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    Methods and compositions for stabilizing catalytic processes
    2.
    发明授权
    Methods and compositions for stabilizing catalytic processes 有权

    公开(公告)号：US08187994B2

    公开(公告)日：2012-05-29

    申请号：US12611714

    申请日：2009-11-03

    申请人： Thomas V. Harris

    发明人： Thomas V. Harris

    IPC分类号： B01J31/06

    CPC分类号： B01J31/40 ,  B01J31/0278 ,  B01J31/0284

    摘要： Methods and compositions for stabilizing the activity of catalytic compositions during catalytic processes, such as alkylation. A catalytic composition comprising a partially deactivated ionic liquid catalyst may be regenerated by reaction with a metal to form reactivated catalyst and an inorganic catalyst precursor; and the catalytic composition may be amended in-process by addition of an organic catalyst precursor for reaction with the inorganic catalyst precursor to form fresh ionic liquid catalyst. The organic catalyst precursor may be protected from water, e.g., during handling, by hydrophobic material(s).

    Regeneration of ionic liquid catalyst using a regeneration metal in the presence of added hydrogen
    3.
    发明授权
    Regeneration of ionic liquid catalyst using a regeneration metal in the presence of added hydrogen 有权
    在加入氢气存在下使用再生金属再生离子液体催化剂

    公开(公告)号：US07825055B2

    公开(公告)日：2010-11-02

    申请号：US11408335

    申请日：2006-04-21

    申请人： Saleh Elomari ,  Thomas V. Harris

    发明人： Saleh Elomari ,  Thomas V. Harris

    IPC分类号： B01J38/60

    CPC分类号： B01J38/10 ,  B01J31/0239 ,  B01J31/0284 ,  B01J31/0288 ,  B01J31/40 ,  B01J38/58 ,  B01J2231/4205

    摘要： A process for regenerating a used acidic ionic liquid catalyst comprising contacting the used ionic liquid catalyst with at least one ‘regeneration’ metal in a regeneration zone in the presence of added hydrogen under regeneration conditions for a time sufficient to increase the activity of the ionic liquid catalyst is described. In one embodiment, regeneration is conducted in the presence of a hydrocarbon solvent.

    摘要翻译： 一种用于再生所用酸性离子液体催化剂的方法，包括在再生条件下，在加入的氢气存在下，将所用离子液体催化剂与再生区中的至少一种“再生”金属接触一段足以提高离子液体活性的时间 催化剂。 在一个实施方案中，在烃溶剂存在下进行再生。

    REGENERATION OF IONIC LIQUID CATALYST AND RECOVERY OF AN OIL
    5.
    发明申请
    REGENERATION OF IONIC LIQUID CATALYST AND RECOVERY OF AN OIL 有权
    离子液体催化剂的再生和油的回收

    公开(公告)号：US20100234208A1

    公开(公告)日：2010-09-16

    申请号：US12705943

    申请日：2010-02-15

    申请人： Thomas V. Harris ,  Saleh Elomari

    发明人： Thomas V. Harris ,  Saleh Elomari

    IPC分类号： B01J38/48

    CPC分类号： B01J27/125 ,  B01J27/32 ,  B01J31/0239 ,  B01J31/0268 ,  B01J31/0284 ,  B01J31/0288 ,  B01J31/1616 ,  B01J31/26 ,  B01J31/40 ,  B01J38/10 ,  B01J2231/64 ,  C07C2/862 ,  Y02P20/584

    摘要： A process for regenerating a used acidic ionic liquid catalyst, comprising: a. contacting the catalyst and hydrogen with a supported hydrogenation catalyst under hydrogenation conditions; and b. recovering a conjunct polymer that is a clear and colorless oil from the catalyst. A process for regenerating a used acidic ionic liquid catalyst which has been deactivated by conjunct polymers comprising the steps of contacting the used catalyst and hydrogen with a supported hydrogenation catalyst in a reaction zone under hydrogenation conditions in the presence of an inert hydrocarbon in which saturated conjunct polymers are soluble for a time sufficient to hydrogenate at least a portion of the conjunct polymers; and recovering the saturated conjunct polymers. Also, a process comprising: contacting the used acidic ionic liquid catalyst and hydrogen with a hydrogenation catalyst comprising a hydrogenation component under hydrogenation conditions; and recovering a conjunct polymer that is a clear and colorless oil.

    摘要翻译： 一种再生使用的酸性离子液体催化剂的方法，包括：a。 在氢化条件下使催化剂和氢与负载的氢化催化剂接触; 和b。 从催化剂中回收一种透明无色油的结合聚合物。 一种已经被结合聚合物失活的已使用的酸性离子液体催化剂的方法，包括以下步骤：在氢化条件下，在惰性烃存在下，使反应区中的所用催化剂和氢与负载氢化催化剂接触，其中饱和连接 聚合物可溶解足以氢化至少一部分结合聚合物的时间; 并回收饱和的结合聚合物。 而且，一种方法包括：在氢化条件下使用酸性离子液体催化剂和氢气与包含氢化组分的氢化催化剂接触; 并回收澄清无色油的结合聚合物。

    Ionic liquid catalyst having enhanced activity
    8.
    发明授权
    Ionic liquid catalyst having enhanced activity 有权
    具有增强活性的离子液体催化剂

    公开(公告)号：US07666811B2

    公开(公告)日：2010-02-23

    申请号：US11315750

    申请日：2005-12-20

    申请人： Saleh Elomari ,  Thomas V. Harris

    发明人： Saleh Elomari ,  Thomas V. Harris

    IPC分类号： B01J31/00 ,  B01J27/135

    CPC分类号： C07D213/20 ,  B01J27/125 ,  B01J27/32 ,  B01J31/0278 ,  B01J31/0284 ,  B01J31/0288 ,  B01J31/40 ,  C07C2/62 ,  C07C2531/02 ,  Y02P20/584 ,  C07C9/16

    摘要： A process for producing acidic ionic liquid catalyst having enhanced activity comprising combining fresh acidic ionic liquid catalyst, a metal and a Broensted acid in a reaction zone for a time sufficient to increase the activity of the ionic liquid catalyst is disclosed.A process for producing acidic ionic liquid catalyst having enhanced activity comprising the steps of combining fresh ionic liquid catalyst, a metal and HCl in a reaction zone for a time sufficient to increase the activity of the fresh ionic liquid catalyst; removing reaction product from the reaction zone and recovering at least a portion of the treated ionic liquid catalyst is also disclosed.

    摘要翻译： 公开了一种生产具有增强活性的酸性离子液体催化剂的方法，其包括在反应区中将新鲜的酸性离子液体催化剂，金属和布朗斯台德酸组合足以提高离子液体催化剂活性的时间。 一种生产具有增强活性的酸性离子液体催化剂的方法，包括以下步骤：将新鲜离子液体催化剂，金属和HCl在反应区中混合足以增加新鲜离子液体催化剂活性的时间; 从反应区除去反应产物并回收至少一部分经处理的离子液体催化剂。