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    Process for upgrading fischer-tropsch syncrude using thermal cracking and oligomerization
    2.
    发明授权
    Process for upgrading fischer-tropsch syncrude using thermal cracking and oligomerization 失效
    使用热裂解和低聚提升费 - 托合成原料的方法

    公开(公告)号：US06703535B2

    公开(公告)日：2004-03-09

    申请号：US10125879

    申请日：2002-04-18

    申请人： David R. Johnson ,  Christopher A. Simmons ,  Donald H. Mohr ,  Stephen J. Miller ,  Stephen K. Lee ,  William L. Schinski ,  Michael S. Driver ,  William J. Cannella

    发明人： David R. Johnson ,  Christopher A. Simmons ,  Donald H. Mohr ,  Stephen J. Miller ,  Stephen K. Lee ,  William L. Schinski ,  Michael S. Driver ,  William J. Cannella

    IPC分类号： C07C204

    CPC分类号： C10G2/32 ,  Y10S208/95

    摘要： A process for upgrading a Fischer-Tropsch feedstock which comprises (a) recovering from a Fischer-Tropsch reactor a Fischer-Tropsch wax fraction and a Fischer-Tropsch condensate fraction, wherein the Fischer-Tropsch condensate fraction contains alcohols boiling below about 370° C.; (b) contacting the Fischer-Tropsch condensate fraction with a dehydration catalyst in a dehydration zone under dehydration conditions pre-selected to convert at least some of the alcohols present in said fraction into olefins and recovering a first intermediate effluent from said dehydration zone; (c) pyrolyzing the paraffins in the Fischer-Tropsch wax fraction in a thermal cracking zone under thermal cracking conditions pre-selected to crack the Fischer-Tropsch wax molecules to form olefins and collecting a second intermediate effluent from the thermal cracking zone; (d) passing the first and second intermediate effluents recovered from steps (b) and (c) to an oligomerization zone containing an oligomerization catalyst under oligomerization conditions to form an oligomerization mixture having a higher molecular weight than either of said first and second intermediate effluent; (e) hydrofinishing the oligomerization mixture in a hydrofinishing zone; and (f) recovering from the hydrofinishing zone a C10 plus hydrocarbon product, most preferably a lubricating base oil.

    摘要翻译： 一种用于升级费 - 托原料的方法，其包括（a）从费 - 托反应器中回收费 - 托蜡馏分和费 - 托冷凝馏分，其中所述费 - 托冷凝馏分含有沸点低于约370℃的醇 。 （b）在脱水条件下，将脱水催化剂与脱水催化剂接触，预先将所述馏分中存在的至少一些醇转化成烯烃并从所述脱水区回收第一中间体流出物; （c）在热裂解条件下，在热裂解条件下热分解费 - 托蜡馏分中的链烷烃，预热裂解条件以裂解费 - 托蜡分子以形成烯烃并从热裂解区收集第二中间体流出物; （d）在低聚条件下将从步骤（b）和（c）回收的第一和第二中间流出物通入含有低聚催化剂的低聚区以形成具有比所述第一和第二中间流出物 ; （e）在加氢精制区中加氢精制低聚混合物; 和（f）从加氢精制区回收C10加烃产物，最优选润滑基础油。

    Process to make base oil from thermally cracked waxy feed using ionic liquid catalyst
    5.
    发明授权
    Process to make base oil from thermally cracked waxy feed using ionic liquid catalyst 有权
    使用离子液体催化剂从热裂解蜡质进料制备基础油的方法

    公开(公告)号：US07723556B2

    公开(公告)日：2010-05-25

    申请号：US12498254

    申请日：2009-07-06

    申请人： Saleh Elomari ,  Russell R. Krug ,  Stephen J. Miller

    发明人： Saleh Elomari ,  Russell R. Krug ,  Stephen J. Miller

    IPC分类号： C07C2/68 ,  C07C2/70 ,  C07C2/60

    CPC分类号： C10G50/02 ,  C07C2527/125 ,  C07C2531/02 ,  C10G2400/10 ,  C10M105/04 ,  C10M109/02 ,  C10M127/02 ,  C10M177/00 ,  C10M2205/0285 ,  C10N2220/022 ,  C10N2220/023 ,  C10N2230/02 ,  C10N2270/00 ,  C10M2203/0206

    摘要： We provide a process for making a base oil, comprising: a) selecting an olefin feed produced by thermal cracking of a waxy feed; b) oligomerizing the olefin feed in an ionic liquid oligomerization zone at a set of oligomerization conditions to form an oligomer; and c) alkylating the oligomer in the presence of an isoparaffin, in an ionic liquid alkylation zone, at a set of alkylation conditions to form an alkylated oligomeric product having a kinematic viscosity at 100° C. of 6.9 mm2/s or greater, a VI of at least 134, and a Bromine Number of less than 4. We provide a process to make base oil from an olefin feed produced in a FCC unit. We also provide a process to make two or more viscosity grades of base oil from an olefin feed produced by thermal cracking of a waxy feed.

    摘要翻译： 我们提供一种制备基础油的方法，包括：a）选择通过蜡质进料的热裂解产生的烯烃原料; b）在一组低聚条件下使离子液体低聚区中的烯烃进料低聚以形成低聚物; 和c）在异烷烃存在下，在离子液体烷基化区中，在一组烷基化条件下烷基化低聚物以形成在100℃下的运动粘度为6.9mm 2 / s或更大的烷基化低聚产物， VI至少为134，溴值小于4.我们提供了一种从FCC装置中生产的烯烃原料制备基础油的方法。 我们还提供一种通过蜡质进料的热裂解产生的烯烃原料制备两种或更多种粘度等级的基础油的方法。

    Process for producing a highly paraffinic diesel fuel having a high iso-paraffin to normal paraffin mole ratio
    7.
    发明授权
    Process for producing a highly paraffinic diesel fuel having a high iso-paraffin to normal paraffin mole ratio 失效
    具有高异链烷烃与正常石蜡摩尔比的高度链烷烃类柴油燃料的方法

    公开(公告)号：US06723889B2

    公开(公告)日：2004-04-20

    申请号：US09765585

    申请日：2001-01-22

    申请人： Stephen J. Miller ,  Arthur John Dahlberg ,  Kamala R. Krishna ,  Russell R. Krug

    发明人： Stephen J. Miller ,  Arthur John Dahlberg ,  Kamala R. Krishna ,  Russell R. Krug

    IPC分类号： C07C522

    CPC分类号： C10L1/08 ,  C10G2400/04 ,  Y10S208/95

    摘要： A process for producing a diesel fuel having at least 70% C10+ paraffins, wherein the iso-paraffin to normal paraffin mole ratio is 5:1 and higher. This diesel fuel is produced by from a feed containing at least 40% C10+ normal paraffins and at least 20% C26+ normal paraffins. It is produced by contacting that feed in an isomerization/cracking reaction zone a feed with a catalyst comprising a SAPO-11 and platinum in the presence of hydrogen (hydrogen:feed ratio of from 1,000 to 10,000 SCFB) at a temperature of from 340° C. to 420° C., a pressure of from 100 psig to 600 psig, and a liquid hourly space velocity of from 0.1 hr−1 to 1.0 hr−1.

    摘要翻译： 一种制备具有至少70％的C 10 +烷烃的柴油的方法，其中异链烷烃与正常的石蜡摩尔比为5:1以上。 该柴油由含有至少40％C 10 +正链烷烃和至少20％C26 +正链烷烃的原料生产。 通过在异构化/裂化反应区中将进料与含有SAPO-11和铂的催化剂在氢气存在下（氢气：进料比为1,000至10,000SCFB），使该进料在340℃的温度下接触而制备 至420℃，压力为100psig至600psig，液时空速为0.1小时-1.0小时-1。

    Process for making a lube base stock from a lower molecular weight feedstock using at least two oligomerization zones
    9.
    发明授权
    Process for making a lube base stock from a lower molecular weight feedstock using at least two oligomerization zones 失效
    使用至少两个低聚区从较低分子量原料制备润滑油基础油料的方法

    公开(公告)号：US06686511B2

    公开(公告)日：2004-02-03

    申请号：US09758897

    申请日：2001-01-11

    申请人： Stephen J. Miller ,  Dennis J. O'Rear ,  Thomas V. Harris ,  Russell R. Krug

    发明人： Stephen J. Miller ,  Dennis J. O'Rear ,  Thomas V. Harris ,  Russell R. Krug

    IPC分类号： C07C212

    CPC分类号： C10M177/00 ,  C10G50/02 ,  C10G57/02 ,  C10M107/10 ,  C10N2270/00 ,  Y10S208/95

    摘要： A process for making a lube base stock wherein an olefinic feedstock is separated into a light olefin fraction and a medium olefin fraction. The light olefin fraction is contacted with a first oligomerization catalyst in a first oligomerization zone to produce a first product. Both the medium olefin fraction and the first product are contacted with a second oligomerization catalyst in a second oligomerization zone to produce a second product. The second product is separated into a light byproduct fraction and a heavy product fraction that includes hydrocarbons in the lube base stock range.

    摘要翻译： 一种制备润滑油基料的方法，其中将烯烃原料分离成轻质烯烃馏分和中等烯烃馏分。 在第一低聚区中轻链烯烃部分与第一低聚催化剂接触以产生第一产物。 中间烯烃部分和第一产物都在第二低聚区中与第二低聚催化剂接触以产生第二产物。 将第二产物分离成轻质副产物馏分和在润滑油基料范围内包含烃的重质产物馏分。

    PRODUCTION OF HIGH QUALITY LUBRICANT BRIGHT STOCK
    10.
    发明申请
    PRODUCTION OF HIGH QUALITY LUBRICANT BRIGHT STOCK 有权
    生产高品质润滑剂亮度库存

    公开(公告)号：US20090120838A1

    公开(公告)日：2009-05-14

    申请号：US12191716

    申请日：2008-08-14

    申请人： Stephen J. Miller ,  Russell R. Krug

    发明人： Stephen J. Miller ,  Russell R. Krug

    IPC分类号： C10G69/02

    CPC分类号： C10G65/12 ,  C10M101/02 ,  C10M2203/1085 ,  C10N2230/02 ,  C10N2230/10

    摘要： A process for producing a lubricant bright stock from a very heavy feed obtained from a petroleum crude is disclosed. The bright stock produced by the present process has a reduced cloud point and better oxidation stability relative to bright stocks prepared by conventional methods. The process comprises the steps of providing a petroleum residuum-derived stream; separating the residuum-derived stream at a distillation cut point in the range of 1150° F. to 1300° F., into a heavy fraction and at least one light fraction; hydrocracking the at least one light fraction under conditions to reduce the concentration of sulfur and nitrogen to suitable levels for hydroisomerization dewaxing; and dewaxing at least a portion of the hydrocracked stream under hydroisomerization conditions to produce a lubricant bright stock.

    摘要翻译： 公开了从由石油原油获得的非常重的原料生产润滑剂光亮原料的方法。 本方法生产的光亮料相对于通过常规方法制备的光亮油墨具有降低的浊点和更好的氧化稳定性。 该方法包括以下步骤：提供来自石油残渣的流; 将在1150°F至1300°F范围内的蒸馏切割点的残渣衍生物流分离成重馏分和至少一种轻馏分; 在将硫和氮的浓度降低到加氢异构化脱蜡的合适水平的条件下加氢裂化至少一种轻馏分; 并在加氢异构化条件下将至少一部分加氢裂化物流脱蜡以产生润滑剂光亮原料。