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    Method for esterification of free fatty acids in triglycerides
    3.
    发明申请
    Method for esterification of free fatty acids in triglycerides 审中-公开
    在甘油三酸酯中游离脂肪酸酯化的方法

    公开(公告)号：US20100121087A1

    公开(公告)日：2010-05-13

    申请号：US12454649

    申请日：2009-05-21

    申请人： Rajiv Manohar Banavali ,  Robert Tryon Hanlon ,  Alfred Karl Schultz

    发明人： Rajiv Manohar Banavali ,  Robert Tryon Hanlon ,  Alfred Karl Schultz

    IPC分类号： C11C3/00

    CPC分类号： C11C3/003 ,  C11C3/08 ,  Y02E50/13 ,  Y02P30/20

    摘要： A method for esterification of free fatty acids with methanol. The method has steps of: (a) contacting a heterogeneous esterification catalyst in a reactor with a reaction mixture containing: (i) methanol and (ii) a triglyceride mixture containing 70-99.8 wt % triglycerides and 0.2-30 wt % free fatty acids, under conditions suitable for esterification, to produce a product stream; (b) separating water and methanol from the product stream to produce a dried product stream; (c) contacting the dried product stream with methanol to produce a methanol-rich phase and a triglyceride-rich phase; and (d) separating the methanol-rich phase and recycling it to the reactor.

    摘要翻译： 游离脂肪酸与甲醇酯化的方法。 该方法具有以下步骤：（a）将反应器中的异相酯化催化剂与反应混合物接触，所述反应混合物包含：（i）甲醇和（ii）含有70-99.8wt％甘油三酸酯和0.2-30wt％游离脂肪酸的甘油三酯混合物 在适于酯化的条件下，产生产物流; （b）从产物流中分离水和甲醇以产生干燥的产物流; （c）使干燥产物流与甲醇接触以产生富含甲醇的相和富含甘油三酯的相; 和（d）分离富含甲醇的相并将其再循环到反应器中。

    Method for selective esterification of free fatty acids in triglycerides
    8.
    发明申请
    Method for selective esterification of free fatty acids in triglycerides 审中-公开
    在甘油三酯中选择性酯化游离脂肪酸的方法

    公开(公告)号：US20110065943A1

    公开(公告)日：2011-03-17

    申请号：US12586003

    申请日：2009-09-16

    申请人： Rajiv Manohar Banavali ,  Alfred Karl Schultz

    发明人： Rajiv Manohar Banavali ,  Alfred Karl Schultz

    IPC分类号： C11C3/00

    CPC分类号： C11C3/003

    摘要： A method for the selective esterification of free fatty acids, alone or in triglycerides, with C1-C8 aliphatic alcohols or diols. The method uses a selective heterogeneous esterification catalyst. The catalyst is contacted with a reaction mixture containing a triglyceride having at least 0.5% free fatty acids, or a reaction mixture containing only free fatty acids, and a C1-C8 aliphatic alcohol or diol under conditions suitable for esterification.

    摘要翻译： 用C1-C8脂族醇或二醇选择性酯化单独或甘油三酸酯的游离脂肪酸的方法。 该方法使用选择性异相酯化催化剂。 使催化剂与含有至少0.5％游离脂肪酸的甘油三酯或仅含游离脂肪酸的反应混合物和C1-C8脂族醇或二醇在适于酯化的条件下反应混合物接触。