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公开(公告)号：US06512142B1
公开(公告)日：2003-01-28
申请号：US09572499
申请日：2000-05-18
IPC分类号： C07C5710
摘要： A granulated product of potassium sorbate (i) has an overall pore volume of 0.3 ml/g or less, (ii) has an Na content of 450 ppm or less, or (iii) has an overall pore volume of 0.4 ml/g or less, or a granule hardness of 15% or less, and an Na content of 1000 ppm or less. The granulated product is obtained, for example, (i) by granulating a potassium sorbate aqueous solution through fluidized bed granulation drying, (ii) by neutralizing sorbic acid with a potassium sorbate having a molar ratio of Na to K (Na/K) of 0.0024 or less to yield potassium sorbate, and granulating the potassium sorbate, or (iii) by neutralizing sorbic acid with a potassium sorbate having a molar ratio of Na to K (Na/K) of 0.006 or less to yield potassium sorbate, and moisture-conditioning 100 parts by weight of the potassium sorbate with 1 to 8.5 parts by weight of water and 1 to 8 parts by weight of a water-soluble organic solvent and subjecting the resulting mixture to extrusion granulation. The granulated product of potassium sorbate has a highly stable hue over time.
摘要翻译： 山梨酸钾（i）的造粒产物的总孔体积为0.3ml / g以下，（ii）Na含量为450ppm以下，或（iii）总孔体积为0.4ml / g，或 或者颗粒硬度为15％以下，Na含量为1000ppm以下。 得到造粒物，例如，（i）通过流化床造粒干燥将山梨酸钾水溶液制粒，（ii）通过用山梨酸钾与Na摩尔比K（Na / K）的山梨酸钾中和山梨酸 0.0024以下，得到山梨酸钾，并使山梨酸钾成粒，或者（iii）通过用摩尔比为Na〜K（Na / K）为0.006以下的山梨酸钾中和山梨酸，得到山梨酸钾， 用1〜8.5重量份的水和1〜8重量份的水溶性有机溶剂调节100重量份的山梨酸钾，并将所得混合物进行挤出造粒。 山梨酸钾的粒状产品随着时间的推移具有高度稳定的色调。
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公开(公告)号：US5337668A
公开(公告)日：1994-08-16
申请号：US151247
申请日：1993-11-12
IPC分类号： G03F1/00 , G03F9/00 , H01L21/027 , H01L21/30 , B41F1/34
CPC分类号： G03F9/00
摘要： Plural types of register mark configurations are displayed in window W1, and a specified page layout pattern is displayed in window W2. A plurality of register mark candidate positions, which can be decided according to the page layout pattern, are also displayed in window W2. The operator selects one of the register mark configurations available and also selects a register mark candidate position to locate the register mark. The selected register mark will be located at the selected candidate position after rotation by the specified rotation angle.
摘要翻译： 多个类型的对位标记配置显示在窗口W1中，窗口W2中显示指定的页面布局图案。 可以在窗口W2中显示可以根据页面布局图案来确定的多个对准标记候选位置。 操作员选择可用的一个寄存器标记配置，并且还选择一个寄存器标记候选位置来定位寄存器标记。 所选择的对准标记将位于旋转后所选择的候选位置指定的旋转角度。
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公开(公告)号：US5731255A
公开(公告)日：1998-03-24
申请号：US504547
申请日：1995-07-20
申请人： Li Rui Pan , Tomohide Ina , Kazuyuki Matsuoka
发明人： Li Rui Pan , Tomohide Ina , Kazuyuki Matsuoka
CPC分类号： B01J31/1616 , B01J31/24 , B01J31/2404 , C07C67/38 , B01J2231/321 , B01J2531/80 , B01J2531/822 , B01J2531/824 , B01J2531/828 , B01J2531/842 , B01J2531/845 , B01J2531/847 , B01J31/1895
摘要： A carbonylation catalytic system comprises (A) a combination of (A1) a Group VIII metal source of Periodic Table of the Elements (e.g., palladium, palladium chloride) supported on a carrier, (A2) a ligand such as triphenylphosphine and (A3) an acid such as an alkyl-sulfonic acid, or (B) a combination of (B1) the Group VIII metal source except for palladium (e.g., a platinum compound), (B2) a ligand such as triphenylphosphine and (B3) an electron donative compound having an electron donability .DELTA..nu.D of not less than 2 (for instance, an amine such as a heterocyclic tertiary amine). The catalytic system (B) may further comprise (B4) an acid such as methanesulfonic acid. In the presence of the catalytic system (A) or (B), an acetylenic or olefinic unsaturated compound is allowed to react with carbon monoxide and a nucleophilic compound having an active hydrogen such as water, an alcohol and a carboxylic acid in a liquid phase to give an unsaturated or saturated carboxylic acid or an ester thereof with high transformation rate and selectivity.
摘要翻译： 羰基化催化体系包括（A）负载在载体上的（A1）元素周期表第Ⅷ族金属源（例如钯，氯化钯），（A2）配体如三苯基膦和（A3） 一种酸如烷基磺酸，或（B）除了钯（例如铂化合物）之外的（B1）第Ⅷ族金属源，（B2）配体如三苯基膦和（B3）电子的组合 具有不小于2的电子偶联性DELTA nu D的助孕化合物（例如，胺如杂环叔胺）。 催化体系（B）还可以包含（B4）酸，例如甲磺酸。 在催化体系（A）或（B）的存在下，允许炔属或烯属不饱和化合物与一氧化碳和具有活性氢的亲核化合物如水，醇和羧酸在液相中反应 得到具有高转化率和选择性的不饱和或饱和羧酸或其酯。
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公开(公告)号：US5386056A
公开(公告)日：1995-01-31
申请号：US178315
申请日：1994-01-12
申请人： Kazuyuki Matsuoka
发明人： Kazuyuki Matsuoka
IPC分类号： C07C319/18 , C07C319/20 , C07C323/52 , C07C319/00
CPC分类号： C07C319/20 , C07C319/18 , Y02P20/582
摘要： Methyl 2-hydroxy-4-methylthiobutanoate and formamide are produced by means of reacting 2-hydroxy-4-methylthiobutanamide obtained by hydration of 2-hydroxy-4-methylthiobutyronitrile with methyl formate. Said methyl 2-hydroxy-4-methylthiobutanoate is hydrolyzed to give 2-hydroxy-4-methylthiobutanoic acid and methanol. No sulfuric acid is employed as a reacting agent, hence exhaustion of a large quantity of ammonium sulfate is prevented. Formamide and methanol thus produced can be recycled as reactants.
摘要翻译： PCT No.PCT / JP93 / 00659 Sec。 371日期：1994年1月12日 102（e）日期1994年1月12日PCT提交1993年5月20日PCT公布。 公开号WO93 / 23372 日期：1993年11月25日。2-羟基-4-甲硫基丁酸甲酯和甲酰胺是通过使2-羟基-4-甲硫基丁腈与甲酸甲酯水合得到的2-羟基-4-甲硫基丁酰胺反应制得的。 将所述2-羟基-4-甲硫基丁酸甲酯水解，得到2-羟基-4-甲硫基丁酸和甲醇。 不使用硫酸作为反应剂，因此可以防止大量的硫酸铵的耗尽。 如此生产的甲酰胺和甲醇可作为反应物再循环。
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公开(公告)号：US06215031B1
公开(公告)日：2001-04-10
申请号：US09155242
申请日：1998-09-24
IPC分类号： C07C3113
CPC分类号： C07C49/757 , C07C29/145 , C07C35/02 , C07C35/08 , C07C45/33 , C07C45/34 , C07C49/523 , C07C2601/14
摘要： The present invention relates to a 3-hydroxymethylcycloalkanol of the following formula (1), and a process for production of a 3-hydroxymethylcycloalkanol of the formula (1) by reduction of 3-formylcycloalkanone or 3-formylcycloalkenone. In accordance with the present invention, 3-hydroxymethylcycloalkanol, which is useful as the starting material for the production of polymers, can be produced with high conversion and high selectivity.
摘要翻译： 本发明涉及下式（1）的3-羟甲基环烷醇和通过还原3-甲酰基环烷酮或3-甲酰基环烯酮制备式（1）的3-羟甲基环烷醇的方法。根据本发明 可以以高转化率和高选择性制备可用作聚合物生产原料的3-羟甲基环烷醇。
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6.发明授权
公开(公告)号：US5879841A
公开(公告)日：1999-03-09
申请号：US707647
申请日：1996-09-05
CPC分类号： H04N1/3873
摘要： A unit image area is specified, and unit image data representing a unit image in the unit image area is prepared. A plurality of the unit image areas are laid out on an image plane in a multi-composing manner, whereby layout information representing the multi-composing layout of the unit image areas is created. Mask data representing a plurality of multi-composed unit image areas are then prepared, based on the unit image area data and the layout information. Generated subsequently is an image recording signal representing unit images to be respectively drawn in the plurality of unit image areas, which are expressed by the mask data, on the image plane. Multi-duplicated images are eventually recorded on a photosensitive material according to the image recording signal without using a photocomposer.
摘要翻译： 指定单位图像区域，并且准备表示单位图像区域中的单位图像的单位图像数据。 多个单位图像区域以多组合方式布置在图像平面上，由此创建表示单位图像区域的多组合布局的布局信息。 然后，基于单位图像区域数据和布局信息准备表示多个多组合单位图像区域的掩模数据。 随后产生表示在图像平面上分别绘制在由掩模数据表示的多个单位图像区域中的单位图像的图像记录信号。 根据图像记录信号，多重复图像最终被记录在感光材料上，而不使用光电投影仪。
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公开(公告)号：US5763652A
公开(公告)日：1998-06-09
申请号：US611877
申请日：1996-03-06
IPC分类号： C07C51/02 , C07C51/06 , C07C51/08 , C07C231/06 , C07C51/62 , C07C51/367
CPC分类号： C07C51/02 , C07C231/065 , C07C51/06 , C07C51/08 , Y02P20/584
摘要： A nitrile compound or an amide compound is hydrolyzed in the presence of an inorganic acid or other acidic catalyst or an alkali metal hydroxide or other basic catalyst, and the by-produced ammonium salt of the acidic catalyst or the produced salt of a carboxylic acid and a base is electrodialysed to form an acid and ammonia or aqueous ammonia, or to form a base and ammonia. The obtained acid or base may be recycled as a catalyst for the hydrolysis of the nitrile compound or amide compound, and the obtained ammonia is reutilized as a nitrogen source for the nitrile compound or amide compound. Such amide compound may be produced by hydration of a nitrite compound in the presence of a manganese oxide.
摘要翻译： 腈化合物或酰胺化合物在无机酸或其它酸性催化剂或碱金属氢氧化物或其它碱性催化剂以及酸式催化剂的副产物铵盐或所产生的羧酸盐的存在下水解，和 电渗析碱以形成酸和氨或氨水，或形成碱和氨。 获得的酸或碱可以作为腈化合物或酰胺化合物的水解的催化剂再循环，所得氨被作为腈化合物或酰胺化合物的氮源再利用。 这种酰胺化合物可以通过在氧化锰存在下水合亚硝酸盐化合物来制备。
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8.发明申请Basic metal nitrate, process for producing the same and gas generating agent composition 审中-公开碱金属硝酸盐，其制备方法和气体发生剂组合物公开(公告)号：US20070119530A1
公开(公告)日：2007-05-31
申请号：US11216149
申请日：2005-09-01
申请人： Xingxi Zhou , Kazuyuki Matsuoka , Jianzhou Wu , Yo Yamato , Takeshi Takahori , Kaoru Yamazaki
发明人： Xingxi Zhou , Kazuyuki Matsuoka , Jianzhou Wu , Yo Yamato , Takeshi Takahori , Kaoru Yamazaki
IPC分类号： C06B31/00
CPC分类号： C06D5/06 , C01B21/48 , C01G1/08 , C01G3/08 , C01P2002/74 , C01P2004/61 , C01P2004/62 , C01P2006/80 , C06B31/00
摘要： A basic metal nitrate suitable as an oxidizing agent for a gas generating agent, which is a basic metal nitrate having a good thermal stability and meeting at least one requirement of the following (a) to (d): (a) a particle diameter of 0.5 to 40 μm; (b) a degree of crystallinity having 0.4 deg or less of a half band width of the peak in the X-ray analysis; (c) an initiation temperature of weight loss being 220° C. or higher according to TG-DTA analysis; and (d) an impurity content of 1,000 ppm or less based on Na atom. Also, a gas generating composition which has a low toxicity, a high burning rate, and a low combustion temperature and which is used in a gas generator for an air bag. The gas generating composition comprises (a) tetrazole derivatives, guanidine derivatives or a mixture thereof, (b) a basic metal nitrate, and (c) a binder and/or a slag-forming agent.
摘要翻译： 适合作为气体发生剂氧化剂的碱金属硝酸盐，其是具有良好热稳定性并满足以下（a）至（d）的至少一项要求的碱金属硝酸盐：（a） 0.5至40 mum; （b）在X射线分析中的峰的半带宽度为0.4度以下的结晶度; （c）根据TG-DTA分析，重量损失的起始温度为220℃以上; 和（d）基于Na原子的杂质含量为1,000ppm以下。 另外，一种气体发生剂组合物，其具有低毒性，高燃烧速率和低燃烧温度，并且用于气囊的气体发生器。 气体发生组合物包含（a）四唑衍生物，胍衍生物或其混合物，（b）碱金属硝酸盐，和（c）粘合剂和/或成渣剂。
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公开(公告)号：US6100430A
公开(公告)日：2000-08-08
申请号：US142624
申请日：1998-09-10
IPC分类号： B01J27/199 , C07B61/00 , C07C209/26 , C07C211/36 , C07C211/44 , C07C211/54 , C07C211/57 , C07C211/40
CPC分类号： C07C211/36
摘要： An alicyclic polyamine of the formula (1) ##STR1## wherein Y.sub.1 represents a saturated aliphatic hydrocarbon group and R.sub.1 through R.sub.4 are the same or different and each represents hydrogen atom, an alkyl group, a cycloalkyl group, an aryl group, or an aralkyl group. The alicyclic polyamine can be obtained by subjecting a 3-formylcycloalkanone or 3-formylcycloalkenone to reductive amination reaction.
摘要翻译： PCT No.PCT / JP98 / 00192 Sec。 371日期：1998年9月10日 102（e）1998年9月10日PCT PCT 1月20日PCT PCT。 第WO98 / 32729号公报 日期：1998年7月30日，式（1）的脂环族多胺其中Y1表示饱和脂肪族烃基，R1〜R4相同或不同，表示氢原子，烷基，环烷基，芳基或 芳烷基。 脂环族多胺可以通过使3-甲酰基环烷酮或3-甲酰基环烯酮进行还原胺化反应来获得。
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公开(公告)号：US5932454A
公开(公告)日：1999-08-03
申请号：US992545
申请日：1997-12-17
CPC分类号： C12P11/00 , C12P13/02 , C12P7/42 , Y10S435/822
摘要： The method comprises (1) a carboxylic acid salt providing step comprising permitting a strain of microorganism or a preparation derived from the microorganism to act upon a nitrile to thereby (a) provide at least the corresponding amide which is then hydrolyzed in the presence of a base to provide a salt of the corresponding carboxylic acid or (b) provide a salt of the corresponding carboxylic acid and (2) an electrodialysis step comprising subjecting the carboxylic acid salt provided in the step (1) to electrodialysis to provide the corresponding carboxylic acid and base. Carboxylic acids can be produced without formation of ammonium hydrogen sulfate and other byproducts. The microorganism includes microorganisms of the genera Pantoea and Gordona. The ammonia formed in the step (1) can be reused as a nitrogen source in a nitrile production line.
摘要翻译： 该方法包括（1）羧酸盐提供步骤，包括允许微生物菌株或衍生自微生物的制剂作用于腈上，由此（a）提供至少相应的酰胺，然后在 提供相应羧酸的盐，或（b）提供相应羧酸的盐和（2）电渗析步骤，包括使步骤（1）中提供的羧酸盐进行电渗析以提供相应的羧酸 和基地。 可以在不形成硫酸氢铵和其它副产物的情况下生产羧酸。 微生物包括Pantoea属和Gordona属的微生物。 在步骤（1）中形成的氨可以在腈生产线中作为氮源再利用。
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