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    Process for preparing aminopolycarboxylates proceeding from amino acids
    1.
    发明授权
    Process for preparing aminopolycarboxylates proceeding from amino acids 失效
    由氨基酸制备氨基多羧酸盐的方法

    公开(公告)号：US08785685B2

    公开(公告)日：2014-07-22

    申请号：US13430105

    申请日：2012-03-26

    申请人： Robert Baumann ,  Markus Christian Biel ,  Axel Franzke ,  Thomas Heidenfelder ,  Paul Klingelhoefer ,  Alfred Oftring

    发明人： Robert Baumann ,  Markus Christian Biel ,  Axel Franzke ,  Thomas Heidenfelder ,  Paul Klingelhoefer ,  Alfred Oftring

    IPC分类号： C07C227/18 ,  C07C227/02

    CPC分类号： C07C227/18 ,  C07C227/02 ,  C07C227/12 ,  C07C229/16 ,  C07C229/12

    摘要： The present invention relates to a process for preparing aminopolycarboxylates proceeding from an amino acid which, in a first process step is reacted with ethylene oxide to give an intermediate mixture comprising the corresponding dialkanolamine, and then the intermediate mixture, in a second process step is converted catalytically using a base to the corresponding aminopolycarboxylate, wherein the amino acid, before the reaction with ethylene oxide in the first process step, is supplied to a partial neutralization with 0.70 to 0.99 equivalent of base per acid group, or, in the first process step, an amino acid which has already been partly neutralized with 0.70 to 0.99 equivalent of base per acid group is used.

    摘要翻译： 本发明涉及从氨基酸制备氨基多羧酸盐的方法，该方法在第一工艺步骤与环氧乙烷反应得到包含相应的二链烷醇胺的中间体混合物，然后在第二工艺步骤中将中间体混合物转化 催化地将碱用于相应的氨基多羧酸盐，其中在与第一工艺步骤中的环氧乙烷反应之前，将氨基酸以0.70-0.99当量的碱/酸组供应至部分中和，或者在第一工艺步骤 使用已经用0.70〜0.99当量碱的每个酸基部分中和的氨基酸。

    PROCESS FOR PREPARING AMINOPOLYCARBOXYLATES PROCEEDING FROM AMINO ACIDS
    2.
    发明申请
    PROCESS FOR PREPARING AMINOPOLYCARBOXYLATES PROCEEDING FROM AMINO ACIDS 失效
    用于制备从氨基酸处理的氨基羟基羧酸酯的方法

    公开(公告)号：US20120264973A1

    公开(公告)日：2012-10-18

    申请号：US13430105

    申请日：2012-03-26

    申请人： Robert Baumann ,  Markus Christian Biel ,  Axel Franzke ,  Thomas Heidenfelder ,  Paul Klingelhoefer ,  Alfred Oftring

    发明人： Robert Baumann ,  Markus Christian Biel ,  Axel Franzke ,  Thomas Heidenfelder ,  Paul Klingelhoefer ,  Alfred Oftring

    IPC分类号： C07C227/18

    CPC分类号： C07C227/18 ,  C07C227/02 ,  C07C227/12 ,  C07C229/16 ,  C07C229/12

    摘要： The present invention relates to a process for preparing aminopolycarboxylates proceeding from an amino acid which, in a first process step is reacted with ethylene oxide to give an intermediate mixture comprising the corresponding dialkanolamine, and then the intermediate mixture, in a second process step is converted catalytically using a base to the corresponding aminopolycarboxylate, wherein the amino acid, before the reaction with ethylene oxide in the first process step, is supplied to a partial neutralization with 0.70 to 0.99 equivalent of base per acid group, or, in the first process step, an amino acid which has already been partly neutralized with 0.70 to 0.99 equivalent of base per acid group is used.

    摘要翻译： 本发明涉及从氨基酸制备氨基多羧酸盐的方法，该方法在第一工艺步骤与环氧乙烷反应得到包含相应的二链烷醇胺的中间体混合物，然后在第二工艺步骤中将中间体混合物转化 催化地将碱用于相应的氨基多羧酸盐，其中在与第一工艺步骤中的环氧乙烷反应之前，将氨基酸以0.70-0.99当量的碱/酸组供应至部分中和，或者在第一工艺步骤 使用已经用0.70〜0.99当量碱的每个酸基部分中和的氨基酸。

    PROCESS FOR PREPARING AMINOPOLYCARBOXYLATES
    6.
    发明申请
    PROCESS FOR PREPARING AMINOPOLYCARBOXYLATES 有权
    制备氨基羟基羧酸酯的方法

    公开(公告)号：US20120302783A1

    公开(公告)日：2012-11-29

    申请号：US13437093

    申请日：2012-04-02

    申请人： Robert BAUMANN ,  Markus Christian Biel ,  Axel Franzke ,  Alfred Oftring ,  Friedhelm Teich ,  Paul Klingelhoefer ,  Marie Katrin Schröter

    发明人： Robert BAUMANN ,  Markus Christian Biel ,  Axel Franzke ,  Alfred Oftring ,  Friedhelm Teich ,  Paul Klingelhoefer ,  Marie Katrin Schröter

    IPC分类号： C07C227/02

    CPC分类号： C07C227/02

    摘要： What is proposed is a process for preparing aminopolycarboxylates proceeding from the corresponding polyalkanolamines by oxidative dehydrogenation in the presence of a catalyst comprising 1 to 90% by weight of copper, based on the total weight of the catalyst, using a base, which comprises first performing a partial conversion of the polyalkanolamine to a reaction mixture comprising the aminopolycarboxylate at a temperature in the range from 140 to 180° C. until at least 10 to 90 mol % of the polyalkanolamine has been depleted, and then continuing the conversion at elevated temperature.

    摘要翻译： 提出的是一种制备在相应的聚链烷醇胺上通过氧化脱氢在催化剂存在下进行的氨基多羧酸盐的方法，所述催化剂包含1至90重量％的铜，基于催化剂的总重量，使用碱，其包括首先进行 在140〜180℃的温度范围内将聚链烷醇胺部分转化成含有氨基多羧酸盐的反应混合物，直到聚链烷醇胺的至少10〜90摩尔％已经耗尽，然后在升高的温度下继续转化。