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公开(公告)号：US07814776B2
公开(公告)日：2010-10-19
申请号：US11719120
申请日：2005-11-10
IPC分类号： G01N29/02
CPC分类号： B82Y30/00 , B82Y15/00 , G01N27/06 , G01N29/022 , G01N29/036 , G01N2291/0212 , G01N2291/0215 , G01N2291/0237 , G01N2291/0256 , G01N2291/02863 , G01N2291/0422 , G01N2291/0423 , G01N2291/0426 , G01N2291/0427 , G01N2291/101
摘要： Methods for sensing and building sensors provide for adding nanotubes to a sensor to improve characteristics such as the Q-factor associated with the sensor. Mass loading and damping characteristics of micromachined quartz crystal resonators on which a thin film of debundled single-walled carbon nanotube (SWNT) has been deposited are disclosed. An absolute mass sensitivity of ˜100 fg was experimentally measured by monitoring the continuous desorption of gases from SWNT surfaces in a vacuum ambient.
摘要翻译： 用于感测和构建传感器的方法提供了向传感器添加纳米管以改善诸如与传感器相关联的Q因子的特性。 公开了其上已经沉积有分解的单层碳纳米管（SWNT）的薄膜的微加工石英晶体谐振器的质量负载和阻尼特性。 通过在真空环境中监测来自SWNT表面的气体的连续解吸，实验测量了约100fg的绝对质量灵敏度。
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2.发明申请公开(公告)号：US20090145233A1
公开(公告)日：2009-06-11
申请号：US11719120
申请日：2005-11-10
IPC分类号： G01H11/00
CPC分类号： B82Y30/00 , B82Y15/00 , G01N27/06 , G01N29/022 , G01N29/036 , G01N2291/0212 , G01N2291/0215 , G01N2291/0237 , G01N2291/0256 , G01N2291/02863 , G01N2291/0422 , G01N2291/0423 , G01N2291/0426 , G01N2291/0427 , G01N2291/101
摘要： Methods for sensing and building sensors provide for adding nanotubes to a sensor to improve characteristics such as the Q-factor associated with the sensor. Mass loading and damping characteristics of micromachined quartz crystal resonators on which a thin film of debundled single-walled carbon nanotube (SWNT) has been deposited are disclosed. An absolute mass sensitivity of ˜100 fg was experimentally measured by monitoring the continuous desorption of gases from SWNT surfaces in a vacuum ambient.
摘要翻译： 用于感测和构建传感器的方法提供了向传感器添加纳米管以改善诸如与传感器相关联的Q因子的特性。 公开了其上已经沉积有分解的单层碳纳米管（SWNT）的薄膜的微加工石英晶体谐振器的质量负载和阻尼特性。 通过在真空环境中监测来自SWNT表面的气体的连续解吸，实验测量了约100fg的绝对质量灵敏度。
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公开(公告)号：US08317983B1
公开(公告)日：2012-11-27
申请号：US12798377
申请日：2010-04-02
IPC分类号： B01J19/12
CPC分类号： C23C14/0605 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C23C14/228 , C23C14/28 , C23C14/541
摘要： Single walled carbon nanotubes are produced in a novel apparatus by the laser-induced ablation of moving carbon target. The laser used is of high average power and ultra-fast pulsing. According to various preferred embodiments, the laser produces and output above about 50 watts/cm2 at a repetition rate above about 15 MHz and exhibits a pulse duration below about 10 picoseconds. The carbon, carbon/catalyst target and the laser beam are moved relative to one another and a focused flow of “side pumped”, preheated inert gas is introduced near the point of ablation to minimize or eliminate interference by the ablated plume by removal of the plume and introduction of new target area for incidence with the laser beam. When the target is moved relative to the laser beam, rotational or translational movement may be imparted thereto, but rotation of the target is preferred.
摘要翻译： 单壁碳纳米管通过激光诱导的移动碳靶的消融在新型装置中产生。 使用的激光器具有高平均功率和超快速脉冲。 根据各种优选实施例，激光器以高于约15MHz的重复频率产生并输出高于约50瓦特/平方厘米，并且表现出低于约10皮秒的脉冲持续时间。 碳，碳/催化剂靶和激光束相对于彼此移动，并且在消融点附近引入侧面泵送的预热惰性气体的聚焦流，以通过去除羽流来最小化或消除被消融的羽流的干扰， 用激光束引入新的目标区域入射。 当目标相对于激光束移动时，可以赋予旋转或平移运动，但是靶的旋转是优选的。
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公开(公告)号：US07014737B2
公开(公告)日：2006-03-21
申请号：US10174477
申请日：2002-06-17
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/17 , C01B2202/02 , Y10S977/845
摘要： Disclosed are methods of purifying mixtures comprising nanofibers and/or nanotubes and residual catalyst particles that are covered by outer layers of the nanotube or nanofiber material. The mixtures are exposed to electromagnetic radiation, which induces localized heating in the residual catalyst particles. The localized heating creates breaches in the outer layers. Thereafter, the residual catalyst particles may be removed under relatively mild conditions that do not significantly affect the structural integrity of the nanotubes or nanofibers. The methods of the invention have been used to particular advantage in the purification of single wall carbon nanotubes (SWNTs) synthesized using metal catalysts. For these SWNTs, microwave radiation is preferably used to induce the localized heating, the outer layers are preferably removed at least in part by carrying out the localized heating under air, and the residual catalyst may be removed by exposure to relatively dilute aqueous acid.
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公开(公告)号：US20100219383A1
公开(公告)日：2010-09-02
申请号：US12530369
申请日：2008-03-07
申请人： Peter C. Eklund
发明人： Peter C. Eklund
CPC分类号： B82Y40/00 , B82Y10/00 , B82Y30/00 , C01B32/162 , C01B2202/02 , H01L51/0048
摘要： The present invention generally relates to methods and apparatus for the synthesis or preparation of boron-doped single-walled carbon nanotubes (B-SWCNTs). The invention provides a high yield, single step method for producing large quantities of continuous macroscopic carbon fiber from single-wall carbon nanotubes using inexpensive carbon feedstocks wherein the carbon nanotubes are produced by in situ boron substitutional doping. In one embodiment, the nanotubes disclosed are used, singularly or in multiples, in power transmission cables, in solar cells, in batteries, as antennas, as molecular electronics, as probes and manipulators, and in composites. It is another object of this invention to provide macroscopic carbon fiber made by such a method.
摘要翻译： 本发明一般涉及用于合成或制备硼掺杂单壁碳纳米管（B-SWCNT）的方法和装置。 本发明提供了一种高产率的单步法，用于使用廉价的碳原料从单壁碳纳米管制备大量的连续宏观碳纤维，其中碳纳米管是通过原位硼取代掺杂生产的。 在一个实施例中，公开的纳米管单独地或多次地用于输电电缆，太阳能电池，电池，天线，分子电子学，探针和操纵器以及复合材料中。 本发明的另一个目的是提供由这种方法制成的宏观碳纤维。
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公开(公告)号：US5453413A
公开(公告)日：1995-09-26
申请号：US73533
申请日：1993-06-08
申请人： Peter C. Eklund
发明人： Peter C. Eklund
IPC分类号： B01D53/22 , B01D71/02 , C01B13/02 , C01B31/02 , C30B23/02 , G03C1/73 , G03F7/027 , B01J20/20
CPC分类号： B82Y30/00 , B01D53/228 , B01D71/021 , B82Y40/00 , C01B13/0262 , C01B31/0206 , C01B31/0213 , C30B23/02 , C30B29/02 , G03C1/73 , G03F7/027 , Y10S977/736
摘要： Compounds consisting of two or more fullerenes (e.g., a C.sub.60 dimer) and a film or powder which includes covalently linked fullerene molecules. Also disclosed is a fullerene film or powder with gas molecules or atoms uniformly disposed therein, as well as a method of diffusing gas molecules or atoms into or through a film or powder made of pristine fullerene molecules.
摘要翻译： 由两种或更多种富勒烯（例如C 60二聚体）组成的化合物和包含共价连接的富勒烯分子的膜或粉末。 还公开了具有均匀地设置在其中的气体分子或原子的富勒烯膜或粉末，以及将气体分子或原子扩散到通过由原始富勒烯分子制成的膜或粉末中的方法。
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7.发明申请In vivo photodynamic therapy of cancer via a near infrared agent encapsulated in calcium phosphate nanoparticles 有权通过封装在磷酸钙纳米粒子中的近红外线的体内光动力治疗癌症公开(公告)号：US20100247436A1
公开(公告)日：2010-09-30
申请号：US12657556
申请日：2010-01-22
申请人： James H. Adair , Mark Kester , Peter C. Eklund , Karen L. Eklund , Erhan Altinoglu , Brian M. Barth , Timothy J. Russin , James M.D. Kaiser , Thomas T. Morgan
发明人： James H. Adair , Mark Kester , Peter C. Eklund , Karen L. Eklund , Erhan Altinoglu , Brian M. Barth , Timothy J. Russin , James M.D. Kaiser , Thomas T. Morgan
CPC分类号： A61K41/0057 , A61K9/51 , A61K47/6921 , A61K47/6923
摘要： Nano-encapsulated photosensitizers and their use in the treatment of tumors and/or imaging is described. Preferably, the photosensitizers are encapsulated in a calcium phosphate nanoparticle (CPNP). Encapsulating the PS in a CPNP increases the half-life of the PS, increases absorption of the PS into the target cell tissue, increases the photostability of the PS, increases the photoefficiency of the PS, increases in vivo retention of the PS, or combinations thereof, ultimately making it a highly efficacious agent for use in photodynamic therapy, imaging target tissues, vessels, or tumors, and/or detecting or locating tumors.
摘要翻译： 描述了纳米包封的光敏剂及其在治疗肿瘤和/或成像中的用途。 优选地，将光敏剂包封在磷酸钙纳米颗粒（CPNP）中。 将PS封装在CPNP中增加PS的半衰期，增加PS进入靶细胞组织的吸收，增加PS的光稳定性，增加PS的光效，增加PS的体内保留或组合 最终使其成为用于光动力疗法，成像靶组织，血管或肿瘤，和/或检测或定位肿瘤的高效药物。
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公开(公告)号：US06869583B2
公开(公告)日：2005-03-22
申请号：US10120827
申请日：2002-04-12
CPC分类号： B82Y30/00 , B82Y40/00 , C01B3/001 , C01B3/0021 , C01B32/17 , C01B2202/02 , D01F9/12 , Y02E60/325 , Y02E60/327 , Y10S977/848
摘要： Carbon structures, e.g. carbon nano-fibers, suitable for absorbing hydrogen at low pressures and low temperatures are produced by a selective oxidation and/or acid reflux process. The process includes heating an impure mixture containing a crystalline form of carbon in the presence of an oxidizing gas at a temperature and time sufficient to selectively oxidize and remove a substantial amount of any amorphous carbon impurities from the mixture. Metal containing impurities can be removed from the mixture by exposing the desired carbon and accompanying impurities to an acid to produce a carbon fiber that is substantially free of both non-fiber carbon impurities and metal impurities. Another aspect of the present invention includes purified carbon structures that can store hydrogen at low pressures and temperatures.
摘要翻译： 碳结构，例如 通过选择性氧化和/或酸回流过程产生适合于在低压和低温下吸收氢的碳纳米纤维。 该方法包括在氧化气体存在下加热含有结晶形式的不纯的混合物，该温度和时间足以选择性氧化和从混合物中除去大量的任何无定形碳杂质。 通过将所需的碳和伴随的杂质暴露于酸中以产生基本上不含非纤维碳杂质和金属杂质的碳纤维，可以从混合物中除去含金属杂质。 本发明的另一方面包括可以在低压和低温下储存氢的纯化碳结构。
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公开(公告)号：US07692116B1
公开(公告)日：2010-04-06
申请号：US10188525
申请日：2002-07-03
IPC分类号： B23K26/12
CPC分类号： C23C14/0605 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C23C14/228 , C23C14/28 , C23C14/541
摘要： Single walled carbon nanotubes are produced in a novel apparatus by the laser-induced ablation of moving carbon target. The laser used is of high average power and ultra-fast pulsing. According to various preferred embodiments, the laser produces an output above about 50 watts/cm2 at a repetition rate above about 15 MHz and exhibits a pulse duration below about 10 picoseconds. The carbon, carbon/catalyst target and the laser beam are moved relative to one another and a focused flow of “side pumped”, preheated inert gas is introduced near the point of ablation to minimize or eliminate interference by the ablated plume by removal of the plume and introduction of new target area for incidence with the laser beam. When the target is moved relative to the laser beam, rotational or translational movement may be imparted thereto, but rotation of the target is preferred.
摘要翻译： 单壁碳纳米管通过激光诱导的移动碳靶的消融在新型装置中产生。 使用的激光器具有高平均功率和超快速脉冲。 根据各种优选实施例，激光器以高于约15MHz的重复频率产生大于约50瓦特/平方厘米的输出，并且表现出低于约10皮秒的脉冲持续时间。 碳，碳/催化剂靶和激光束相对于彼此移动，并且在消融点附近引入预热的惰性气体的聚焦流动，以最小化或消除被消除的羽流的干扰， 羽流和引入新的目标区域与激光束的入射。 当目标相对于激光束移动时，可以赋予旋转或平移运动，但是靶的旋转是优选的。
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公开(公告)号：US07338648B2
公开(公告)日：2008-03-04
申请号：US10326276
申请日：2002-12-23
IPC分类号： B82B3/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/1272 , Y10S977/843
摘要： The present invention is directed towards a method of producing single wall carbon nanotubes which comprises providing a catalyst comprising an alumina support and a component selected from the group consisting of reduced Fe, reduced Fe/Mo, Fe oxide, and Fe/Mo oxide, and growing, in an inert atmosphere, single wall carbon nanotubes by passing a gas comprising methane over the catalyst at a temperature and for a time sufficient to grow single wall carbon nanotubes. The invention is also directed towards a single wall carbon nanotube produced by such a method. The invention is also directed towards a catalyst for producing SWNTs, wherein the catalyst comprises an alumina support and a component selected from the group consisting of reduced Fe, reduced Fe/Mo, Fe oxide, and Fe/Mo oxide.
摘要翻译： 本发明涉及一种制备单壁碳纳米管的方法，其包括提供包含氧化铝载体和选自还原Fe，还原Fe / Mo，Fe氧化物和Fe / Mo氧化物的组分的催化剂，以及 在惰性气氛中通过在包含甲烷的气体在催化剂上经过足以使单壁碳纳米管生长的温度和时间内使单壁碳纳米管生长。 本发明还涉及通过这种方法制备的单壁碳纳米管。 本发明还涉及用于制备SWNT的催化剂，其中催化剂包含氧化铝载体和选自还原Fe，还原Fe / Mo，Fe氧化物和Fe / Mo氧化物的组分。
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