Preparation process of quaternary phosphonium hydroxide
    1.
    发明授权
    Preparation process of quaternary phosphonium hydroxide 失效
    季鏻氢氧化物的制备方法

    公开(公告)号:US4761493A

    公开(公告)日:1988-08-02

    申请号:US24074

    申请日:1987-03-10

    IPC分类号: C07F9/54 C08G77/08 C07F9/02

    CPC分类号: C07F9/54

    摘要: A quaternary phosphonium hydroxide, which is represented by the following general formula (II): ##STR1## wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 mean independently an alkyl group having 1-8 carbon atoms, a phenyl group or a benzyl group, is prepared by dissolving a quaternary phosphonium halide represented by the following general formula (I): ##STR2## wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 has the same meaning as defined above and X denotes a chlorine, bromine or iodine atom, in a solvent selected from water, lower alcohols and aqueous lower alcohols, and then bringing the resultant solution into contact with a strongly basic anion exchange resin (OH-form).

    摘要翻译: 由下列通式(II)表示的季鏻氢氧化物:其中R1,R2,R3和R4独立地表示具有1-8个碳原子的烷基,苯基或苄基 通过溶解由以下通式(I)表示的季鏻卤化物制备:其中R 1,R 2,R 3和R 4具有与上述相同的含义,X表示氯,溴或碘原子 在选自水,低级醇和低级醇的溶剂中,然后将所得溶液与强碱性阴离子交换树脂(OH-型)接触。