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公开(公告)号：US4543242A
公开(公告)日：1985-09-24
申请号：US651944
申请日：1984-09-19
IPC分类号： C01B21/083
CPC分类号： C01B21/0835
摘要： NF.sub.3 is prepared with good yields by reaction between fluorine gas and an ammonium complex of a metal fluoride, such as (NH.sub.4).sub.3 AlF.sub.6, in solid phase. The metal flouride ammonium complex may be one additionally containing an alkali metal, such as (NH.sub.4).sub.2 NaAlF.sub.6. The gas-solid reaction is carried out preferably at temperatures above 80.degree. C. and at relatively low partial pressures of fluorine in the gas phase of the reaction system, so that the reaction is easy to control.
摘要翻译： 通过氟气与诸如（NH 4）3 AlF 6等金属氟化物的铵络合物的固相反应制备NF 3。 金属氟化铵络合物可以另外含有碱金属如（NH 4）2 NaAlF 6。 气固反应优选在高于80℃的温度和在反应体系的气相中相对较低的氟分压下进行，使得反应易于控制。
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公开(公告)号：US5017499A
公开(公告)日：1991-05-21
申请号：US330898
申请日：1989-03-31
申请人： Kohzo Hakuta , Minoru Aramaki , Takashi Suenaga , Mitsuo Kodama , Hisaji Nakano , Shinsuke Nakagawa
发明人： Kohzo Hakuta , Minoru Aramaki , Takashi Suenaga , Mitsuo Kodama , Hisaji Nakano , Shinsuke Nakagawa
CPC分类号： H01S3/104 , G01N31/005 , G01N33/0052 , H01S3/225 , Y10T436/12 , Y10T436/19 , Y10T436/204998 , Y10T436/207497
摘要： The concentration of molecular fluorine in a mixed gas such as an excimer laser gas can be determined easily, quickly and accurately by passing the mixed gas through a column packed with an alakli metal or alkaline earth metal compound which has no halogen atom and reacts with fluorine to form a solid fluoride together with molecular oxygen and/or carbon dioxide and measuring the concentration of oxygen or carbon dioxide in the fluorine-free gas flowed out of the packed column. If the mixed gas initially contains molecular oxygen or carbon dioxide, its concentration is measured separately after fixing fluorine in another column packed with an element which forms a fluoride. This analyzing method can be used in a feedback control system for controlling the concentration of fluorine in an excimer laser gas during operation of the laser to thereby stabilize the laser output power.
摘要翻译： 混合气体如准分子激光气体中的分子氟的浓度可以通过使混合气体通过填充有不含卤素原子并与氟反应的碱金属或碱土金属化合物的柱而容易，准确地测定 与分子氧和/或二氧化碳一起形成固体氟化物，并测量从填充塔流出的无氟气体中的氧气或二氧化碳的浓度。 如果混合气体最初含有分子氧或二氧化碳，则在将氟固定在填充有形成氟化物的元素的另一柱中后，分别测量其浓度。 该分析方法可以用于反馈控制系统，用于在激光器的操作期间控制准分子激光气体中的氟浓度，从而稳定激光输出功率。
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公开(公告)号：US4740982A
公开(公告)日：1988-04-26
申请号：US909702
申请日：1986-09-22
申请人： Kohzo Hakuta , Minoru Aramaki , Takashi Suenaga
发明人： Kohzo Hakuta , Minoru Aramaki , Takashi Suenaga
摘要： A laser gas used in a rare gas halide excimer laser is efficiently refined with little loss of the essential rare gas such as Kr, Ar or Xe by contact of the laser gas with a solid alkaline compound, e.g. Ca(OH).sub.2, for conversion of acidic impurities and also the halogen source gas such as F.sub.2 or HCl into solid metal halides and contact of the remaining gas with zeolite which is adsorbent of the remaining impurities. When the halogen source gas comprises a highly oxidizing fluorine matter the laser gas is first brought into contact with a reactive metal, e.g. Si or Fe, to convert the oxidizing fluorine matter into metal fluorides to thereby prevent formation of O.sub.2, which is obstructive to the laser operation, by reaction of the oxidizing matter with the alkaline compound. The halogen source gas too can be recovered by initially cooling the laser gas so as to cause condensation of the rare gas and impurities having relatively high boiling points and leave the halogen source gas, which is lower in boiling point, in gas phase.
摘要翻译： 在稀有气体卤化物准分子激光器中使用的激光气体通过激光气体与固体碱性化合物的接触，如Kr，Ar或Xe等几乎不损失基本稀有气体而被有效地精炼。 Ca（OH）2，用于将酸性杂质以及卤素源气体如F2或HCl转化成固体金属卤化物，并将剩余气体与作为其余杂质的吸附剂的沸石接触。 当卤素源气体包含高度氧化的氟物质时，激光气体首先与反应性金属接触，例如， Si或Fe，将氧化性氟物质转化为金属氟化物，由此氧化物质与碱性化合物的反应，可以防止形成对激光作业产生阻碍的O 2。 卤素源气体也可以通过初始冷却激光气体来回收，以使稀有气体和沸点相对较高的杂质冷凝，并且在气相中留下沸点较低的卤素源气体。
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公开(公告)号：US5004829A
公开(公告)日：1991-04-02
申请号：US506206
申请日：1990-04-09
IPC分类号： C07C303/00 , C07C309/06
CPC分类号： C07C303/00 , Y10S203/06 , Y10S203/90
摘要： (CF.sub.3 SO.sub.2).sub.2 O is formed by reaction of CF.sub.3 SO.sub.3 H with P.sub.2 O.sub.5 and taken out of the reaction system by distillation, but the residue of the distillation contains a considerable amount of unreacted CF.sub.3 SO.sub.3 H. From the residue unreacted by adding water or a phosphoric acid solution, preferably the latter, to the residue to obtain a fluidic mixture containing an adequate amount of water and subjecting the mixture to distillation, preferably under reduced pressure at temperatures ranging from 180.degree. to 280.degree. C. It is possible to form additional CF.sub.3 SO.sub.3 H during the recovery process by adding a metal salt of CF.sub.3 SO.sub.3 H to the aformentioned mixture since the metal salt is decomposed by phosphoric acid contained in the mixture.
摘要翻译： （CF 3 SO 2）2 O通过CF 3 SO 3 H与P 2 O 5的反应形成，并通过蒸馏从反应体系中取出，但蒸馏残余物含有大量未反应的CF 3 SO 3 H。 从残留物中加入水或磷酸溶液未反应的残余物加入到残渣中，得到含有足量水的流体混合物，优选在180-280℃的温度下进行减压蒸馏 在回收过程中可以通过向上述混合物中加入CF 3 SO 3 H的金属盐形成另外的CF 3 SO 3 H，因为金属盐被混合物中所含的磷酸分解。
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5.发明授权Method of refining tungsten hexafluoride containing molybdenum hexafluoride as an impurity 失效精制含有十五烷基硫脲的硝基二氢呋喃的方法
公开(公告)号：US5234679A
公开(公告)日：1993-08-10
申请号：US866347
申请日：1992-04-10
IPC分类号： C01G41/04
CPC分类号： C01G41/04
摘要： A method of refining tungsten hexafluoride containing molybdenum hexafluoride as an impurity includes the step of contacting the tungsten hexafluoride with at least one metal selected from the group consisting of Mo, W, Cu, Ni, Fe, Co, Zn, Ti, Al, Ca and Mg at a temperature ranging from 100.degree. to 500.degree. C. Molybdenum hexafluoride is efficiently removed from the tungsten hexafluoride by the method.
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6.发明申请公开(公告)号：US20110176042A1
公开(公告)日：2011-07-21
申请号：US13122317
申请日：2009-09-16
IPC分类号： H04N5/335
CPC分类号： H04N5/3742 , H01L27/14609 , H01L27/14614 , H01L27/14641 , H01L27/14643 , H04N5/347 , H04N5/3698 , H04N5/37455 , H04N5/37457 , H04N5/378
摘要： Provided is a solid-state imaging element including pixel signal read lines, and a pixel signal reading unit for reading pixel signals from a pixel unit via the pixel signal read line. The pixel unit includes a plurality of pixels arranged in a matrix form, each pixel including a photoelectric conversion element. In the pixel unit, a shared pixel in which an output node is shared among a plurality of pixels is formed, and a pixel signal of each pixel in the shared pixel is capable of being selectively output from the shared output node to a corresponding one of the pixel signal read lines. The pixel signal reading unit sets a bias voltage for a load element which is connected to the pixel signal read line and in which current dependent on a bias voltage flows in the load element, to a voltage causing a current value to be higher than current upon a reference bias voltage when there is no difference between added charge amounts, when addition of pixel signals of the respective pixels in the shared pixel is driven.
摘要翻译： 提供了包括像素信号读取线的固态成像元件和用于经由像素信号读取线从像素单元读取像素信号的像素信号读取单元。 像素单元包括以矩阵形式布置的多个像素，每个像素包括光电转换元件。 在像素单元中，形成其中在多个像素之间共享输出节点的共享像素，并且共享像素中的每个像素的像素信号能够被选择性地从共享输出节点输出到 像素信号读取线。 像素信号读取单元设置连接到像素信号读取线的负载元件的偏置电压，并且其中取决于偏置电压的电流在负载元件中流动到使电流值高于当前值的电流 当驱动共享像素中的各个像素的像素信号的相加时，当添加的电荷量之间没有差异时，参考偏置电压。
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7.发明授权
公开(公告)号：US5112149A
公开(公告)日：1992-05-12
申请号：US622230
申请日：1990-12-03
申请人： Takashi Suenaga
发明人： Takashi Suenaga
CPC分类号： B41J3/28 , G06K15/028
摘要： A manual sweeping printer has a linear thermal head and sweeps in a direction perpendicular to an arranging direction of the thermal head, thereby performing printing. The printer alternately drives two adjacent heating elements to perform 2-time-division printing. When a sweeping velocity of the printer exceeds a maximum sweeping velocity set in accordance with a printing speed, a divisional driving sequence is controlled to perform staggered printing.
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公开(公告)号：US07992265B2
公开(公告)日：2011-08-09
申请号：US12216506
申请日：2008-07-07
申请人： Takashi Suenaga
发明人： Takashi Suenaga
IPC分类号： B42F1/00
摘要： A fastening apparatus using magnetism enables to fasten an object with a magnetic material to a target surface. The apparatus has a substrate which is flexible and provided at its reverse side with a sticking coat for removably attaching to the target surface, and a magnet receiving hole surrounded by the sticking coat penetrating through the substrate; a flat magnet housed into the magnet receiving hole; an outer film which is fixed on the substrate for separating the flat magnet and the object. The flat magnet is able to be removed out from the magnet receiving hole.
摘要翻译： 使用磁性的紧固装置能够将具有磁性材料的物体紧固到目标表面。 该装置具有柔性的基板，其背面设置有用于可移除地附着到目标表面的粘贴涂层，以及由穿透基板的粘着涂层包围的磁体接收孔; 容纳在磁体容纳孔中的扁平磁体; 固定在基板上用于分离扁平磁体和物体的外部膜。 扁平磁体能够从磁体接收孔中取出。
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公开(公告)号：US5069887A
公开(公告)日：1991-12-03
申请号：US639541
申请日：1991-01-10
IPC分类号： C01B21/083
CPC分类号： C01B21/0837 , C01B21/0832
摘要： The invention provides a selective adsorption method for refining NF.sub.3 gas containing CF.sub.4 as impurity. At a temperature not higher than 10.degree. C. the NF.sub.3 gas is brought into contact with a crystalline and porous synthetic zeolite, which is substantially uniform in pore size and about 4.9 .ANG. in effective pore size and is commerciallized under the name of molecular sieve 5A, on condition that the content of water of crystallinity in the synthetic zeolite is 1-10 wt. %, and preferably 6-10 wt. %. The synthetic zeolite efficiently adsorbs NF.sub.3 with little adsorption of CF.sub.4.
摘要翻译： 本发明提供了一种选择性吸附方法，用于精炼含有CF4的NF3气体作为杂质。 在不高于10℃的温度下，使NF 3气体与结晶和多孔合成沸石接触，该沸石的孔径基本上是均匀的，有效孔径约为4.9埃，并以分子筛5A的名义商业化 在合成沸石中的结晶水含量为1-10wt。 ％，优选6-10wt。 ％。 合成沸石有效吸附NF3，几乎不吸附CF4。
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10.发明授权公开(公告)号：US08773557B2
公开(公告)日：2014-07-08
申请号：US13122317
申请日：2009-09-16
CPC分类号： H04N5/3742 , H01L27/14609 , H01L27/14614 , H01L27/14641 , H01L27/14643 , H04N5/347 , H04N5/3698 , H04N5/37455 , H04N5/37457 , H04N5/378
摘要： Provided is a solid-state imaging element including pixel signal read lines, and a pixel signal reading unit for reading pixel signals from a pixel unit via the pixel signal read line. The pixel unit includes a plurality of pixels arranged in a matrix form, each pixel including a photoelectric conversion element. In the pixel unit, a shared pixel in which an output node is shared among a plurality of pixels is formed, and a pixel signal of each pixel in the shared pixel is capable of being selectively output from the shared output node to a corresponding one of the pixel signal read lines. The pixel signal reading unit sets a bias voltage for a load element which is connected to the pixel signal read line and in which current dependent on a bias voltage flows in the load element, to a voltage causing a current value to be higher than current upon a reference bias voltage when there is no difference between added charge amounts, when addition of pixel signals of the respective pixels in the shared pixel is driven.
摘要翻译： 提供了包括像素信号读取线的固态成像元件和用于经由像素信号读取线从像素单元读取像素信号的像素信号读取单元。 像素单元包括以矩阵形式布置的多个像素，每个像素包括光电转换元件。 在像素单元中，形成其中在多个像素之间共享输出节点的共享像素，并且共享像素中的每个像素的像素信号能够被选择性地从共享输出节点输出到 像素信号读取线。 像素信号读取单元设置连接到像素信号读取线的负载元件的偏置电压，并且其中取决于偏置电压的电流在负载元件中流动到使电流值高于当前值的电流 当驱动共享像素中的各个像素的像素信号的相加时，当添加的电荷量之间没有差异时，参考偏置电压。
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