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公开(公告)号：US5728857A
公开(公告)日：1998-03-17
申请号：US813588
申请日：1997-03-07
申请人： Takashi Kobayashi , Tadashi Amano , Hideshi Kurihara , Tomohisa Suzuki , Toshio Shinohara , Tohru Nishikawa
发明人： Takashi Kobayashi , Tadashi Amano , Hideshi Kurihara , Tomohisa Suzuki , Toshio Shinohara , Tohru Nishikawa
CPC分类号： C07F7/0818
摘要： Silicon-containing peroxyester compounds, for example, represented by the following formula: ##STR1## useful as a polymerization initiator, which compounds can produce vinyl chloride polymers having a high quality in a high yield and in a short reaction time.
摘要翻译： 含硅的过氧化酯化合物，例如可用作聚合引发剂的下式表示：该化合物可以以高产率和短的反应时间产生高质量的氯乙烯聚合物。
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2.发明授权1,1,2,2-tetramethylpropylperoxy esters and method for preparing vinyl polymers 失效1,1,2,2-四甲基丙基过氧酯和乙烯基聚合物的制备方法
公开(公告)号：US5783647A
公开(公告)日：1998-07-21
申请号：US566509
申请日：1995-12-04
申请人： Takashi Kobayashi , Tadashi Amano , Hideshi Kurihara , Toshio Shinohara , Yoshitaka Okuno , Tohru Nishikawa
发明人： Takashi Kobayashi , Tadashi Amano , Hideshi Kurihara , Toshio Shinohara , Yoshitaka Okuno , Tohru Nishikawa
CPC分类号： C08F4/34 , C07C409/38 , C08F14/06
摘要： Novel 1,1,2,2-tetramethylpropylperoxy esters are provided. They are useful as a polymerization initiator in polymerizing vinyl chloride, vinylidene chloride and vinyl acetate monomers, with the advantage of completing polymerization within a short time.
摘要翻译： 提供了新的1,1,2,2-四甲基丙基过氧酯。 它们可用作聚合氯乙烯，偏二氯乙烯和乙酸乙烯酯单体中的聚合引发剂，其优点是在短时间内完成聚合。
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3.发明授权
公开(公告)号：US5739222A
公开(公告)日：1998-04-14
申请号：US672448
申请日：1996-06-28
摘要： A vinyl chloride polymer is prepared through suspension polymerization of a vinyl chloride monomer in the presence of a polymerization initiator in a reactor. The reactor is charged with up to 4/5 of the overall monomer charge to initiate polymerization. Polymerization is carried out under a certain saturated vapor pressure of P1 kgf/cm.sup.2 at a preset polymerization temperature. When the internal pressure of the reactor declines to P2 kgf/cm.sup.2, the remainder of the overall monomer charge is continuously fed to the reactor so as to maintain the internal pressure within the range of (P1-.DELTA.P) wherein .DELTA.P=P1-P2 ranges from 0.1 to 2.0 kgf/cm.sup.2. A vinyl chloride polymer having a high degree of polymerization is efficiently produced while alleviating the load of heat removal.
摘要翻译： 通过聚合引发剂在反应器中的氯乙烯单体的悬浮聚合制备氯乙烯聚合物。 向反应器中加入高达+ E，总体单体电荷的4/5 + EE以引发聚合。 在预定的聚合温度下，在一定饱和蒸气压P1kgf / cm2下进行聚合。 当反应器的内部压力下降到P2kgf / cm 2时，将总体单体进料的剩余部分连续地供给到反应器中，以将内部压力保持在（P1- DELTA P）的范围内，其中DELTA P = P1- P2的范围为0.1至2.0kgf / cm2。 有效地制造具有高聚合度的氯乙烯聚合物，同时减轻除热负荷。
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公开(公告)号：US06242562B1
公开(公告)日：2001-06-05
申请号：US09468951
申请日：1999-12-22
申请人： Takashi Kobayashi , Tadashi Amano
发明人： Takashi Kobayashi , Tadashi Amano
IPC分类号： C08F624
摘要： A process for producing a vinyl chloride polymer is provided which includes the steps of: (A) suspension polymerizing vinyl chloride or a monomer mixture containing vinyl chloride, in an aqueous medium to obtain a polymer slurry; (B) stripping unreacted monomers remaining in the polymer slurry; and (C) subjecting the polymer slurry having passed through the step (B), to dehydration at a temperature of from 80° C. to 95° C., preferably within 60 minutes after the stripping. According to this process, the polymer cake obtained after the polymer slurry Is dehydrated can be made to have a greatly low water content. Hence the drying time in the drying step can be shortened to bring about an improvement in productivity and also to achieve a reduction of energy consumption in the drying step and consequently a reduction of production cost. Vinyl chloride polymer dried products having good anti-initial discoloration properties can be obtained.
摘要翻译： 提供了一种制备氯乙烯聚合物的方法，其包括以下步骤：（A）在水性介质中将氯乙烯或含有氯乙烯的单体混合物悬浮聚合以获得聚合物浆料;（B）将未反应的单体残留在 聚合物浆料; 和（C）使通过步骤（B）的聚合物浆料在80℃至95℃的温度下脱水，优选在剥离后60分钟内脱水。 根据该方法，可以使聚合物浆料脱水后得到的聚合物饼具有极低的含水量。 因此，干燥步骤中的干燥时间可以缩短，从而实现生产率的提高，并且还能够实现干燥步骤中的能量消耗的降低，从而降低生产成本。 可以获得具有良好抗初始变色特性的氯乙烯聚合物干燥产品。
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5.发明授权公开(公告)号：US06448372B2
公开(公告)日：2002-09-10
申请号：US09764093
申请日：2001-01-19
IPC分类号： C08F624
摘要： A process for producing a vinyl chloride polymer, including the steps of (a) subjecting a vinyl chloride monomer alone or a monomer mixture containing a vinyl chloride, to suspension polymerization in water; (b) subjecting the resultant vinyl chloride polymer slurry to stripping to remove an unreacted monomer remaining therein; and (c) dehydrating the polymer slurry having been subjected to stripping. In the polymerization step (a), the ratio of water/monomer is set in a weight ratio of from 0.80 to 1.50, and the viscosity at 20° C. of the polymer slurry to be fed to the stripping step is previously kept adjusted to 0.30 Pa·s or lower. In the stripping step (c), the residual unreacted monomer in the polymer slurry can efficiently be removed using steam in a smaller quantity, thus the vinyl chloride polymer can be produced at a high productivity.
摘要翻译： 一种制备氯乙烯聚合物的方法，包括以下步骤：（a）使单独的氯乙烯单体或含有氯乙烯的单体混合物在水中悬浮聚合; （b）将得到的氯乙烯聚合物浆料进行汽提以除去其中残留的未反应单体; 和（c）使经过剥离的聚合物浆料脱水。 在聚合步骤（a）中，将水/单体的比例设定为0.80至1.50的重量比，并将预先进料到汽提步骤的聚合物浆料的20℃下的粘度预先保持在 0.30 Pa.s以下。 在汽提步骤（c）中，聚合物淤浆中残留的未反应单体可以用较少量的蒸汽有效地除去，从而可以高生产率生产氯乙烯聚合物。
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公开(公告)号：US06339132B1
公开(公告)日：2002-01-15
申请号：US09634643
申请日：2000-08-08
申请人： Takashi Kobayashi , Fumiaki Adachi , Fujio Sato , Tadashi Amano
发明人： Takashi Kobayashi , Fumiaki Adachi , Fujio Sato , Tadashi Amano
IPC分类号： C08F218
CPC分类号： C08F6/001 , Y02P20/582 , C08L27/06
摘要： A process for regenerating unreacted vinyl chloride monomers is provided which has the step of compressing by means of an compressor an unreacted vinyl chloride monomer recovered from a process of vinyl chloride polymer production; compressing the same in contact with a lubricating oil fed into the compressor. In this process, the lubricating oil contains a polymerization inhibitor. Hence, even when this lubricating oil is circulated and reused as a lubricating oil after its separation from the unreacted vinyl chloride monomer, any vinyl chloride monomer remaining in the lubricating oil can effectively be kept from polymerizing in lubricating-oil circulation lines.
摘要翻译： 提供了一种用于再生未反应的氯乙烯单体的方法，其具有通过压缩机压缩由氯乙烯聚合物生产过程回收的未反应的氯乙烯单体的步骤; 将其压缩成与供给到压缩机中的润滑油接触。 在该方法中，润滑油含有阻聚剂。 因此，即使在将该润滑油与未反应的氯乙烯单体分离后作为润滑油循环再利用时，残留在润滑油中的任何氯乙烯单体也能够在润滑油循环管线中有效地聚合。
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公开(公告)号：US10077485B2
公开(公告)日：2018-09-18
申请号：US14409549
申请日：2012-06-27
IPC分类号： C22C38/26 , C21D6/00 , C22C38/00 , C22C38/06 , C22C38/04 , C21D9/46 , C21D8/02 , C22C38/02 , C22C38/24 , C22C38/38 , C23C8/26
CPC分类号： C21D9/46 , C21D6/002 , C21D6/005 , C21D6/008 , C21D8/0226 , C21D8/0263 , C21D2211/005 , C21D2211/009 , C22C38/00 , C22C38/001 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/24 , C22C38/26 , C22C38/38 , C23C8/26
摘要： A steel sheet for soft-nitriding has a composition containing: C: 0.05% or more to 0.10% or less; Si: 0.5% or less; Mn: 0.7% or more to 1.5% or less; P: 0.05% or less; S: 0.01% or less; Al: 0.01% or more to 0.06% or less; Cr: 0.5% or more to 1.5% or less; V: 0.03% or more to 0.30% or less; and N: 0.005% or less, on a mass percent basis, wherein a ratio of amount of solute V to the V content (amount of solute V/V content) is more than 0.50, and balance comprises Fe and incidental impurities, and a complex-phase microstructure containing ferrite and pearlite.
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公开(公告)号：US20150299830A1
公开(公告)日：2015-10-22
申请号：US14408662
申请日：2012-06-27
CPC分类号： C22C38/26 , C21D6/002 , C21D6/005 , C21D6/008 , C21D8/0263 , C21D9/46 , C21D2211/005 , C21D2211/009 , C22C38/00 , C22C38/001 , C22C38/002 , C22C38/02 , C22C38/04 , C22C38/06 , C23C8/32
摘要： A steel sheet for soft-nitriding has a composition containing: C: 0.05% or more to 0.10% or less; Si: 0.5% or less; Mn: 0.7% or more to 1.5% or less; P: 0.05% or less; S: 0.01% or less; Al: 0.01% or more to 0.06% or less; Cr: 0.5% or more to 1.5% or less; Nb: 0.005% or more to 0.025% or less; and N: 0.005% or less, on a mass percent basis, such that C and Nb satisfy 0.10≦Nb/C≦0.30 (where C and Nb are respective contents of the elements (by mass %)), wherein balance comprises Fe and incidental impurities, and a microstructure that is a complex-phase microstructure containing ferrite and pearlite, and the microstructure having a ratio of a microstructure other than the ferrite and the pearlite of 1% or less, and the microstructure having a ratio of polygonal ferrite in the ferrite of less than 50%.
摘要翻译： 软氮化钢板的组成为：C：0.05％以上且0.10％以下， Si：0.5％以下; Mn：0.7％以上至1.5％以下; P：0.05％以下; S：0.01％以下; Al：0.01％以上至0.06％以下; Cr：0.5％以上至1.5％以下; Nb：0.005％以上至0.025％以下; 和N：0.005％以下，C和Nb满足0.10＆nlE; Nb / C＆lt; NlE; 0.30（其中，C和Nb分别为元素含量（质量％）），其中余量包含Fe 和杂质，以及包含铁素体和珠光体的复相组织的显微组织以及具有1％以下的铁素体和珠光体以外的组织比的微结构，以及具有多边形铁素体 在铁素体中小于50％。
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公开(公告)号：US08866123B2
公开(公告)日：2014-10-21
申请号：US13884331
申请日：2010-11-22
IPC分类号： H01L47/00 , H01L45/00 , H01L29/792 , H01L27/24 , H01L29/66 , H01L27/115
CPC分类号： H01L27/2436 , H01L27/1157 , H01L27/11582 , H01L27/2409 , H01L27/2454 , H01L27/2481 , H01L27/249 , H01L29/66833 , H01L29/7926 , H01L45/06 , H01L45/1226 , H01L45/1233 , H01L45/144 , H01L45/1608 , H01L45/1616 , H01L45/1683
摘要： A vertical chain memory includes two-layer select transistors having first select transistors which are vertical transistors arranged in a matrix, and second select transistors which are vertical transistors formed on the respective first select transistors, and a plurality of memory cells connected in series on the two-layer select transistors. With this configuration, the adjacent select transistors are prevented from being selected by respective shared gates, the plurality of two-layer select transistors can be selected, independently, and a storage capacity of a non-volatile storage device is prevented from being reduced.
摘要翻译： 垂直链式存储器包括具有第一选择晶体管的两层选择晶体管，它们是以矩阵形式排列的垂直晶体管，第二选择晶体管是形成在各个第一选择晶体管上的垂直晶体管，以及多个存储单元串联连接 双层选择晶体管。 利用这种配置，防止相邻的选择晶体管被相应的共享栅极选择，可以独立地选择多个两层选择晶体管，并且防止非易失性存储装置的存储容量减小。
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公开(公告)号：US08835872B2
公开(公告)日：2014-09-16
申请号：US13806989
申请日：2011-06-23
申请人： Takashi Kobayashi
发明人： Takashi Kobayashi
IPC分类号： H01J37/20
CPC分类号： H01J37/20 , H01J2237/20285 , H01J2237/20292 , H01J2237/2817 , H01L21/68
摘要： A sample stage device (10) is so configured as to calculate ideal position information xtg(i), tg(i) per predetermined period that is unaffected by drive conditions relating to gaps (25, 26), etc., and to determine, per predetermined cycle and in real time, deviations dx(i), dy(i) between real-time measured positions x(i), y(i) by position detectors comprising laser interferometers (33, 34), etc., and ideal position information xtg(i), tg(i). In addition, it calculates, based on deviations dx(i), dy(i) thus determined, such speed command values vx(i), vy(i) for motors (27, 28) that measured values x(i), y(i) would follow ideal position information xtg(i), tg(i), and performs stable and high-speed positioning control for a sample table (11) through feedback control that controls speed in real time. Thus, with respect to a sample stage device, it is possible to provide a stable and high-speed positioning control method for a sample table, which is capable of suppressing noise caused by thermal drift and vibration, without being affected by drive conditions, such as the initial states of gaps, etc.
摘要翻译： 样品台装置（10）被配置为计算不受与间隙（25,26）等有关的驱动条件的影响的每预定周期的理想位置信息xtg（i），tg（i） 并且实时地通过包括激光干涉仪（33,34）的位置检测器等实时测量位置x（i），y（i）之间的偏差dx（i），dy（i）和理想 位置信息xtg（i），tg（i）。 另外，根据如此确定的偏差dx（i），dy（i），计算出测量值x（i），y（i）的电动机（27,28）的速度指令值vx（i），vy （i）将遵循理想位置信息xtg（i），tg（i），并且通过实时控制速度的反馈控制对样本表（11）执行稳定和高速定位控制。 因此，对于样品台装置，可以提供一种用于样品台的稳定且高速的定位控制方法，其能够抑制由热漂移和振动引起的噪声，而不受驱动条件的影响，例如 作为差距的初始状态等
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