Process for producing carbonic acid ester
    1.
    发明授权
    Process for producing carbonic acid ester 失效
    生产碳酸酯的方法

    公开(公告)号:US5258541A

    公开(公告)日:1993-11-02

    申请号:US844982

    申请日:1992-02-27

    IPC分类号: C07C68/00 C07C69/96

    CPC分类号: C07C68/005

    摘要: A carbonic acid ester is produced by reacting an alcohol with carbon monoxide and oxygen in the presence of a catalyst comprising a cupric salt of a weak acid and/or a cupric halide and an alkaline earth metal salt of a weak acid and/or an alkaline earth metal halide.

    摘要翻译: 在含有弱酸和/或二卤化铜的铜盐和弱酸和/或碱的碱土金属盐的催化剂存在下,使醇与一氧化碳和氧气反应制备碳酸酯 地球金属卤化物。

    PHOTOSENSITIVE COMPOSITION FOR VOLUME HOLOGRAM RECORDING AND PRODUCING METHOD THEREOF
    3.
    发明申请
    PHOTOSENSITIVE COMPOSITION FOR VOLUME HOLOGRAM RECORDING AND PRODUCING METHOD THEREOF 审中-公开
    用于体积霍乱记录的感光性组合物及其制备方法

    公开(公告)号:US20110200918A1

    公开(公告)日:2011-08-18

    申请号:US13124813

    申请日:2009-10-28

    IPC分类号: G03F7/00

    摘要: A photosensitive composition (I) for volume hologram recording includes a binder polymer (A), a photo-induced cationically polymerizable compound (B), a photoinitiator (C), and a sensitizing dye (D), in which the binder polymer (A) is a polymer containing naphthalene rings and having a weight-average molecular weight of 1×104 to 100×104. A method produces a photosensitive composition (II) for volume hologram recording by mixing a binder polymer (A′), a photo-induced cationically polymerizable compound (B′), a photoinitiator (C′), and a sensitizing dye (D′), in which the photo-induced cationically polymerizable compound (B′) has been subjected to a heating treatment at a temperature equal to or lower than the boiling point of the compound (B′).

    摘要翻译: 用于体积全息记录的光敏组合物(I)包括粘合剂聚合物(A),光引发性阳离子聚合性化合物(B),光引发剂(C)和增感染料(D)),其中粘合剂聚合物 )是含有萘环的聚合物,其重均分子量为1×104〜100×104。 通过混合粘合剂聚合物(A'),光引发的可阳离子聚合的化合物(B'),光引发剂(C')和敏化染料(D'),通过混合生产用于体积全息图记录的光敏组合物(II) 其中光诱导的可阳离子聚合的化合物(B')已经在等于或低于化合物(B')的沸点的温度下进行加热处理。

    Colored photosensitive composition for color filter, color filter, and process for the production thereof

    公开(公告)号:US20060257759A1

    公开(公告)日:2006-11-16

    申请号:US10536389

    申请日:2003-11-28

    IPC分类号: G02B5/20

    摘要: The present invention relates to: a colored photosensitive composition for a color filter; a color filter obtained by curing the colored photosensitive composition; and a method of producing a color filter. The colored photosensitive composition is characterized by including: a polyether compound represented by the following formula (4), having multiple polymerizable unsaturated groups and one or more acid groups in one molecule; a coloring matter; and a curable resin and/or an ethylenically unsaturated compound to be optionally added. In the formula (4), R′ represents a residue —RHm-1 of an organic compound RHm containing “m” pieces of active hydrogen atoms in one molecule, or a group derived from the residue; R represents a residue obtained by removing an active hydrogen atom from an organic compound having the active hydrogen atom; “m” represents an integer of 1 to 30; R4 to R13 each represent a hydrogen atom, a hydrocarbon group having 1 to 10 carbon atoms, or a hydrocarbon group having 1 to 10 carbon atoms and an unsaturated group, provided that the unsaturated group contains —OCO—CR3═CR1R2, R1 and R2 each represent a hydrogen atom, R3 represents a hydrogen atom or a hydrocarbon group having 1 to 10 carbon atoms, and at least one of R4 to R13 represents a hydrocarbon group having 1 to 10 carbon atoms and the unsaturated group; R15 represents a residue of a polybasic acid anhydride; X represents —COOH, —OPO(OH)a(OR)b, or —OSO3R (provided that R represents a hydrogen atom, a methyl group, or an ethyl group, “a” represents 1 or 0, and “a+b”=2); “n” represents an integer of 1 or more, and the number of structural units in the entire molecule represented by n is in the range of 2 to 50; and “p” represents 0 when X represents —OPO(OH)a(OR)b or —OSO3R, while “p” represents an integer of 1 or more when X represents —COOH. The method of producing a color filter is characterized by including the steps of: applying the colored photosensitive composition onto a substrate; subjecting the colored photosensitive composition applied onto the substrate to pattern exposure to photo-cure the colored photosensitive composition in an exposed portion; and developing the colored photosensitive composition subjected to the pattern exposure to leave a pattern-like colored layer obtained by photo-curing the colored photosensitive composition on the substrate. As a result, a colored photosensitive composition for a color filter having high developability and high photosensitivity with a diluted alkali and suitable for image-forming applications such as a pigment-dispersed resist, a color filter obtained by curing the composition, and a color filter are obtained.

    High purity 1,3-propanediol derivative solvent, process for producing the same, and use thereof
    5.
    发明授权
    High purity 1,3-propanediol derivative solvent, process for producing the same, and use thereof 失效
    高纯度1,3-丙二醇衍生物溶剂及其制备方法及其用途

    公开(公告)号:US06610638B1

    公开(公告)日:2003-08-26

    申请号:US09701663

    申请日:2000-11-30

    IPC分类号: C07C4500

    摘要: The present invention No. I is to obtain a high purity 3-alkoxy-1-propanol having the content of alcoholic impurities of not more than 0.3% by weight by allowing to react acrolein with a linear or branched alcohol having a carbon number of 1-4 using acrolein having the content of propionaldehyde of not more than 1% by weight as a raw material, a 3-alkoxy-1-propanol is produced by a hydrogenation reaction using hydrogen of a reaction mass under the presence of a catalyst, followed by recovering through a distillation of the 3-alkoxy-1-propanol having the content of alcoholic impurities of not more than 0.3% by weight from a crude solution in the hydrogenation reaction.

    摘要翻译: 本发明No.1是通过使丙烯醛与碳数为1的直链或支链醇反应,得到醇含量不超过0.3重量%的高纯度3-烷氧基-1-丙醇 -4使用丙醛含量不超过1重量%的丙烯醛作为原料,通过在催化剂存在下使用反应物料的氢气进行氢化反应制备3-烷氧基-1-丙醇,随后 通过在氢化反应中从粗溶液中蒸馏出醇含量不超过0.3重量%的3-烷氧基-1-丙醇。

    Curable resin composition for nanoimprint
    6.
    发明授权
    Curable resin composition for nanoimprint 失效
    用于纳米压印的可固化树脂组合物

    公开(公告)号:US08530539B2

    公开(公告)日:2013-09-10

    申请号:US12866398

    申请日:2009-01-08

    IPC分类号: C08F2/46 C08J3/28

    摘要: Disclosed is a photocurable resin composition for nanoimprint, containing a curable monomer component with or without a binder resin. The composition further contains 0.001 to 5 parts by weight of a compound having a reactive functional group and a hydrophobic functional group in the same molecular skeleton, per 100 parts by weight of the total amount of the curable monomer component and binder resin. Preferably, the reactive functional group is at least one functional group selected from the group consisting of hydroxyl groups, epoxy groups, vinyl ether groups, oxetanyl groups, alkoxysilane groups, and free-radically polymerizable vinyl groups, and the hydrophobic functional group is at least one functional group selected from the group consisting of fluorine-containing groups, alkylsilane groups, alicyclic hydrocarbon groups, and aliphatic hydrocarbon groups having 4 or more carbon atoms.

    摘要翻译: 公开了一种用于纳米压印的光固化树脂组合物,其含有具有或不具有粘合剂树脂的可固化单体组分。 该组合物相对于固化性单体成分和粘合剂树脂的总量相对于100重量份还含有0.001〜5重量份的具有相同分子骨架的反应性官能团和疏水性官能团的化合物。 反应性官能团优选为选自羟基,环氧基,乙烯基醚基,氧杂环丁烷基,烷氧基硅烷基和自由基聚合性乙烯基中的至少一种官能团,疏水官能团为至少 一个选自含氟基团,烷基硅烷基团,脂环族烃基和具有4个或更多个碳原子的脂族烃基的官能团。

    Vinyl ether compounds and polymerizable compositions
    8.
    发明授权
    Vinyl ether compounds and polymerizable compositions 失效
    乙烯基醚化合物和可聚合组合物

    公开(公告)号:US07985866B2

    公开(公告)日:2011-07-26

    申请号:US12076625

    申请日:2008-03-20

    IPC分类号: C07D305/14 C07D305/00

    摘要: Disclosed is an oxetane-containing vinyl ether compound including one or more aromatic or non-aromatic carbocycles and/or two or more vinyl ether structures, such as a compound of Formula: wherein Ring Z1 is non-aromatic carbocycle; Ra is vinyl group of Formula: wherein each of R1, R2, and R3 is hydrogen or C1-C4 alkyl; Wa is single bond or organic group having a valence of (m+1); X1 is, for example, hydrocarbon; “m” and “q” are each 1 or 2; and “p” is 0 to 5. Also disclosed is an alicyclic epoxy-containing vinyl ether compound of Formula: wherein Ring Z2 is non-aromatic carbocycle; Rb is vinyl group of Formula: wherein R4, R5 and R6 are each hydrogen or C1-C4 alkyl; Wb is single bond or organic group having a valence of (r+1); Rc and Rd are hydrogen or alkyl; and “r” and “s” are 1 or 2.

    摘要翻译: 公开了包含一种或多种芳族或非芳族碳环和/或两个或多个乙烯基醚结构的含氧杂环丁烷的乙烯基醚化合物,例如下式的化合物:其中环Z1是非芳族碳环; Ra是式的乙烯基:其中R 1,R 2和R 3各自是氢或C 1 -C 4烷基; Wa是单键或化合价(m + 1)的有机基团; X1是例如烃; “m”和“q”分别为1或2; 并且“p”为0至5.还公开了下式的脂环族环氧基乙烯基醚化合物:其中环Z2是非芳族碳环; Rb是式的乙烯基:其中R 4,R 5和R 6各自为氢或C 1 -C 4烷基; Wb是单键或化合价(r + 1)的有机基团; Rc和R d是氢或烷基; “r”和“s”为1或2。

    Compounds, polymers of them, processes for the preparation of both, and
compositions containing the compounds
    9.
    发明授权
    Compounds, polymers of them, processes for the preparation of both, and compositions containing the compounds 失效
    它们的化合物,聚合物,二者的制备方法和含有该化合物的组合物

    公开(公告)号:US6063898A

    公开(公告)日:2000-05-16

    申请号:US125161

    申请日:1998-08-13

    摘要: The first aspect of the invention provides a novel compound containing a reactive functional group represented by formula (1)R.sup.2 --O--CO--NH--CH.dbd.CH--R.sup.1 (1)wherein R.sup.1 represents a hydrogen atom, an aromatic hydrocarbon group, or a saturated or unsaturated aliphatic hydrocarbon group, R.sup.2 represents a formula comprising alicyclic functionality.The second aspect provides an active energy ray-curable unsaturated resin composition prepared by mixing a reaction product of the above-mentioned compound (1) with an unsaturated resin containing an acid group and with a diluent. The composition can be cured by active energy rays, and it can be used as an alkali developable and active energy ray-curable type resist resin composition.The third aspect provides an active energy ray-polymerizable unsaturated resin composition obtainable by allowing to react an unsaturated compound (E) containing an alicyclic epoxy group represented by formula (1) with a colloidal silica (F) in the presence of a metal chelate and/or metal alkoxide (G). A powder-state active energy ray-polymerizable unsaturated resin composition is obtained by removing a solvent from the composition.A fourth aspect of the invention provides a composition which comprises a copolymer of a specified polysiloxane-based macromonomer with a compound represented by formula (1), and an organic aluminum chelate compound, and the composition is curable at low-temperatures.

    摘要翻译: PCT No.PCT / JP97 / 04660 Sec。 371日期1998年8月13日 102(e)日期1998年8月13日PCT 1997年12月17日PCT公布。 第WO98 / 27079号公报 日本1998年6月25日本发明的第一方面提供了含有由式(1)表示的反应性官能团的新化合物,R2-O-CO-NH-CH = CH-R1(1)其中R1表示氢原子, 芳族烃基或饱和或不饱和脂族烃基,R 2表示包含脂环官能团的式。 第二方面提供通过将上述化合物(1)的反应产物与含有酸基的不饱和树脂和稀释剂混合而制备的活性能量射线固化型不饱和树脂组合物。 组合物可以通过活性能量射线固化,可以用作碱显影性和活性能量射线固化型抗蚀剂树脂组合物。 第三方面提供一种活性能量射线聚合性不饱和树脂组合物,其通过在金属螯合物的存在下使含有式(1)表示的脂环式环氧基的不饱和化合物(E)与胶体二氧化硅(F)反应而得到, /或金属醇盐(G)。 通过从组合物中除去溶剂,得到粉末状活性能量射线可聚合不饱和树脂组合物。 本发明的第四方面提供了一种组合物,其包含特定的聚硅氧烷基大分子单体与式(1)表示的化合物的共聚物和有机铝螯合物,并且该组合物在低温下是可固化的。