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    Blocked mercaptosilane coupling agents for filled rubbers
    4.
    发明授权
    Blocked mercaptosilane coupling agents for filled rubbers 有权

    公开(公告)号：US07074876B2

    公开(公告)日：2006-07-11

    申请号：US09986515

    申请日：2001-11-09

    申请人： Richard W. Cruse ,  Robert J. Pickwell ,  Keith J. Weller ,  Eric R. Pohl

    发明人： Richard W. Cruse ,  Robert J. Pickwell ,  Keith J. Weller ,  Eric R. Pohl

    IPC分类号： C07F7/04 ,  C07F7/08 ,  C07F7/10 ,  C07F9/165 ,  C07F9/38

    CPC分类号： C07F9/4075 ,  C07F7/1804 ,  C07F9/1651 ,  C08J3/203 ,  C08J2321/00 ,  C08K3/013 ,  C08K3/36 ,  C08K5/0025 ,  C08K5/5406 ,  C08K5/548 ,  C08L9/00 ,  C08L9/06 ,  C08L21/00 ,  C08L2666/08

    摘要： Disclosed herein is a blocked mercaptosilane selected from the group consisting of [[(ROC(═O))p—(G)j]k—Y—S]r—G—(SiX3)s; and  (1) [(X3Si)q—G]a—[Y—[S—G—SiX3]b]c  (2) wherein Y is a polyvalent species (Q)zA(═E) selected from the group consisting of —C(═NR)—; —SC(═NR)—; —SC(═O)—; —OC(═O)—; —S(═O)—; —S(═O)2—; —OS(═O)2—; (—NR)S(═O)2—; —SS(═O)—; —OS(═O)—; (—NR)S(═O)—; —SS(═O)2—; (—S)2P(═O)—; —(—S)P(═O)—; —P(═O)(—)2; (—S)2P(═S)—; —(—S)P(═S)—; —P(═S)(—)2; (—NR)2P(═O)—; (—NR)(—S)P(═O)—; (—O)(—NR)P(═O)—; (—O)(—S)P(═O)—; (—O)2P(═O)—; —(—O)P(═O)—; —(—NR)P(═O)—; (—NR)2P(═S)—; (—NR)(—S)P(═S)—; (—O)(—NR)P(═S)—; (—O)(—S)P(═S)—; (—O)2P(═S)—; —(—O)P(═S)—; and —(—NR)P(═S)—; wherein the atom A attached to unsaturated heteroatom E is attached to the sulfur which in turn is linked via a group G to the silicon atom; each R is chosen independently from hydrogen, straight, cyclic, or branched alkyl that may or may not contain unsaturation, alkenyl groups, aryl groups, and aralkyl groups, with each R containing from 1 to 18 carbon atoms;each G is independently a monovalent or polyvalent group derived by substitution of alkyl, alkenyl, aryl, or aralkyl, wherein G can contain from 1 to 18 carbon atoms, with the proviso that G is not such that the blocked mercaptosilane would contain an α,β-unsaturated carbonyl that can undergo polymerization reactions, and if G is univalent, G can be a hydrogen atom;X is independently selected from the group consisting of —Cl, —Br, RO—, RC(═O)O—, R2C═NO—, R2NO—, R2N—, —R, and —(OSiR2)t(OSiR3) wherein each R is as above and at least one X is not —R;p is 0 to 5; r is 1 to 3; z is 0 to 2; q is 0 to 6; a is 0 to 7; b is 1 to 3; j is 0 to 1, but it may be 0 only if p is 1; c is 1 to 6; t is 0 to 5; s is 1 to 3; k is 1 to 2; with the provisos that (I) if A is carbon, sulfur or sulfonyl, then (i) a+b is 2 and (ii) k is 1; (II) if A is phosphorus, then a+b is 3 unless both (i) c is greater than 1 and (ii) b is 1, in which case a is c+1; and (III) if A is phosphorus, then k is 2.

    Silane compositions, processes for their preparation and rubber compositions containing same
    8.
    发明授权
    Silane compositions, processes for their preparation and rubber compositions containing same 有权
    硅烷组合物，其制备方法和含有它们的橡胶组合物

    公开(公告)号：US07531588B2

    公开(公告)日：2009-05-12

    申请号：US10918828

    申请日：2004-08-13

    申请人： Keith J. Weller ,  Lesley Hwang ,  Richard W. Cruse ,  Leda Gonzalez ,  Robert J. Pickwell ,  Martin Hofstetter ,  Wesley E. Sloan ,  Prashant G. Joshi

    发明人： Keith J. Weller ,  Lesley Hwang ,  Richard W. Cruse ,  Leda Gonzalez ,  Robert J. Pickwell ,  Martin Hofstetter ,  Wesley E. Sloan ,  Prashant G. Joshi

    IPC分类号： C08K5/24 ,  C07F7/04

    CPC分类号： C08K5/5425 ,  C07F7/1804 ,  C08K5/5406 ,  C08L21/00

    摘要： Silane compositions of the general formula are provided herein comprising [(RO)x(R1)(3-x)—Si-Mt]q-L-[(Ra)cAr—(CR2═CR22)y]z wherein R and R1 are independently a hydrocarbon group of from 1 to about 20 carbon atoms; R2 are each independently hydrogen or a hydrocarbon group of from 1 to about 20 carbon atoms; M optionally is a divalent hydrocarbon connecting group of from 1 to about 20 carbon atoms to link the silicon atom and the L group; L is a covalently bound hydrocarbon linking group of from 1 to about 20 carbon atoms or a heteroatom linking group selected from the group consisting of —O—, —S—, —NR3— wherein R3 is hydrogen or a hydrocarbon group of from 1 to about 20 carbon atoms; Ra is an alkyl group of 1 to 12 carbon atoms; Ar is a substituted or unsubstituted aromatic group; q is an integer of 1 to 4; t and c are each independently 0 or 1; and x, y and z are each independently integers of 1 to 3, inclusive, with the proviso that t is 1 when L is a heteroatom group. Also provided are processes for preparing the silane compositions and rubber composition comprising the silane compositions.

    摘要翻译： 本文提供的硅烷组合物包括<？in-line-formula description =“In-line Formulas”end =“lead”？> [（RO）x（R1）（3-x）-Si-Mt] qL- [（Ra）cAr-（CR2-CR22）y] z <βin-line-formula description =“In-line Formulas”end =“tail”？>其中R和R 1独立地为1 至约20个碳原子; R 2各自独立地为氢或1〜约20个碳原子的烃基; M任选是1至约20个碳原子的连接硅原子和L基团的二价烃连接基团; L是共价键合的1至约20个碳原子的烃连接基团或选自-O - ， - S - ， - NR 3 - 的杂原子连接基团，其中R 3是氢或1〜 约20个碳原子; Ra是1〜12个碳原子的烷基; Ar是取代或未取代的芳基; q为1〜4的整数， t和c各自独立地为0或1; 并且x，y和z各自独立地为1〜3的整数，条件是当L为杂原子基团时，t为1。 还提供了制备包含硅烷组合物的硅烷组合物和橡胶组合物的方法。

    Coupling agents for mineral-filled elastomer compositions
    10.
    发明授权
    Coupling agents for mineral-filled elastomer compositions 有权
    矿物填充弹性体组合物的偶联剂

    公开(公告)号：US07531680B2

    公开(公告)日：2009-05-12

    申请号：US11443937

    申请日：2006-05-31

    申请人： Richard W. Cruse ,  Robert J. Pickwell

    发明人： Richard W. Cruse ,  Robert J. Pickwell

    IPC分类号： C07F7/18

    CPC分类号： C08K5/548 ,  C08K5/5419 ,  C08K9/06 ,  C08L21/00

    摘要： A composition of matter is disclosed that comprises at least one silane coupling agent for coupling an elastomer and a filler wherein said silane comprises at least one hydrolysable group that, upon compounding said silane with said elastomer and filler, is released to yield a compound that improves downstream processability of the compounded composition or the properties of the final rubber product or both.

    摘要翻译： 公开了一种物质组合物，其包含用于偶联弹性体和填料的至少一种硅烷偶联剂，其中所述硅烷包含至少一种可水解基团，在将所述硅烷与所述弹性体和填料混合后，其可释放以产生改进的化合物 复合组合物的下游加工性或最终橡胶制品的性能或两者兼有。