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    Alkylene oxide block polymers usable as defoamers
    2.
    发明授权
    Alkylene oxide block polymers usable as defoamers 失效
    可用作消泡剂的环氧烷嵌段聚合物

    公开(公告)号：US4745231A

    公开(公告)日：1988-05-17

    申请号：US893756

    申请日：1986-08-06

    申请人： Fritz Lange ,  Rainer Hoefer ,  Karl-Heinz Schmid ,  Adolf Asbeck ,  Klaus Herrmann

    发明人： Fritz Lange ,  Rainer Hoefer ,  Karl-Heinz Schmid ,  Adolf Asbeck ,  Klaus Herrmann

    IPC分类号： B01D19/04 ,  C08G65/26 ,  C08G65/28 ,  C08G65/32 ,  C08G65/34 ,  C11D3/37 ,  C07C43/11

    CPC分类号： B01D19/04 ,  B01D19/0404 ,  C08G65/2609 ,  C11D3/0026 ,  C11D3/3707 ,  Y10S516/92

    摘要： Block polymers usable as defoamers have the following formula ##STR1## in which R represents a glycerol or polyglycerol function having a degree of polymerization x of from 1 to 6 and the indices y is equal to (x-z+2), z is equal to (x-y+2), a is equal to 1 to 15, b is equal to 50 to 200 c is equal to 1 to 15, d is equal to 20 to 150 and e is equal to 1 to 15, with the proviso that the sums (a+c+e) is equal to 2 to 20, (b+d) is equal to 50 to 250 and (c+e) is equal to 1 to 15, and y has a value of at least 1.The block polymers are prepared by reaction of glycerol or polyglycerol having a degree of polymerization x with ethylene oxide, then with propylene oxide and, finally, again with ethylene oxide, preferably in the presence of alkaline etherification catalysts.

    摘要翻译： 可用作消泡剂的嵌段聚合物具有下式（IMAGE），其中R表示聚合度x为1至6且指数y等于（x-z + 2）的甘油或聚甘油官能团，z等于 至（x-y + 2），a等于1至15，b等于50至200c等于1至15，d等于20至150，e等于1至15，其中 条件是（a + c + e）之和等于2至20，（b + d）等于50至250，（c + e）等于1至15，y至少为 嵌段聚合物通过具有聚合度x与环氧乙烷然后与环氧丙烷的甘油或聚甘油反应制备，最后再次与环氧乙烷反应，优选在碱性醚化催化剂的存在下进行。

    Polymerization emulsifiers
    3.
    发明授权
    Polymerization emulsifiers 失效
    聚合乳化剂

    公开(公告)号：US4657999A

    公开(公告)日：1987-04-14

    申请号：US801016

    申请日：1985-11-22

    申请人： Rainer Hoefer ,  Karl-Heinz Schmid ,  Bernd Wegemund

    发明人： Rainer Hoefer ,  Karl-Heinz Schmid ,  Bernd Wegemund

    IPC分类号： C08F2/30 ,  B01F17/56 ,  C08F2/24 ,  C08F2/00

    CPC分类号： C08F2/24

    摘要： The use of alkyl glycosides of C.sub.8 -C.sub.22 alkanols and reducing sugars, in which one sugar chain containing on average from 1 to 10 sugar residues attached to one another by glycoside bonds is present for every alkyl group, as co-emulsifiers or emulsifiers in the emulsion polymerization of ethylenically unsaturated monomers.

    摘要翻译： 使用C8-C22链烷醇和还原糖的烷基糖苷，其中通过糖苷键将平均1至10个糖残基彼此相连的一个糖链作为每个烷基存在，作为共乳化剂或乳化剂 烯属不饱和单体的乳液聚合。

    Foam inhibitors for polymer dispersions
    4.
    发明授权
    Foam inhibitors for polymer dispersions 失效
    用于聚合物分散体的泡沫抑制剂

    公开(公告)号：US4981893A

    公开(公告)日：1991-01-01

    申请号：US136237

    申请日：1987-12-21

    申请人： Rainer Hoefer ,  Karl-Heinz Schmid ,  Adolf Asbeck ,  Uwe Held

    发明人： Rainer Hoefer ,  Karl-Heinz Schmid ,  Adolf Asbeck ,  Uwe Held

    IPC分类号： B01J13/00 ,  B01D19/04 ,  B01F17/42 ,  C08F2/30

    CPC分类号： C08F2/30 ,  B01D19/0404

    摘要： Compounds corresponding to the following formulaR.sub.1 --(CH.sub.2).sub.m --O--(CH.sub.2 CH.sub.2).sub.n --R.sub.2in which R.sub.1 is the phenyl radical or a phenyl radical which is substituted by linear or branched alkyl radicals containing a total of from 1 to 18 carbon atoms, R.sub.2 is a C.sub.4 -C.sub.8 alkyl radical, m=0 or 1 and n=3 to 30, are used as dispersants with foam-inhibiting properties in aqueous polymer dispersions and latices.

    摘要翻译： 对应于下式R1-（CH2）mO-（CH2CH2）n-R2的化合物，其中R 1是苯基或被含有总共1至18个碳原子的直链或支链烷基取代的苯基， R2是C4-C8烷基，m = 0或1，n = 3〜30，在聚合物水分散体和胶乳中用作具有泡沫抑制性质的分散剂。

    Continuous bulk polymerization process
    7.
    发明授权
    Continuous bulk polymerization process 失效
    连续本体聚合工艺

    公开(公告)号：US06362296B1

    公开(公告)日：2002-03-26

    申请号：US09183229

    申请日：1998-10-30

    申请人： Shruti Singhal ,  Rainer Hoefer ,  John E. Nowicki ,  George Roth ,  Darmesh Chovatia ,  Shailesh Shah

    发明人： Shruti Singhal ,  Rainer Hoefer ,  John E. Nowicki ,  George Roth ,  Darmesh Chovatia ,  Shailesh Shah

    IPC分类号： C08J22010

    CPC分类号： C08F20/18 ,  C08F20/10

    摘要： The invention relates to a process for producing a polymer or copolymer from monomer material comprising an acrylate, methacrylate, or mixture of such monomers, which comprises the steps of: (a) charging into a continuous tube reactor a feedstock comprising said monomer material and a polymerization initiator; (b) maintaining a flow rate of said material through the reactor at a reaction temperature in the reactor and under pressure sufficient to provide a residence time of the feedstock in the reactor during which polymerization will occur, to form a resin product in the reactor, and said resulting resin product comprising unreacted monomer, and (c) devolatilizing said resin product exiting the reactor to remove unreacted monomers, to provide a substantially monomer-free resin product. Further, the invention relates to resin product made by the process. In particular, the invention relates to resin that has a weight average molecular weight of 10,000 or less, and a glass transition temperature of less than 0° C., preferably −20° C. or lower. The resin product of the invention is particularly useful as an additive for coating and casting resin systems.

    摘要翻译： 本发明涉及由包含丙烯酸酯，甲基丙烯酸酯或这些单体的混合物的单体材料制备聚合物或共聚物的方法，其包括以下步骤：（a）将连续管式反应器装入包含所述单体材料的原料和 聚合引发剂; （b）在反应器中的反应温度和足够的压力下保持所述材料通过反应器的流速，以提供原料在聚合反应期间的停留时间，以便在反应器中形成树脂产物， 并且所述得到的树脂产品包含未反应的单体，和（c）使离开反应器的所述树脂产物脱挥发分以除去未反应的单体，以提供基本上不含单体的树脂产物。 此外，本发明涉及通过该方法制备的树脂产品。 特别地，本发明涉及重均分子量为10,000以下，玻璃化转变温度低于0℃，优选为-20℃以下的树脂。 本发明的树脂产品特别可用作涂料和浇铸树脂体系的添加剂。

    Method of coating electrically conductive substrates
    8.
    发明授权
    Method of coating electrically conductive substrates 失效
    涂敷导电性基材的方法

    公开(公告)号：US6146512A

    公开(公告)日：2000-11-14

    申请号：US194825

    申请日：1998-12-03

    申请人： Rainer Hoefer ,  Heinz-Guenther Schulte ,  Harald Frommelius

    发明人： Rainer Hoefer ,  Heinz-Guenther Schulte ,  Harald Frommelius

    IPC分类号： B01D19/04 ,  C08F2/58 ,  C08G65/332 ,  C09D5/44 ,  C09D7/12 ,  C09D171/02 ,  C25D13/10 ,  C08K3/20

    CPC分类号： C08G65/332 ,  C09D171/02 ,  C09D5/4492

    摘要： A process for controlling foam in a water-based electrophoretic coating bath for coating an electrically conductive substrate wherein the bath contains at least one cathodically depositable synthetic resin by adding to the bath a polyalkylene oxide compound whose oxyalkyl groups contain 2 to 4 carbon atoms and the terminal OH groups are esterified with a carboxylic acid or etherified with an allyl or methyl aryl group and has a solubility of more than 50 parts by weight in 100 parts by weight of water at 25.degree. C.

    摘要翻译： PCT No.PCT / EP97 / 02621 Sec。 371日期1998年12月3日第 102（e）日期1998年12月3日PCT提交1997年5月22日PCT公布。 公开号WO97 / 46628 PCT 日期1997年12月11日一种用于在水性电泳涂层中控制泡沫的方法，用于涂覆导电基材，其中所述浴含有至少一种阴极可沉积的合成树脂，其通过向所述浴中加入氧烷基含有2至 4个碳原子和末端OH基团被羧酸酯化或用烯丙基或甲基芳基醚化，并且在25℃下在100重量份水中的溶解度大于50重量份。

    Fatty oil ex Helianthus annuus for the production of emulsifiers for emulsion polymerization
    10.
    发明授权
    Fatty oil ex Helianthus annuus for the production of emulsifiers for emulsion polymerization 失效
    向日葵的脂肪油生产用于乳液聚合的乳化剂

    公开(公告)号：US5296576A

    公开(公告)日：1994-03-22

    申请号：US955393

    申请日：1992-10-01

    申请人： Rainer Hoefer ,  Horst Eierdanz

    发明人： Rainer Hoefer ,  Horst Eierdanz

    IPC分类号： B01F17/00 ,  C08F2/24 ,  C08F2/26 ,  C08K5/09

    CPC分类号： C08F2/26

    摘要： The use of fatty oil ex Helianthus annuus containing 78 to 92% by weight oleic acid and 2 to 10% by weight linoleic acid for the production of alkali metal, ammonium and/or alkanolammonium salts of optionally dihydroxy-substituted fatty acids as emulsifiers for emulsion polymerization. Excellent polymerization results are obtained despite the high linoleic acid content.

    摘要翻译： 使用含有78〜92重量％油酸和2〜10重量％亚油酸的向日葵的脂肪油用于生产任选的二羟基取代的脂肪酸的碱金属，铵和/或烷醇铵盐作为乳液的乳化剂 聚合。 尽管亚油酸含量高，但仍获得良好的聚合效果。