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公开(公告)号：US4840837A
公开(公告)日：1989-06-20
申请号：US214067
申请日：1988-07-01
CPC分类号： B41M5/42 , B41M5/392 , B41M5/395 , B41M5/423 , B41M5/44 , Y10S428/913 , Y10S428/914 , Y10T428/24802 , Y10T428/24901 , Y10T428/24942 , Y10T428/24975 , Y10T428/265 , Y10T428/31551 , Y10T428/31573 , Y10T428/31576 , Y10T428/31587 , Y10T428/31725 , Y10T428/3175 , Y10T428/31757 , Y10T428/31786 , Y10T428/31797 , Y10T428/31801 , Y10T428/31913 , Y10T428/3192 , Y10T428/31928
摘要： A heat transfer medium composed of a base material having thereon in order outwardly from the base material;(a) a colorless or light color heat-fusible transfer layer (A) containing from about 55 to 95 wt % of a wax and from about 5 to 45 wt % of a thermoplastic resin compatible with the wax, based on the whole amount of layer (A); and(b) a heat-softenable ink layer (B) containing from about 50 to 90 wt % of a thermoplastic resin incompatible with the wax in the layer (A) and having adhesion upon heating, from about 3 to 30 wt % of a heat-fusible lubricant, and a coloring material, based on the whole amount of layer (B);the viscosity of layer (A) being from about 100 c.p. to 1,000 c.p. at a temperature 20.degree. C. higher than the melting point of layer (A) shown by a differential scanning calorimeter.The heat transfer medium provides transferred images excellent in rubbing resistance and distinctness.
摘要翻译： 一种传热介质，由其上具有从基材向外依次的基材构成; （a）含有约55至95重量％的蜡和约5至45重量％的与蜡相容的热塑性树脂的无色或浅色热熔转印层（A），基于全部量的 层（A）; 和（b）含有约50〜90重量％的与层（A）中的蜡不相容的热塑性树脂并具有加热粘合性的热软化油墨层（B），约3〜30重量％ 基于层（B）的总量的热熔润滑剂和着色材料; 层（A）的粘度为约100cp. 至1000c.p. 在比差示扫描量热计所示的层（A）的熔点高20℃的温度下进行。 传热介质提供耐摩擦性和清晰度优异的转印图像。
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2.发明授权Method for preparing fluorination catalyst used to fluorinate halogenated hydrocarbons 失效制备用于氟化卤代烃的氟化催化剂的方法
公开(公告)号：US5849658A
公开(公告)日：1998-12-15
申请号：US435166
申请日：1995-05-05
申请人： Takashi Shibanuma , Yoshio Iwai , Satoshi Koyama
发明人： Takashi Shibanuma , Yoshio Iwai , Satoshi Koyama
IPC分类号： B01J23/26 , B01J37/26 , C07C17/20 , C07C17/21 , B01J27/132
CPC分类号： C07C17/21 , B01J23/26 , B01J37/26 , C07C17/206
摘要： A method for preparing a fluorination catalyst is disclosed, wherein the catalyst contains chromium oxide, has a specific surface area of from 170 m.sup.2 g to 300 m.sup.2 /g, catalyzes the fluorination of a halogenated hydrocarbon with hydrogen fluoride, and has a high activity and long catalyst life. The method includes mixing an aqueous solution of a chromium salt with aqueous ammonia to precipitate chromium hydroxide, drying the precipitated chromium hydroxide, sintering the dried chromium hydroxide, and fluorinating the sintered chromium hydroxide to obtain the chromium oxide catalyst.
摘要翻译： 公开了一种制备氟化催化剂的方法，其中催化剂含有氧化铬，比表面积为170m 2 / g至300m 2 / g，催化用氟化氢氟化卤代烃，具有较高的活性和长 催化剂寿命。 该方法包括将铬盐水溶液与氨水混合以沉淀氢氧化铬，干燥沉淀的氢氧化铬，烧结干燥的氢氧化铬，氟化烧结的氢氧化铬得到氧化铬催化剂。
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公开(公告)号：US5475166A
公开(公告)日：1995-12-12
申请号：US282565
申请日：1994-07-29
申请人： Satoshi Koyama , Yukio Homoto , Naoki Esaka
发明人： Satoshi Koyama , Yukio Homoto , Naoki Esaka
CPC分类号： C07C19/08 , C07C17/206 , C07C17/21
摘要： In a process for preparing 1,1,1-trifluorochloroethane by reacting, in a gas phase, trichloroethylene and hydrogen fluoride, when the reactant gases are diluted with a gas which is inactive to the reaction, it is very easy to control a reaction temperature, and when a generated gas from the reaction of 1,1,1-trifluorochloroethane and hydrogen fluoride is used as a diluent gas, generation of 1,1-difluoroethylene is suppressed to a very low level while not influencing the reaction between trichloroethylene and hydrogen fluoride.
摘要翻译： 在通过在气相中使三氯乙烯和氟化氢反应制备1,1,1-三氟氯乙烷的方法中，当反应气体用对反应无活性的气体稀释时，非常容易控制反应温度 ，当使用来自1,1,1-三氟氯乙烷和氟化氢的反应产生的气体作为稀释气体时，1,1-二氟乙烯的产生被抑制到非常低的水平，同时不影响三氯乙烯与氢气之间的反应 氟化物。
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公开(公告)号：US5352657A
公开(公告)日：1994-10-04
申请号：US865637
申请日：1992-04-09
申请人： Utako Endo , Satoshi Koyama , Kazuo Okamura , Tomoji Kawai , Koichi Kitazawa
发明人： Utako Endo , Satoshi Koyama , Kazuo Okamura , Tomoji Kawai , Koichi Kitazawa
CPC分类号： H01L39/2419 , C04B35/4521 , C04B35/4525 , H01L39/126 , Y10S505/737 , Y10S505/782
摘要： A bismuth system oxide superconductor comprising the 110 K phase is effectively prepared by a process comprising the steps of mixing a bismuth compound, a strontium compound, a calcium compound, a copper compound and optionally a lead compound, optionally provisionally sintering the mixture, and sintering the mixture.
摘要翻译： 包含110K相的铋系氧化物超导体通过包括以下步骤的方法有效地制备，所述方法包括以下步骤：混合铋化合物，锶化合物，钙化合物，铜化合物和任选的铅化合物，任选地将该混合物预烧结，并烧结 混合物。
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公开(公告)号：US5326913A
公开(公告)日：1994-07-05
申请号：US897261
申请日：1992-06-11
申请人： Hirokazu Aoyama , Satoshi Koyama
发明人： Hirokazu Aoyama , Satoshi Koyama
IPC分类号： C07C19/10 , C07C17/275 , C07C17/278 , C07C17/26
CPC分类号： C07C17/278
摘要： A fluorinated compound of the formula:R--CCl.sub.2 CF.sub.2 CF.sub.3 (I)in which R is a perfluoroalkyl group, a perchloroalkyl group, a polyfluoroalkyl group, a polychloroalkyl group or a polychloropolyfluoroalkyl group, each having at least one carbon atom is prepared at a high selectivity and a high yield by reacting tetrafluoroethylene with a compound of the formula:R--CFCl.sub.2 (II)in which R is the same as defined above in the presence of a Lewis acid.
摘要翻译： 以高选择性制备具有至少一个碳原子的R为全氟烷基，全氯烷基，多氟烷基，多氯烷基或聚氯多氟烷基的式R-CCl 2 CF 2 CF 3（I）的含氟化合物 并且通过使四氟乙烯与式R-CFCl 2（II）的化合物反应，其中R在路易斯酸存在下与上述相同。
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公开(公告)号：US5026605A
公开(公告)日：1991-06-25
申请号：US343649
申请日：1989-04-27
申请人： Ikuo Kitamura , Hideki Aomi , Satoshi Koyama , Katsushi Tokunaga , Kazuo Okamura
发明人： Ikuo Kitamura , Hideki Aomi , Satoshi Koyama , Katsushi Tokunaga , Kazuo Okamura
CPC分类号： B01J27/22 , C01B31/303 , G11B5/70626 , G11B5/712 , C01P2002/72 , C01P2004/80 , C01P2006/42 , C01P2006/60 , Y10T428/2991 , Y10T428/2993
摘要： Iron carbide fine particles which have a coating layer of at least one metal compound selected from the group consisting of copper compound and manganese compound.
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公开(公告)号：US06676809B1
公开(公告)日：2004-01-13
申请号：US08967539
申请日：1997-11-12
IPC分类号： B01D336
摘要： Hydrogen fluoride is effectively removed from a mixture of hydrogen fluoride, dichloromethane, chlorofluoromethane and/or difluoromethane by distilling the mixture so that two-component azeotropic mixtures of hydrogen fluoride and dichloromethane, hydrogen fluoride and chlorofluoromethane and hydrogen fluoride and difluoromethane are removed, or by liquid-separating the mixture into an upper liquid phase rich in hydrogen fluoride and a lower liquid phase not rich in hydrogen fluoride before each liquid phase is distilled as described above.
摘要翻译： 通过蒸馏混合物从氟化氢，二氯甲烷，氯氟甲烷和/或二氟甲烷的混合物中有效地除去氟化氢，从而除去氟化氢和二氯甲烷，氟化氢和氯氟甲烷和氟化氢和二氟甲烷的双组分共沸混合物，或通过 如上所述，在每个液相被蒸馏之前，将混合物液体分离成富含氟化氢的上液相和不富含氟化氢的较低液相。
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公开(公告)号：US06311515B1
公开(公告)日：2001-11-06
申请号：US09593523
申请日：2000-06-14
IPC分类号： F25J300
摘要： Hydrogen fluoride is effectively removed from a mixture of hydrogen fluoride, dichloromethane, chlorofluoromethane and/or difluoromethane by distilling the mixture so that two-component azeotropic mixtures of hydrogen fluoride and dichloromethane, hydrogen fluoride and chlorofluoromethane and hydrogen fluoride and difluoromethane are removed, or by liquid-separating the mixture into an upper liquid phase rich in hydrogen fluoride and a lower liquid phase not rich in hydrogen fluoride before each liquid phase is distilled as described above.
摘要翻译： 通过蒸馏混合物从氟化氢，二氯甲烷，氯氟甲烷和/或二氟甲烷的混合物中有效地除去氟化氢，从而除去氟化氢和二氯甲烷，氟化氢和氯氟甲烷和氟化氢和二氟甲烷的双组分共沸混合物，或通过 如上所述，在每个液相被蒸馏之前，将混合物液体分离成富含氟化氢的上液相和不富含氟化氢的较低液相。
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9.发明授权Azeotropes of hydrogen fluoride with dichloromethane, difluoromethane and chlorofluoromethane 失效氟化氢与二氯甲烷，二氟甲烷和氯氟甲烷的共沸物
公开(公告)号：US5523015A
公开(公告)日：1996-06-04
申请号：US162010
申请日：1993-12-09
摘要： Hydrogen fluoride is effectively removed from a mixture of hydrogen fluoride, dichloromethane, chlorofluoromethane and/or difluoromethane by distilling the mixture so that two-component azeotropic mixtures of hydrogen fluoride and dichloromethane, hydrogen fluoride and chlorofluoromethane and hydrogen fluoride and difluoromethane are removed, or by liquid-separating the mixture into an upper liquid phase rich in hydrogen fluoride and a lower liquid phase not rich in hydrogen fluoride before each liquid phase is distilled as described above.
摘要翻译： PCT No.PCT / JP93 / 00455 Sec。 371日期1993年12月9日第 102（e）日期1993年12月9日PCT 1993年4月9日PCT公布。 出版物WO93 / 21140 日期为1993年10月28日。通过蒸馏混合物，氟化氢，二氯甲烷，氯氟甲烷和/或二氟甲烷的混合物中有效地除去了氟化氢，使得氟化氢和二氯甲烷，氟化氢和氯氟甲烷和氟化氢的双组分共沸混合物 如上所述，在每个液相被蒸馏之前，除去二氯甲烷，或将混合物液分离成富含氟化氢的上部液相和不富含氟化氢的较低液相。
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公开(公告)号：US5434322A
公开(公告)日：1995-07-18
申请号：US78300
申请日：1993-06-25
申请人： Eiji Seki , Satoshi Koyama
发明人： Eiji Seki , Satoshi Koyama
IPC分类号： B01J23/50 , B01J23/42 , B01J23/48 , B01J23/52 , B01J23/56 , B01J23/60 , B01J23/62 , B01J23/652 , B01J23/89 , B01J27/057 , C07B61/00 , C07C17/00 , C07C17/23 , C07C19/08 , C07C21/18
CPC分类号： B01J23/8926 , B01J23/42 , B01J23/48 , B01J23/56 , C07C17/23
摘要： A process for preparing 1,1-dichloro-2,2,2-trifluoroethane characterized in that 1,1,1-trichloro-2,2,2-trifluoroethane is reduced with hydrogen in the presence of a hydrogenating catalyst comprising platinum to which at least one metal selected from the group consisting of silver, copper, gold, tellurium, zinc, chromium, molybdenum and thallium is added.1,1-Dichoro-2,2,2-trifluoroethne can be obtained in a high yield.
摘要翻译： PCT No.PCT / JP92 / 01398 Sec。 371日期：1993年6月25日 102（e）日期1993年6月25日PCT提交1992年10月29日PCT公布。 公开号WO93 / 09080 日期：1993年5月13日。1，一种制备1,1-二氯-2,2,2-三氟乙烷的方法，其特征在于1,1,1-三氯-2,2,2-三氟乙烷在氢气存在下用氢还原 包含铂的氢化催化剂加入至少一种选自银，铜，金，碲，锌，铬，钼和铊的金属。 可以高产率获得1,1-二氯-2,2,2-三氟乙炔。
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