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公开(公告)号：US20080249278A1
公开(公告)日：2008-10-09
申请号：US12076415
申请日：2008-03-18
申请人： Mikihiro Kashio , Toshio Sugizaki , Osamu Moriya
发明人： Mikihiro Kashio , Toshio Sugizaki , Osamu Moriya
IPC分类号： C08G77/04
CPC分类号： C08G77/04 , C08G77/08 , C08K3/32 , H01L33/56 , H01L2224/48091 , H01L2924/00014
摘要： A sealing material for optical elements with excellent transparency, crack resistance, and heat resistance which can produce a cured product of the sealing material and a sealed optical element are provided. The sealing material for optical elements comprising a compound with a ladder structure, which contains a repeating unit of the following formula (A) in the molecule as a major component, the compound being obtained by condensing a compound (1) shown by the formula, R1Si(OR3)P(X1)3-p, and a compound (2) shown by the formula, R2Si(OR4)q(X2)3-q, at a molar ratio of 1:9 to 10:0 in the presence of a phosphoric acid catalyst, wherein R1 represents a group having a reactive functional group, R2 represents an alkyl group having 1 to 20 carbon atoms, R3 and R4 individually represents an alkyl group having 1 to 6 carbon atoms, X1 and X2 individually indicate a halogen atom, p and q individually represent an integer from 0 to 3, and l, m, and n individually represent 0 or an arbitrary integer, provided that l and n are not 0 at the same time.
摘要翻译： 提供了可以制造密封材料的固化物和密封光学元件的具有优异的透明性，抗裂性和耐热性的光学元件用密封材料。 用于光学元件的密封材料包括具有梯形结构的化合物，其在分子中含有下式（A）的重复单元作为主要成分，所述化合物是通过将下式表示的化合物（1） R 1（或3）3个（X 1）3-p 和由下式表示的化合物（2）：R 2 Si（OR 4）q（X 2）2 >）3-q，在磷酸催化剂存在下，摩尔比为1:9至10:0，其中R 1表示具有反应性的基团 官能团R 2表示具有1至20个碳原子的烷基，R 3和R 4独立地表示具有1至 6个碳原子，X 1和X 2各自表示卤素原子，p和q分别表示0〜3的整数，l，m和n分别表示 0或任意整数，条件是l和n不是 0同时。
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公开(公告)号：US08080604B2
公开(公告)日：2011-12-20
申请号：US12073058
申请日：2008-02-28
IPC分类号： C09J183/04 , C08G77/12
CPC分类号： C08F230/08 , C08G77/04 , C08G77/14 , C08G77/26 , C08G77/28 , C09J7/38 , C09J183/04 , C09J2483/00
摘要： An adhesive containing a ladder-type polysilsesquioxane which firmly bonds metals and synthetic resins and an adhesive sheet having an adhesive layer formed by using the adhesive on at least one side of a substrate are provided. An adhesive comprises a ladder-type polysilsesquioxane having a recurring unit of the following formula (I) in the molecule, wherein R1 represents a polymerizable functional group, and R2 represents the same group as R1, an alkyl group having 1 to 6 carbon atoms which may have a substituent, an alkoxy group having 1 to 6 carbon atoms which may have a substituent, or a phenyl group which may have a substituent, and the adhesive sheet has an adhesive layer formed by using the adhesive on at least one side of the substrate.
摘要翻译： 提供了一种含有梯形型聚倍半硅氧烷的粘合剂，其牢固地粘合金属和合成树脂，并且提供了具有通过在基材的至少一侧上使用粘合剂形成的粘合剂层的粘合片。 粘合剂包括分子中具有下式（I）的重复单元的梯型聚倍半硅氧烷，其中R1表示可聚合官能团，R2表示与R1相同的基团，具有1至6个碳原子的烷基， 可以具有取代基，可以具有取代基的具有1〜6个碳原子的烷氧基或可具有取代基的苯基，并且所述粘合片具有通过在所述粘合剂的至少一面上使用所述粘合剂形成的粘合剂层 基质。
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公开(公告)号：US20080249271A1
公开(公告)日：2008-10-09
申请号：US12073058
申请日：2008-02-28
CPC分类号： C08F230/08 , C08G77/04 , C08G77/14 , C08G77/26 , C08G77/28 , C09J7/38 , C09J183/04 , C09J2483/00
摘要： An adhesive containing a ladder-type polysilsesquioxane which firmly bonds metals and synthetic resins and an adhesive sheet having an adhesive layer formed by using the adhesive on at least one side of a substrate are provided. An adhesive comprises a ladder-type polysilsesquioxane having a recurring unit of the following formula (I) in the molecule, wherein R1 represents a polymerizable functional group, and R2 represents the same group as R1, an alkyl group having 1 to 6 carbon atoms which may have a substituent, an alkoxy group having 1 to 6 carbon atoms which may have a substituent, or a phenyl group which may have a substituent, and the adhesive sheet has an adhesive layer formed by using the adhesive on at least one side of the substrate.
摘要翻译： 提供了一种含有梯形型聚倍半硅氧烷的粘合剂，其牢固地粘合金属和合成树脂，并且提供了具有通过在基材的至少一侧上使用粘合剂形成的粘合剂层的粘合片。 粘合剂包括在分子中具有下式（I）的重复单元的梯型聚倍半硅氧烷，其中R 1表示可聚合官能团，R 2表示 可以具有取代基的碳原子数1〜6的烷基，可以具有取代基的碳原子数为1〜6的烷氧基，或可以具有取代基的苯基 具有取代基，并且所述粘合片具有通过在所述基材的至少一侧上使用所述粘合剂形成的粘合剂层。
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公开(公告)号：US08470953B2
公开(公告)日：2013-06-25
申请号：US13195591
申请日：2011-08-01
申请人： Mikihiro Kashio , Toshio Sugizaki , Osamu Moriya
发明人： Mikihiro Kashio , Toshio Sugizaki , Osamu Moriya
CPC分类号： C08G77/04 , C08G77/08 , C08K3/32 , H01L33/56 , H01L2224/48091 , H01L2924/00014
摘要： A sealing material for optical elements with excellent transparency, crack resistance, and heat resistance which can produce a cured product of the sealing material and a sealed optical element are provided. The sealing material for optical elements comprising a compound with a ladder structure, which contains a repeating unit of the following formula (A) in the molecule as a major component, the compound being obtained by condensing a compound (1) shown by the formula, R1Si(OR3)P(X1)3-p, and a compound (2) shown by the formula, R2Si(OR4)q(X2)3-q, at a molar ratio of 1:9 to 10:0 in the presence of a phosphoric acid catalyst, wherein R1 represents a group having a reactive functional group, R2 represents an alkyl group having 1 to 20 carbon atoms, R3 and R4 individually represents an alkyl group having 1 to 6 carbon atoms, X1 and X2 individually indicate a halogen atom, p and q individually represent an integer from 0 to 3, and l, m, and n individually represent 0 or an arbitrary integer, provided that l and n are not 0 at the same time.
摘要翻译： 提供了可以制造密封材料的固化物和密封光学元件的具有优异的透明性，抗裂性和耐热性的光学元件用密封材料。 用于光学元件的密封材料包括具有梯形结构的化合物，其在分子中含有下式（A）的重复单元作为主要成分，所述化合物是通过将下式表示的化合物（1） R1Si（OR3）P（X1）3-p和由式R2Si（OR4）q（X2）3-q表示的化合物（2）的摩尔比为1:9至10:0， 的磷酸催化剂，其中R 1表示具有反应性官能团的基团，R 2表示具有1至20个碳原子的烷基，R 3和R 4各自表示具有1至6个碳原子的烷基，X 1和X 2各自表示 卤素原子，p和q分别表示0〜3的整数，l，m，n分别表示0或任意的整数，条件是l和n不同时为0。
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公开(公告)号：US20110288257A1
公开(公告)日：2011-11-24
申请号：US13195591
申请日：2011-08-01
申请人： Mikihiro KASHIO , Toshio Sugizaki , Osamu Moriya
发明人： Mikihiro KASHIO , Toshio Sugizaki , Osamu Moriya
CPC分类号： C08G77/04 , C08G77/08 , C08K3/32 , H01L33/56 , H01L2224/48091 , H01L2924/00014
摘要： A sealing material for optical elements with excellent transparency, crack resistance, and heat resistance which can produce a cured product of the sealing material and a sealed optical element are provided. The sealing material for optical elements comprising a compound with a ladder structure, which contains a repeating unit of the following formula (A) in the molecule as a major component, the compound being obtained by condensing a compound (1) shown by the formula, R1Si(OR3)P(X1)3-p, and a compound (2) shown by the formula, R2Si(OR4)q(X2)3-q, at a molar ratio of 1:9 to 10:0 in the presence of a phosphoric acid catalyst, wherein R1 represents a group having a reactive functional group, R2 represents an alkyl group having 1 to 20 carbon atoms, R3 and R4 individually represents an alkyl group having 1 to 6 carbon atoms, X1 and X2 individually indicate a halogen atom, p and q individually represent an integer from 0 to 3, and l, m, and n individually represent 0 or an arbitrary integer, provided that l and n are not 0 at the same time.
摘要翻译： 提供了可以制造密封材料的固化物和密封光学元件的具有优异的透明性，抗裂性和耐热性的光学元件用密封材料。 用于光学元件的密封材料包括具有梯形结构的化合物，其在分子中含有下式（A）的重复单元作为主要成分，所述化合物是通过将下式表示的化合物（1） R1Si（OR3）P（X1）3-p和由式R2Si（OR4）q（X2）3-q表示的化合物（2）的摩尔比为1:9至10:0， 的磷酸催化剂，其中R 1表示具有反应性官能团的基团，R 2表示具有1至20个碳原子的烷基，R 3和R 4各自表示具有1至6个碳原子的烷基，X 1和X 2各自表示 卤素原子，p和q分别表示0〜3的整数，l，m，n分别表示0或任意的整数，条件是l和n不同时为0。
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公开(公告)号：US08026332B2
公开(公告)日：2011-09-27
申请号：US12076415
申请日：2008-03-18
申请人： Mikihiro Kashio , Toshio Sugizaki , Osamu Moriya
发明人： Mikihiro Kashio , Toshio Sugizaki , Osamu Moriya
IPC分类号： C08G77/00
CPC分类号： C08G77/04 , C08G77/08 , C08K3/32 , H01L33/56 , H01L2224/48091 , H01L2924/00014
摘要： A sealing material for optical elements with excellent transparency, crack resistance, and heat resistance which can produce a cured product of the sealing material and a sealed optical element are provided. The sealing material for optical elements comprising a compound with a ladder structure, which contains a repeating unit of the following formula (A) in the molecule as a major component, the compound being obtained by condensing a compound (1) shown by the formula, R1Si(OR3)P(X1)3-p, and a compound (2) shown by the formula, R2Si(OR4)q(X2)3-q, at a molar ratio of 1:9 to 10:0 in the presence of a phosphoric acid catalyst, wherein R1 represents a group having a reactive functional group, R2 represents an alkyl group having 1 to 20 carbon atoms, R3 and R4 individually represents an alkyl group having 1 to 6 carbon atoms, X1 and X2 individually indicate a halogen atom, p and q individually represent an integer from 0 to 3, and l, m, and n individually represent 0 or an arbitrary integer, provided that l and n are not 0 at the same time.
摘要翻译： 提供了可以制造密封材料的固化物和密封光学元件的具有优异的透明性，抗裂性和耐热性的光学元件用密封材料。 用于光学元件的密封材料包括具有梯形结构的化合物，其在分子中含有下式（A）的重复单元作为主要成分，所述化合物是通过将下式表示的化合物（1） R1Si（OR3）P（X1）3-p和由式R2Si（OR4）q（X2）3-q表示的化合物（2）的摩尔比为1:9至10:0， 的磷酸催化剂，其中R 1表示具有反应性官能团的基团，R 2表示具有1至20个碳原子的烷基，R 3和R 4各自表示具有1至6个碳原子的烷基，X 1和X 2各自表示 卤素原子，p和q分别表示0〜3的整数，l，m，n分别表示0或任意的整数，条件是l和n不同时为0。
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7.发明授权Process for producing polysilsesquioxane graft polymer, pressure-sensitive adhesive, and pressure-sensitive adhesive sheet 有权制造聚倍半硅氧烷接枝聚合物，压敏粘合剂和压敏粘合片的方法公开(公告)号：US07759406B2
公开(公告)日：2010-07-20
申请号：US10584895
申请日：2004-09-22
CPC分类号： C08G77/392 , C08F283/12 , C09J7/38 , C09J151/08 , C09J183/08 , C09J183/10 , C09J2451/00 , Y10T428/2852 , Y10T428/31663
摘要： The present invention provides a process for producing a polysilsesquioxane graft polymer (1) which includes applying ionizing radiation or heat to a mixture including a polysilsesquioxane compound (2) and a vinyl compound (3), a polysilsesquioxane compound including an iniferter group, and a pressure-sensitive adhesive and a pressure-sensitive adhesive sheet using the polymer. According to the present invention, a process for producing a polysilsesquioxane graft polymer which may be used as a pressure-sensitive adhesive exhibiting excellent heat resistance and cohesive force, and the like are provided. In the formula, A represents a linking group, R1 represents a hydrocarbon group which may have a substituent, R2 represents a hydrogen atom or the like, R3 represents a polar group or the like, R4 represents a hydrogen atom or the like, k1 to k3 represent arbitrary positive integers, 1 to n represent zero or an arbitrary positive integer (excluding the case where “m=n=0”), and Q represents an iniferter group.
摘要翻译： 本发明提供一种聚倍半硅氧烷接枝聚合物（1）的制造方法，其包括对包含聚倍半硅氧烷化合物（2）和乙烯基化合物（3）的混合物进行电离辐射或加热，包括引发剂组的聚倍半硅氧烷化合物和 压敏粘合剂和使用该聚合物的压敏粘合片。 根据本发明，提供了可以用作表现出优异的耐热性和内聚力的压敏粘合剂的聚倍半硅氧烷接枝聚合物的制造方法等。 式中，A表示连接基，R 1表示可以具有取代基的烃基，R 2表示氢原子等，R 3表示极性基等，R 4表示氢原子等，k 1〜 k3表示任意正整数，1〜n表示0或任意的正整数（不包括“m = n = 0”的情况），Q表示发射器组。
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8.发明申请Process for Producing Polysilsesquioxane Graft Polymer, Pressure-Sensitive Adhesive, and Pressure-Sensitive Adhesive Sheet 有权生产聚倍半硅氧烷接枝聚合物，压敏粘合剂和压敏粘合片的方法公开(公告)号：US20080051487A1
公开(公告)日：2008-02-28
申请号：US10584895
申请日：2004-09-22
IPC分类号： C08F283/12 , C08F2/46
CPC分类号： C08G77/392 , C08F283/12 , C09J7/38 , C09J151/08 , C09J183/08 , C09J183/10 , C09J2451/00 , Y10T428/2852 , Y10T428/31663
摘要： The present invention provides a process for producing a polysilsesquioxane graft polymer (1) which includes applying ionizing radiation or heat to a mixture including a polysilsesquioxane compound (2) and a vinyl compound (3), a polysilsesquioxane compound including an iniferter group, and a pressure-sensitive adhesive and a pressure-sensitive adhesive sheet using the polymer. According to the present invention, a process for producing a polysilsesquioxane graft polymer which may be used as a pressure-sensitive adhesive exhibiting excellent heat resistance and cohesive force, and the like are provided. In the formula, A represents a linking group, R1 represents a hydrocarbon group which may have a substituent, R2 represents a hydrogen atom or the like, R3 represents a polar group or the like, R4 represents a hydrogen atom or the like, k1 to k3 represent arbitrary positive integers, 1 to n represent zero or an arbitrary positive integer (excluding the case where “m=n=0”), and Q represents an iniferter group.
摘要翻译： 本发明提供一种聚倍半硅氧烷接枝聚合物（1）的制造方法，其包括对包含聚倍半硅氧烷化合物（2）和乙烯基化合物（3）的混合物进行电离辐射或加热，包括引发剂组的聚倍半硅氧烷化合物和 压敏粘合剂和使用该聚合物的压敏粘合片。 根据本发明，提供了可以用作表现出优异的耐热性和内聚力的压敏粘合剂的聚倍半硅氧烷接枝聚合物的制造方法等。 在该式中，A表示连接基，R 1表示可以具有取代基的烃基，R 2表示氢原子等， 3 表示极性基团等，R 4表示氢原子等，k 1〜3 3表示 任意正整数，1至n表示零或任意正整数（不包括“m = n = 0”的情况），Q表示发射器组。
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公开(公告)号：US06284364B1
公开(公告)日：2001-09-04
申请号：US09093716
申请日：1998-06-09
IPC分类号： B32B900
CPC分类号： C08J7/04 , C08J7/045 , C08J2383/02 , Y10T428/259 , Y10T428/28 , Y10T428/2891
摘要： There are disclosed a silicate-containing sheet which comprises a silicate of one metal or at least two composite metals, which metal and metals are selected from the group consisting of the groups 4 to 13 series 4-metals of the periodic table, the groups 4 to 15 series 5-metals of the periodic table, and the lanthanoids series metals, and are preferably selected from the group consisting of Ti, Fe, Co, Ni, Cu, Zn, Ga, Zr, Ag, In, Sn, Sb and Ce ; and further a label comprising the above silicate-containing sheet. The silicate-containing sheet mentioned above can afford a functional sheet which has catalytic actions such as ultraviolet rays-attenuating properties, antimicrobial properties and antifouling properties at a low manufacturing cost.
摘要翻译： 公开了一种含硅酸盐的片材，其包含一种金属或至少两种复合金属的硅酸盐，该金属和金属选自周期表第4至13族4族金属，第4族 优选选自Ti，Fe，Co，Ni，Cu，Zn，Ga，Zr，Ag，In，Sn，Sb和...中的15种5族元素周期表的5族金属和镧系金属， Ce 以及另外包含上述含硅酸盐的片材的标签。 上述含硅酸盐的片材能够以低制造成本提供具有紫外线衰减特性，抗菌性和防污性等催化作用的功能性片材。
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公开(公告)号：US06544641B2
公开(公告)日：2003-04-08
申请号：US09891660
申请日：2001-06-27
IPC分类号： B32B712
CPC分类号： C08J7/04 , C08J2383/02 , Y10T428/259 , Y10T428/28 , Y10T428/2857 , Y10T428/2891 , Y10T428/31667
摘要： There are disclosed a silicate-containing sheet which comprises a silicate of one metal or at least two composite metals, which metal and metals are selected from the group consisting of the groups 4 to 13 series 4-metals of the periodic table, the groups 4 to 15 series 5-metals of the periodic table, and the lanthanoids series metals, and are preferably selected from the group consisting of Ti, Fe, Co, Ni, Cu, Zn, Ga, Zr, Ag, In, Sn, Sb and Ce; and further a label comprising the above silicate-containing sheet. The silicate-containing sheet mentioned above can afford a functional sheet which has catalytic actions such as ultraviolet rays-attenuating properties, antimicrobial properties and antifouling properties at a low manufacturing cost.
摘要翻译： 公开了一种含硅酸盐的片材，其包含一种金属或至少两种复合金属的硅酸盐，该金属和金属选自周期表第4至13族4族金属，第4族 优选选自Ti，Fe，Co，Ni，Cu，Zn，Ga，Zr，Ag，In，Sn，Sb和...中的15种5族元素周期表的5族金属和镧系金属， Ce 以及另外包含上述含硅酸盐的片材的标签。 上述含硅酸盐的片材能够以低制造成本提供具有紫外线衰减特性，抗菌性和防污性等催化作用的功能性片材。
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