Method of making m-chlorobenzotrifluoride
    1.
    发明授权
    Method of making m-chlorobenzotrifluoride 失效
    制备间氯三氟甲苯的方法

    公开(公告)号:US5750811A

    公开(公告)日:1998-05-12

    申请号:US835183

    申请日:1997-04-07

    CPC分类号: C07C25/13 C07C17/12

    摘要: Disclosed is a method of making m-chlorobenzotrifluoride. Benzotrifluoride is reacted with chlorine gas in the presence of about 0.1 to about 5 mole % (based on benzotrifluoride) of a metal chloride which can be FeCl.sub.3, SbCl.sub.3, or AlCl.sub.3 and about 0.025 to about 5.0 mole % (based on benzotrifluoride) of a catalyst having the formula ##STR1## where Z is halogen, alkyl from C.sub.1 to C.sub.6, alkoxy from C.sub.1 to C.sub.6, or fluoroalkyl from C.sub.1 to C.sub.6, n is 0 to 5, and the molar ratio of metal chloride to cocatalyst is about 0.5 to about 4.

    摘要翻译: 公开了一种制备间氯三氟甲苯的方法。 在约0.1至约5摩尔%(基于三氟甲苯)的金属氯化物存在下,使三氟甲苯与氯气反应,所述金属氯化物可以是FeCl 3,SbCl 3或AlCl 3,以及约0.025至约5.0摩尔%(基于三氟甲苯) 具有式“IMAGE”的催化剂,其中Z为卤素,C1至C6的烷基,C1至C6的烷氧基,C1至C6的氟代烷基,n为0至5,金属氯化物与助催化剂的摩尔比为约0.5至 约4。

    Polyimides containing fluorine
    7.
    发明授权
    Polyimides containing fluorine 失效
    含氟的聚酰亚胺

    公开(公告)号:US5484879A

    公开(公告)日:1996-01-16

    申请号:US628750

    申请日:1990-12-17

    IPC分类号: C08G73/10 H01B3/30 C08G69/26

    摘要: Polyimide polymers of the following recurring structure and the corresponding polyamic acids are disclosed: ##STR1## wherein AR.sub.1 is ##STR2## where X is O, S, SO, SO.sub.2, CO, C(CF.sub.3).sub.2, C(CH.sub.3).sub.2, Si(CH.sub.3).sub.2, or a single bond, wherein AR.sub.2 may be pyromellitic dianhydride, a substituted pyromellitic dianhydride, naphthanoic dianhydride, or ##STR3## where Y is O, S, SO, SO.sub.2, CO, C(CF.sub.3).sub.2, C(CH.sub.3).sub.2, Si(CH.sub.3).sub.2 --O--AR--O--, or a single bond, where AR is an aromatic nucleus.

    摘要翻译: 公开了以下重复结构的聚酰亚胺聚合物和相应的聚酰胺酸:其中X 1是X,O,S,SO,SO 2,CO,C(CF 3)2,C(CH 3)2,Si (CH 3)2或单键,其中AR 2可以是1,2,4,5-苯四酸二酐,取代的1,2,4,5-苯四酸二酐,萘磺酸二酐或其中Y是O,S,SO,SO 2,CO,C(CF 3)2,C( CH 3)2,Si(CH 3)2 -O-AR-O-或单键,其中AR是芳香核。

    Automated radiographic inspection system
    9.
    发明授权
    Automated radiographic inspection system 失效
    自动射线检查系统

    公开(公告)号:US4415980A

    公开(公告)日:1983-11-15

    申请号:US239611

    申请日:1981-03-02

    摘要: In an automated real-time radiographic inspection system for detecting flaws, defects or inhomogeneities in manufactured objects, the objects (10, 11, 12, . . . ) to be tested are moved on a conveyor (20) in succession past an X-ray source (30). Penetrating X-ray radiation is transmitted through the objects (10, 11, 12, . . . ) to cause an image to be formed for each object in succession by an electronic imaging system (40). The imaging system (40) generates digital signals representative of the image for each object, and transmits the digital signals to a data processor/comparator (50). One of the objects (10, 11, 12, . . . ) may be considered as a reference object against which the other objects are compared for structural homogeneity. Thus, the electronic images of the objects (11, 12, . . . ) could be compared with the electronic image of, for example, the object (10). Alternatively, the electronic images of the test objects could be compared with an electronic reference image programmed into the data processor/comparator (50), the programmed reference image. The comparison performed by the data processor/comparator (50) is a subtraction process, which eliminates background features common to test and reference images. Thus, any flaw appearing in a test image, but not present in the reference image, stands out in sharp detail. When a flaw occurs in a test image, the subtractive process results in a non-null signal, which activates a conveyor control mechanism (70) for stopping the conveyor (20) so as to enable rejection of the flawed test object.

    摘要翻译: 在用于检测制造对象中的瑕疵,缺陷或不均匀性的自动化实时放射线检查系统中,待测试的物体(10,11,12,...)在输送机(20)上依次通过X射线检测器 射线源(30)。 渗透X射线辐射通过物体(10,11,12 ...)传播,以使得由电子成像系统(40)连续地为每个物体形成图像。 成像系统(40)产生表示每个物体的图像的数字信号,并将数字信号发送到数据处理器/比较器(50)。 可以将对象(10,11,12,...)中的一个视为参考对象,为了结构同质性,对象对其进行比较。 因此,可以将对象(11,12,...)的电子图像与例如对象(10)的电子图像进行比较。 或者,可以将测试对象的电子图像与编程到数据处理器/比较器(50),编程参考图像中的电子参考图像进行比较。 由数据处理器/比较器(50)进行的比较是减法处理,其消除了测试和参考图像共同的背景特征。 因此,出现在测试图像中但是不存在于参考图像中的任何缺陷都是非常详细的。 当在测试图像中发生缺陷时,减法处理产生非空信号,其激活用于停止输送机(20)的输送机控制机构(70),以便能够排除有缺陷的测试对象。

    Methods and apparatus for calcification scoring
    10.
    发明授权
    Methods and apparatus for calcification scoring 失效
    钙化评分方法和装置

    公开(公告)号:US06233304B1

    公开(公告)日:2001-05-15

    申请号:US09199513

    申请日:1998-11-25

    IPC分类号: A61B603

    CPC分类号: G06T7/0012

    摘要: The present invention, in one form, is a method for generating a calcification score in a CT image data using a scoring algorithm. In accordance with one embodiment of the algorithm, a calcium score is determined by identifying a scorable region in the image data, defining at least one region of interest in the scorable region, and determining a density score. After determining a calcium score for each region of interest, a total calcium score is determined. In addition, to correct for unequal and/or non-contiguous spacing of the slices of image data, a weighted total calcium score is determined.

    摘要翻译: 本发明以一种形式是使用评分算法在CT图像数据中产生钙化积分的方法。 根据算法的一个实施例,通过识别图像数据中的可划分区域来确定钙分数,在可划分区域中限定至少一个感兴趣区域,以及确定密度分数。 在确定每个感兴趣区域的钙分数后,确定总钙分数。 另外,为了校正图像数据片段的不等的和/或不连续的间隔,确定加权总钙分数。