摘要:
Static mixer module, consisting of a disc which is provided with a multiplicity of orifices (6) and is structured on its front side and on its rear side by means of channels (4, 5), and in which the orifices (6) are made in the flanks (8) of the inlet channels (4) and open into the flanks (9) of the mixing channels (5). Furthermore, a mixer arrangement is described, which consists of at least two static mixer elements arranged one behind the other, at least one mixer element being a disc-shaped static mixer module. The mixer module and the mixer arrangement are used in pipelines and housings through which a flow passes.
摘要:
A combination static mixer and heat exchanger having heat exchanger tubes (1) which are provided over their circumference with fins (2a, 2b) which have a static mixing effect.
摘要:
A process for concentrating polymers by evaporation is disclosed. The process entails (i) obtaining a mixture containing a polymer and volatile component, the volatile components being present in the mixture at an amount less than 20 wt. % relative to the weight of the mixture, and (ii) introducing the mixture in a downward direction under pressure through a plurality of nozzles arranged vertically and next to one another into a degassing container to form an extrudate. The volatile component contains at least one of residual monomers, oligomers and solvents, and the throughput of the mixture per nozzle is 0.3 to 2 kg/h. The vapor pressure of the volatile component of the extrudate is more than 2.5 bar, and the absolute pressure in the degassing container is 50 to 5000 Pa. The polymer prepared by the process is characterized in that it contains volatile components in an amount of less than 300 ppm.
摘要:
Apparatus for carrying out mass transfer processes with high-viscosity liquids comprising a vertically arranged vessel (1) having a feeder (4) for the liquid to be treated, an outlet (7) for volatile components and an outlet (6) for the treated liquid, the feeder means (4) being equipped with a distributor element (3) having a multiplicity of orifices (8, 10) for subdividing the high-viscosity liquid to be treated into a multiplicity of individual streams, wherein essentially vertically arranged wire loops (2) are disposed in the vicinity of the orifices (8, 10), along which wire loops the high-viscosity liquid runs off under the action of gravity.
摘要:
The invention relates to polycarbonates with extremely low residual levels of volatile constituents and thermal degradation products, and also improved optical properties, especially Yellowness Index (YI) and good thermal stability, from solvent-containing polymer melts. The invention further relates to an apparatus and a process for preparing these polycarbonates with the aid of a devolatilizing extruder with at least three devolatilizing zones, and zones for introducing entraining agent into dispersion are present upstream of at least three devolatilizing zones.
摘要:
A process for producing a polyamide or copolyamide freed from volatile constituents by removing the volatile constituents, in particular the monomers and dimers, in at least two stages from the polymer melt by using an, in particular, gaseous entrainer is described. The invention also relates to polyamide compositions made of polyamide 6 or a copolyamide with a reduced volatile constituent content, as well as moulding compositions made of the above-mentioned polyamides, and moulded articles and fibers which are produced from these moulding compositions.
摘要:
This invention relates to a multistep process for evaporating polymer solutions of thermoplastic polymers and for removing volatile constituents from thermoplastic polymers by indirect heat exchange. The invention relates in particular to a process for evaporating volatile constituents out of polymer solutions using shell-and-tube heat exchangers having a special geometry, coiled-tube evaporators and extrusion evaporators.
摘要:
The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a flash devolatilizer and a vented extruder.
摘要:
The invention relates to an apparatus and a process for devolatilizing solvent-containing polycarbonate solutions. By employing the inventive apparatus, polycarbonates with low residual values of volatile constituents are produced from solvent-containing polymer melts, which improved optical properties, especially yellowness index, with the aid of an apparatus combination of a heatable tubular devolatilizer and a vented extruder.
摘要:
Evaporator apparatus (1) for the treatment of viscous media comprised of at least a feed chamber (2) having a perforated tray (3), a tube-bundle heat exchanger (4) connected thereto having perpendicularly arranged tubes (8) and a devolatilization chamber (5) connected thereto, a discharge unit (6) for the product and a vapor take-off (7) for removing volatile components, the tubes (8) of the heat exchanger (4) having a rectangular cross section over the greater part of their length.