low index dielectric material. The plurality of coating layers of high index dielectric material and the plurality of coating layers of low index dielectric material of the multilayered photonic structure are arranged in an [LH . . . (LH)N . . . L] structure. L is one of the plurality of coating layers of low index dielectric material. H is one of the plurality of coating layers of high index dielectric material. N is a positive integer. The multilayered photonic structure has substantially constant reflectance values for wavelengths of electromagnetic radiation in a visible spectrum over a range of angles of incidence of the electromagnetic radiation.
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公开(公告)号：US09229140B2
公开(公告)日：2016-01-05
申请号：US13014398
申请日：2011-01-26
申请人： Debasish Banerjee , Minjuan Zhang , Masahiko Ishii
发明人： Debasish Banerjee , Minjuan Zhang , Masahiko Ishii
摘要： The present invention provides an omnidirectional ultraviolet (UV)-infrared (IR) reflector. The omnidirectional UV-IR reflector includes a multilayer stack having at least three layers, the at least three layers having at least one first index of refraction material A1 and at least one second index of refraction layer B1. The at least one first index of refraction material layer and the at least one second index of refraction material layer can be alternately stacked on top of each other to provide the at least three layers. In addition, the at least one first index of refraction material layer and the at least one second index of refraction material layer each have a predefined thickness of dA1 and dB1, respectively, with the thickness dA1 not being generally equal to the dB1 thickness such that the multilayer stack has a non-periodic layered structure.
摘要翻译： 本发明提供了全向紫外（UV） - 红外（IR）反射器。 全向UV-IR反射器包括具有至少三层的多层堆叠，所述至少三层具有至少一个第一折射材料折射率A1和至少一个第二折射率折射率层B1。 所述至少一个第一折射材料折射率层和所述至少一个第二折射材料折射率层可以交替地堆叠在彼此的顶部以提供所述至少三个层。 另外，折射材料层和至少一个第二折射材料层的至少一个第一折射率分别具有dA1和dB1的预定厚度，其厚度dA1通常不等于dB1厚度，使得 多层堆叠具有非周期性分层结构。
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7.发明授权公开(公告)号：US08861087B2
公开(公告)日：2014-10-14
申请号：US12389221
申请日：2009-02-19
CPC分类号： G02B5/0825 , G02B1/115 , G02B5/0833 , G02B5/26 , G02B5/28 , G02B13/14 , G02B13/143 , Y10T428/24942
摘要： A multi-layer photonic structure may include alternating layers of high index material and low index material having a form [H(LH)N] where, H is a layer of high index material, L is a layer of low index material and N is a number of pairs of layers of high index material and layers of low index material. N may be an integer ≧1. The low index dielectric material may have an index of refraction nL from about 1.3 to about 2.5. The high index dielectric material may have an index of refraction nH from about 1.8 to about 3.5, wherein nH>nL and the multi-layer photonic structure comprises a reflectivity band of greater than about 200 nm for light having angles of incidence from about 0 degrees to about 80 degrees relative to the multi-layer photonic structure. The multi-layer photonic structure may be incorporated into a paint or coating system thereby forming an omni-directional reflective paint or coating.
摘要翻译： 多层光子结构可以包括具有[H（LH）N]形式的高折射率材料和低折射率材料的交替层，其中H是高折射率材料层，L是低折射率材料层，N是 多层高指数材料和低折射率材料层。 N可以是≧1的整数。 低折射率介电材料可以具有约1.3至约2.5的折射率nL。 高折射率介电材料可以具有约1.8至约3.5的折射率nH，其中对于具有大约0度的入射角的光，nH> nL和多层光子结构包括大于约200nm的反射带 到大约80度相对于多层光子结构。 多层光子结构可以结合到涂料或涂料体系中，从而形成全向反射涂料或涂料。
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8.发明授权公开(公告)号：US08749881B2
公开(公告)日：2014-06-10
申请号：US12388395
申请日：2009-02-18
申请人： Debasish Banerjee , Masahiko Ishii , Minjuan Zhang
发明人： Debasish Banerjee , Masahiko Ishii , Minjuan Zhang
IPC分类号： F21V9/06
CPC分类号： G02B5/26 , G02B5/0825 , G02B5/0833
摘要： Disclosed is a multilayer structure wherein a first layer of a first material having an outer surface and a refracted index between 2 and 4 extends across an outer surface of a second layer having a refractive index between 1 and 3. The multilayer stack has a reflective band of less than 200 nanometers when viewed from angles between 0° and 80° and can be used to reflect a narrow range of electromagnetic radiation in the ultraviolet, visible and infrared spectrum ranges. In some instances, the reflection band of the multilayer structure is less than 100 nanometers. In addition, the multilayer structure can have a quantity defined as a range to mid-range ratio percentage of less than 2%.
摘要翻译： 公开了一种多层结构，其中具有外表面和2和4之间的折射率的第一材料的第一层延伸穿过折射率在1和3之间的第二层的外表面。多层堆叠具有反射带 从0°到80°之间的角度观察时，小于200纳米，可用于在紫外线，可见光和红外光谱范围内反射窄范围的电磁辐射。 在一些情况下，多层结构的反射带小于100纳米。 此外，多层结构可以具有定义为中等范围比例百分比的范围小于2％的量。
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9.发明申请Coatings Containing Polymer Modified Enzyme For Stable Self-Cleaning Of Organic Stains 有权含有聚合物改性酶的涂料用于有机污渍的稳定自清洁公开(公告)号：US20130065291A1
公开(公告)日：2013-03-14
申请号：US13229277
申请日：2011-09-09
申请人： Hongfei Jia , Ping Wang , Liting Zhang , Andreas Buthe , Xueyan Zhao , Songtao Wu , Masahiko Ishii , Minjuan Zhang
发明人： Hongfei Jia , Ping Wang , Liting Zhang , Andreas Buthe , Xueyan Zhao , Songtao Wu , Masahiko Ishii , Minjuan Zhang
IPC分类号： C09D189/00
CPC分类号： C09D189/00 , A61K47/60 , C08G65/33337 , C08L2203/02 , C08L2205/02 , C09D5/024 , C09D7/40 , C09D175/16 , C12N9/14 , C12N9/20 , C12N9/2408 , C12N9/2411 , C12N9/54 , C12N9/96 , C12N11/06 , C12N11/08
摘要： Bioactive coatings that are stabilized against inactivation by weathering are provided including a base associated with a chemically modified enzyme, and, optionally a first polyoxyethylene present in the base and independent of the enzyme. The coatings are optionally overlayered onto a substrate to form an active coating facilitating the removal of organic stains or organic material from food, insects, or the environment.
摘要翻译： 提供了通过耐风化来防止灭活的生物活性涂层，包括与化学修饰的酶相关的碱，以及任选地存在于碱中并独立于酶的第一聚氧乙烯。 涂层任选地覆盖在基底上以形成有助于从食品，昆虫或环境中去除有机污渍或有机材料的活性涂层。
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公开(公告)号：US20120307369A1
公开(公告)日：2012-12-06
申请号：US13572071
申请日：2012-08-10
申请人： Debasish Banerjee , Minjuan Zhang , Songtao Wu , Masahiko Ishii
发明人： Debasish Banerjee , Minjuan Zhang , Songtao Wu , Masahiko Ishii
CPC分类号： G02B5/285 , G02B5/0833 , G02B5/085 , G02B5/286 , G02B27/0012
摘要： A process for designing and manufacturing an omnidirectional structural color (OSC) multilayer stack. The process can include providing a digital processor operable to execute at least one module and a table of index of refraction values corresponding to different materials that are usable for manufacturing an OSC multilayer stack. An initial design for the OSC multilayer stack can be provided and at least one additional layer is added to the initial design OSC multilayer stack to create a modified OSC multilayer stack. In addition, the thickness of each layer of the modified OSC multilayer stack is calculated using a merit function module until an optimized OSC multilayer stack has been calculated.
摘要翻译： 一种设计和制造全向结构颜色（OSC）多层堆叠的方法。 该过程可以包括提供可操作以执行至少一个模块的数字处理器和对应于可用于制造OSC多层堆叠的不同材料的折射率值的表。 可以提供用于OSC多层堆叠的初始设计，并且至少一个附加层被添加到初始设计OSC多层堆叠中以创建修改的OSC多层堆叠。 此外，使用优点功能模块计算修改的OSC多层叠层的每层的厚度，直到已经计算了优化的OSC多层堆叠。
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