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1.发明授权Production of self-supporting ceramic materials having a reduced thickness and containing metal oxides 有权生产具有减小厚度并含有金属氧化物的自支撑陶瓷材料公开(公告)号：US08652703B2
公开(公告)日：2014-02-18
申请号：US13377880
申请日：2010-06-16
IPC分类号： H01M8/10
CPC分类号： C04B35/486 , B01D71/024 , B01D2323/225 , B82Y30/00 , C04B35/50 , C04B35/624 , C04B35/645 , C04B38/0074 , C04B2111/00793 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/44 , C04B2235/449 , C04B2235/528 , C04B2235/5409 , C04B2235/5436 , C04B2235/5454 , C04B2235/549 , C04B2235/6567 , C04B2235/666 , C04B2235/77 , C04B2235/9623 , H01M8/1246 , H01M8/1253 , H01M8/126 , H01M2300/0074 , H01M2300/0077 , Y02E60/525 , Y02P70/56 , C04B35/00
摘要： The present invention relates to a method for manufacturing a metal-oxide-based ceramic, including, in order, the step of inserting, into a flash sintering device, a nanocrystalline powder comprising crystallites and crystallite agglomerates of a ceramic of formula, Zr1-xMxO2, where M is chosen from yttrium, scandium and cerium, or Ce1-xM′xO2, where M′ is chosen from gadolinium, scandium, samarium and yttrium, where x lies between 0 and 0.2, the powder having an average crystallite size of between 5 and 50 nm, an average crystallite agglomerate size of between 0.5 and 20 μm, and a specific surface area of between 20 and 100 m2/g. The invention further includes the step of flash sintering the powder by applying a pressure of between 50 and 150 MPa, at a temperature of between 850° C. and 1400° C., for a time of between 5 and 30 minutes.
摘要翻译： 金属氧化物系陶瓷的制造方法技术领域本发明涉及一种金属氧化物系陶瓷的制造方法，其特征在于，依次包括向闪速烧结装置中插入包含式Zr1-xMxO2陶瓷微晶和微晶团聚体的纳米晶体粉末 其中M选自钇，钪和铈，或Ce1-xM'xO2，其中M'选自钆，钪，钐和钇，其中x在0和0.2之间，该粉末的平均微晶尺寸介于 5和50nm，平均微晶聚集体尺寸在0.5和20μm之间，比表面积在20-100m 2 / g之间。 本发明还包括通过在850℃和1400℃之间的温度下施加50-150MPa的压力来烧制粉末的步骤，时间为5-30分钟。
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2.发明申请PRODUCTION OF SELF-SUPPORTING CERAMIC MATERIALS HAVING A REDUCED THICKNESS AND CONTAINING METAL OXIDES 有权生产具有减少厚度和包含金属氧化物的自支撑陶瓷材料公开(公告)号：US20120094214A1
公开(公告)日：2012-04-19
申请号：US13377880
申请日：2010-06-16
IPC分类号： C04B35/48 , H01M8/12 , C25B13/00 , G01N27/28 , B01D71/02 , B01D69/00 , C04B35/46 , H01M8/10 , B32B5/00 , B82Y40/00 , B82Y30/00
CPC分类号： C04B35/486 , B01D71/024 , B01D2323/225 , B82Y30/00 , C04B35/50 , C04B35/624 , C04B35/645 , C04B38/0074 , C04B2111/00793 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/44 , C04B2235/449 , C04B2235/528 , C04B2235/5409 , C04B2235/5436 , C04B2235/5454 , C04B2235/549 , C04B2235/6567 , C04B2235/666 , C04B2235/77 , C04B2235/9623 , H01M8/1246 , H01M8/1253 , H01M8/126 , H01M2300/0074 , H01M2300/0077 , Y02E60/525 , Y02P70/56 , C04B35/00
摘要： The present invention relates to a method for manufacturing a metal-oxide-based ceramic, including, in order, the step of inserting, into a flash sintering device, a nanocrystalline powder comprising crystallites and crystallite agglomerates of a ceramic of formula, Zr1-xMxO2, where M is chosen from yttrium, scandium and cerium, or Ce1-xM′xO2, where M′ is chosen from gadolinium, scandium, samarium and yttrium, where x lies between 0 and 0.2, the powder having an average crystallite size of between 5 and 50 nm, an average crystallite agglomerate size of between 0.5 and 20 μm, and a specific surface area of between 20 and 100 m2/g. The invention further includes the step of flash sintering the powder by applying a pressure of between 50 and 150 MPa, at a temperature of between 850° C. and 1400° C., for a time of between 5 and 30 minutes.
摘要翻译： 金属氧化物系陶瓷的制造方法技术领域本发明涉及一种金属氧化物系陶瓷的制造方法，其特征在于，依次包括向闪速烧结装置中插入包含式Zr1-xMxO2陶瓷微晶和微晶团聚体的纳米晶体粉末 其中M选自钇，钪和铈，或Ce1-xM'xO2，其中M'选自钆，钪，钐和钇，其中x在0和0.2之间，该粉末的平均微晶尺寸介于 5和50nm，平均微晶聚集体尺寸在0.5和20μm之间，比表面积在20和100m2 / g之间。 本发明还包括通过在850℃和1400℃之间的温度下施加50-150MPa的压力来烧制粉末的步骤，时间为5-30分钟。
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3.发明申请Method for preparing catalysts for heterogeneous catalysis by multiple-phase impregnation, catalysts and use of said catalysts 审中-公开通过多相浸渍，催化剂和所述催化剂的使用制备用于多相催化的催化剂的方法公开(公告)号：US20060153765A1
公开(公告)日：2006-07-13
申请号：US10520524
申请日：2003-07-07
申请人： Cuong Pham-Huu , Nicolas Keller , Marc-Jacques Ledoux , Jean-Mario Nhut , Laurie Pesant , Claude Estournes
发明人： Cuong Pham-Huu , Nicolas Keller , Marc-Jacques Ledoux , Jean-Mario Nhut , Laurie Pesant , Claude Estournes
IPC分类号： C01B31/36 , B01J27/224
CPC分类号： B01D53/94 , B01D53/864 , B01J23/42 , B01J27/224 , B01J35/008 , B01J37/0203 , B01J37/0205
摘要： The invention concerns a method for so-called two-phase impregnation of a β-SiC support with high specific surface area, said method comprising at least the following steps: (a) a first impregnating at least once said support with a polar agent A, (b) a second impregnating which consists in impregnating at least once said support with at least an agent B less polar than agent A. Said method enables the production of novel catalysts for heterogeneous catalysis.
摘要翻译： 本发明涉及一种用于具有高比表面积的所谓的两相浸渍β-SiC载体的方法，所述方法至少包括以下步骤：（a）首先用极性试剂A浸渍至少一次所述载体 ，（b）第二浸渍，其包括至少使用至少一种所述载体至少含有比试剂A极性低的试剂B.所述方法能够生产用于多相催化的新型催化剂。
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4.发明申请PROCESS FOR PRODUCING A THERMAL BARRIER IN A MULTILAYER SYSTEM FOR PROTECTING A METAL PART AND PART EQUIPPED WITH SUCH A PROTECTIVE SYSTEM 审中-公开在用于保护金属部件的多层系统中生产热障的方法和装备有这种保护系统的部件公开(公告)号：US20130344349A1
公开(公告)日：2013-12-26
申请号：US14003339
申请日：2012-03-07
申请人： Juliette Hugot , Mathieu Boidot , Daniel Monceau , Djar Oquab , Claude Estournes
发明人： Juliette Hugot , Mathieu Boidot , Daniel Monceau , Djar Oquab , Claude Estournes
CPC分类号： F01D25/08 , B05D3/068 , C23C24/082 , C23C28/321 , C23C28/3455 , C23C28/36 , F01D5/288 , Y02T50/67 , Y02T50/6765 , Y10T428/12458 , Y10T428/12549
摘要： A method for producing a thermal barrier in a multilayered system for protecting a metal part made of superalloy, by producing a thermal treatment by flash sintering protection materials in layers superposed on the metal part in an SPS machine enclosure. The layers contain, on a superalloy substrate, at least two layers of zirconium-based refractory ceramics. A metal part is produced according to a SPS flash sintering method and contains a superalloy substrate, a metal sub-layer, a TGO oxide layer and the thermal barrier formed by the method. A first ceramic is an inner ceramic designed to have a substantially higher expansion coefficient. An outer ceramic is designed to have at least lower thermal conductivity, and at least one of a sintering temperature or maximum operating temperature that is substantially higher. The thermal barrier has a composition and porosity gradient from the metal sub-layer to the outer ceramic.
摘要翻译： 一种用于在用于保护由超级合金制成的金属部件的多层系统中制造热障的方法，通过在SPS机器壳体中重叠在金属部件上的层中通过闪蒸烧结保护材料进行热处理。 这些层在超级合金基底上含有至少两层锆基耐火陶瓷。 根据SPS快速烧结法制造金属部件，并且包含超合金基板，金属子层，TGO氧化物层和通过该方法形成的热障壁。 第一陶瓷是设计成具有显着更高膨胀系数的内陶瓷。 外陶瓷被设计成具有至少较低的热导率，并且烧结温度或最高工作温度中的至少一个基本上更高。 热屏障具有从金属子层到外部陶瓷的组成和孔隙率梯度。
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5.发明授权Part comprising a coating on a superalloy metal substrate, the coating including a metal underlayer 有权部分包括在超合金金属基底上的涂层，该涂层包括金属底层公开(公告)号：US09546566B2
公开(公告)日：2017-01-17
申请号：US14114680
申请日：2012-04-24
申请人： Jean-yves Guedou , Mathieu Boidot , Claude Estournes , Daniel Monceau , Djar Oquab , Serge Selezneff
发明人： Jean-yves Guedou , Mathieu Boidot , Claude Estournes , Daniel Monceau , Djar Oquab , Serge Selezneff
CPC分类号： F01D25/005 , C23C10/00 , C23C10/28 , C23C10/60 , C23C28/321 , C23C28/3455 , C23C30/00 , Y10T428/12618 , Y10T428/12944
摘要： The invention relates to a part comprising a coating on a superalloy metal substrate, the coating comprising a metal underlayer covering said substrate, the part being characterized in that said metal underlayer contains a base of nickel aluminide and also contains 0.5 at % to 0.95 at % of one or more stabilizer elements M from the group formed by Cu and Ag for stabilizing the gamma and gamma prime phases.
摘要翻译： 本发明涉及一种包括在超合金金属基底上的涂层的部分，该涂层包括覆盖所述基底的金属底层，该部分的特征在于所述金属底层含有镍铝化物的基底，并且还含有0.5at％至0.95at％ 的一种或多种稳定剂元素M来自由Cu和Ag形成的基团，用于稳定γ和γ原相。
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公开(公告)号：US10161262B2
公开(公告)日：2018-12-25
申请号：US14003339
申请日：2012-03-07
申请人： Juliette Hugot , Mathieu Boidot , Daniel Monceau , Djar Oquab , Claude Estournes
发明人： Juliette Hugot , Mathieu Boidot , Daniel Monceau , Djar Oquab , Claude Estournes
摘要： A method for producing a thermal barrier in a multilayered system for protecting a metal part made of superalloy, by producing a thermal treatment by flash sintering protection materials in layers superposed on the metal part in an SPS machine enclosure. The layers contain, on a superalloy substrate, at least two layers of zirconium-based refractory ceramics. A metal part is produced according to a SPS flash sintering method and contains a superalloy substrate, a metal sub-layer, a TGO oxide layer and the thermal barrier formed by the method. A first ceramic is an inner ceramic designed to have a substantially higher expansion coefficient. An outer ceramic is designed to have at least lower thermal conductivity, and at least one of a sintering temperature or maximum operating temperature that is substantially higher. The thermal barrier has a composition and porosity gradient from the metal sub-layer to the outer ceramic.
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7.发明申请PART COMPRISING A COATING ON A SUPERALLOY METAL SUBSTRATE, THE COATING INCLUDING A METAL UNDERLAYER 有权包含超级金属基材的涂料，包括金属底层的涂料公开(公告)号：US20140050940A1
公开(公告)日：2014-02-20
申请号：US14114680
申请日：2012-04-24
申请人： Jean-Yves Guedou , Mathieu Boidot , Claude Estournes , Daniel Monceau , Djar Oquab , Serge Selezneff
发明人： Jean-Yves Guedou , Mathieu Boidot , Claude Estournes , Daniel Monceau , Djar Oquab , Serge Selezneff
IPC分类号： F01D25/00
CPC分类号： F01D25/005 , C23C10/00 , C23C10/28 , C23C10/60 , C23C28/321 , C23C28/3455 , C23C30/00 , Y10T428/12618 , Y10T428/12944
摘要： The invention relates to a part comprising a coating on a superalloy metal substrate, the coating comprising a metal underlayer covering said substrate, the part being characterized in that said metal underlayer contains a base of nickel aluminide and also contains 0.5 at % to 0.95 at % of one or more stabilizer elements M from the group formed by Cu and Ag for stabilizing the gamma and gamma prime phases.
摘要翻译： 本发明涉及一种包括在超合金金属基底上的涂层的部分，该涂层包括覆盖所述基底的金属底层，该部分的特征在于所述金属底层含有镍铝化物的基底，并且还含有0.5at％至0.95at％ 的一种或多种稳定剂元素M来自由Cu和Ag形成的基团，用于稳定γ和γ原相。
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