摘要:
Disclosed is a method of making m-chlorobenzotrifluoride. Benzotrifluoride is reacted with chlorine gas in the presence of about 0.1 to about 5 mole % (based on benzotrifluoride) of a metal chloride which can be FeCl.sub.3, SbCl.sub.3, or AlCl.sub.3 and about 0.025 to about 5.0 mole % (based on benzotrifluoride) of a catalyst having the formula ##STR1## where Z is halogen, alkyl from C.sub.1 to C.sub.6, alkoxy from C.sub.1 to C.sub.6, or fluoroalkyl from C.sub.1 to C.sub.6, n is 0 to 5, and the molar ratio of metal chloride to cocatalyst is about 0.5 to about 4.
摘要:
Disclosed are bis-meta-benzotrifluoride compounds having the general formula ##STR1## where each A is independently selected from the group consisting of NO.sub.2, NH.sub.2, and NH.sub.3.sup.+ Z.sup.-, Z.sup.- is an anion and B is selected from the group consisting of O, CO, S, SO, and SO.sub.2. The diamine compounds are useful as monomers in making polyimides, polyamide-imides, and polyamides.
摘要:
Disclosed are bis-meta-benzotrifluoride compounds having the general formula ##STR1## where each A is independently selected from the group consisting of NO.sub.2, NH.sub.2, and NH.sub.3.sup.+ Z.sup.-, Z.sup.- is an anion and B is selected from the group consisting of O, CO, S, SO, and SO.sub.2. The diamine compounds are useful as monomers in making polyimides, polyamide-imides, and polyamides.
摘要:
This invention relates to terbium activated silicate luminescent glasses exhibiting reduced afterglow and enhanced luminescence due to incorporation therein of selected rare earth oxides of cerium, europium and godolinium.
摘要:
Disclosed are glycidyl diamines having the formulas ##STR1## where n is 1 or 2, m is 0, 1, or 2, X is Y or ##STR2## and Y is --, O, S, SO, SO.sub.2, CO, C(CH.sub.3).sub.2, or C(CF.sub.3).sub.2. An epoxy resin can be made by mixing the glycidyl diamine with an epoxy curing agent. The epoxy resins can be used as adhesives or to make composites.
摘要:
A process for the production of diaryl ethers which comprises heating, to a temperature of 80.degree. C. to 220.degree. C., a compound of the formula ##STR1## wherein X and Y are selected from the group consisting of H, CN, CO.sub.2 H, CHO, NO.sub.2, and CF.sub.3, provided that both X and Y may not simultaneously be H, in a solvent, in the presence of an inorganic base selected from the group consisting of the alkali metal carbonates, bicarbonates, and hydroxides, and in the presence of a catalyst selected from the group consisting of benzoic acid, substituted benzoic acids, C2-C4 aliphatic carboxylic acids, and alkali metal salts of said acids.
摘要:
Polyimide polymers of the following recurring structure and the corresponding polyamic acids are disclosed: ##STR1## wherein AR.sub.1 is ##STR2## where X is O, S, SO, SO.sub.2, CO, C(CF.sub.3).sub.2, C(CH.sub.3).sub.2, Si(CH.sub.3).sub.2, or a single bond, wherein AR.sub.2 may be pyromellitic dianhydride, a substituted pyromellitic dianhydride, naphthanoic dianhydride, or ##STR3## where Y is O, S, SO, SO.sub.2, CO, C(CF.sub.3).sub.2, C(CH.sub.3).sub.2, Si(CH.sub.3).sub.2 --O--AR--O--, or a single bond, where AR is an aromatic nucleus.
摘要:
This invention relates to novel fluorinated N,N-bis-imides of the formula ##STR1## wherein R is a bivalent radical of the formula ##STR2## The compounds are particularly useful as monomers in the preparation of high performance polymer.
摘要:
In an automated real-time radiographic inspection system for detecting flaws, defects or inhomogeneities in manufactured objects, the objects (10, 11, 12, . . . ) to be tested are moved on a conveyor (20) in succession past an X-ray source (30). Penetrating X-ray radiation is transmitted through the objects (10, 11, 12, . . . ) to cause an image to be formed for each object in succession by an electronic imaging system (40). The imaging system (40) generates digital signals representative of the image for each object, and transmits the digital signals to a data processor/comparator (50). One of the objects (10, 11, 12, . . . ) may be considered as a reference object against which the other objects are compared for structural homogeneity. Thus, the electronic images of the objects (11, 12, . . . ) could be compared with the electronic image of, for example, the object (10). Alternatively, the electronic images of the test objects could be compared with an electronic reference image programmed into the data processor/comparator (50), the programmed reference image. The comparison performed by the data processor/comparator (50) is a subtraction process, which eliminates background features common to test and reference images. Thus, any flaw appearing in a test image, but not present in the reference image, stands out in sharp detail. When a flaw occurs in a test image, the subtractive process results in a non-null signal, which activates a conveyor control mechanism (70) for stopping the conveyor (20) so as to enable rejection of the flawed test object.
摘要:
The present invention, in one form, is a method for generating a calcification score in a CT image data using a scoring algorithm. In accordance with one embodiment of the algorithm, a calcium score is determined by identifying a scorable region in the image data, defining at least one region of interest in the scorable region, and determining a density score. After determining a calcium score for each region of interest, a total calcium score is determined. In addition, to correct for unequal and/or non-contiguous spacing of the slices of image data, a weighted total calcium score is determined.