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9 条记录 (耗时 0.015 秒)

    Stable and homogeneous aqueous formulations of surfactants
    1.
    发明授权
    Stable and homogeneous aqueous formulations of surfactants 失效
    表面活性剂的稳定且均匀的水性制剂

    公开(公告)号：US5389280A

    公开(公告)日：1995-02-14

    申请号：US821682

    申请日：1992-01-16

    申请人： Thomas Martini ,  Karl-Heinz Keil ,  Ignaz Wimmer

    发明人： Thomas Martini ,  Karl-Heinz Keil ,  Ignaz Wimmer

    IPC分类号： B01F17/24 ,  B01F17/00 ,  B01J13/00 ,  C11D1/12 ,  C11D1/28 ,  C11D1/52 ,  C11D1/66 ,  C11D1/72 ,  C11D1/74 ,  C11D1/83 ,  C09D9/00 ,  C11D7/32 ,  C11D7/50

    CPC分类号： B01F17/0085 ,  C11D1/12 ,  C11D1/83 ,  C11D1/28 ,  C11D1/526 ,  C11D1/667 ,  C11D1/72 ,  C11D1/74

    摘要： Stable and homogeneous aqueous formulations of surfactantsStable and homogeneous aqueous formulations of surfactants having an HLB value of less than or equal to 13, which additionally contain a compound of the formula I ##STR1## in which R.sup.1 is C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -alkenyl, phenyl, alkylphenyl or phenalkyl having in each case 1 to 4 carbon atoms in the alkyl chain or cyclohexyl, R.sup.2 is hydrogen or one of the radicals mentioned for R.sup.1, or R.sup.1 and R.sup.2, together with the nitrogen atom, are a heterocyclic radical, M is an alkali metal cation, an ammonium cation or one equivalent of an alkaline earth metal or aluminium cation and m and n in each case independently of one another are numbers from 6 to 8.By the presence of the compounds of the formula I, it is possible to prepare stable and homogeneous aqueous formulations even from those surfactants which are otherwise only sparingly soluble or not soluble at all in water.

    摘要翻译： 稳定且均匀的表面活性剂水性制剂具有HLB值小于或等于13的表面活性剂的稳定且均匀的水性制剂，其另外含有式I化合物（I），其中R 1是C 1 -C 8 - 烷基 ，在烷基链或环己基中各自为1至4个碳原子的C1-C8-烯基，苯基，烷基苯基或苯烷基，R2为氢或R1或R1和R2所提及的一个基团，以及氮原子 是杂环基，M是碱金属阳离子，铵阳离子或一当量的碱土金属或铝阳离子，m和n在每种情况下彼此独立地为6至8.通过存在 式I的化合物，即使从那些仅在微溶于水或不溶于水的那些表面活性剂中，也可制备稳定和均匀的水性制剂。

    Process for the purification of alkylene oxide adducts
    2.
    发明授权
    Process for the purification of alkylene oxide adducts 失效
    烯化氧加合物的纯化方法

    公开(公告)号：US5012013A

    公开(公告)日：1991-04-30

    申请号：US516133

    申请日：1990-04-26

    申请人： Ignaz Wimmer ,  Siegfried Billenstein

    发明人： Ignaz Wimmer ,  Siegfried Billenstein

    IPC分类号： B01J27/10 ,  B01J27/135 ,  C07B61/00 ,  C07C41/34 ,  C07C43/11 ,  C08G65/30

    CPC分类号： C07C41/34 ,  C08G65/30

    摘要： A novel process for the purification of an alkylene oxide adduct which has been prepared using halogen-containing metal catalysts and contains halogen-containing compounds and also metals as impurities comprises treating the alkylene oxide adduct which is to be purified with an excess of alkali metal compound and adjusting the pH of the alkaline mixture obtained to a value of at most 7 using an acid, with the proviso that the water content of the product mixture which is then present is at least 0.1% by weight, relative to the weight of the product. This product mixture is freed from water and other solvents, this resulting in the precipitation in coarse crystalline form of salts which are insoluble in the alkylene oxide adduct and which can be easily separated off to isolate the desired pure alkylene oxide adduct.

    摘要翻译： 使用含卤素的金属催化剂制备并含有含卤素的化合物以及金属作为杂质的用于净化环氧烷烃加合物的新方法包括用过量的碱金属化合物处理待纯化的烯化氧加合物 并使用酸将所得到的碱性混合物的pH调节至至多7，条件是当前存在的产物混合物的水含量相对于产物的重量为至少0.1重量％ 。 该产物混合物不含水和其它溶剂，这导致沉淀在粗结晶形式的盐，其不溶于环氧烷加合物，并且可以容易地分离出来以分离所需的纯氧化烯加合物。

    Alkoxylation catalyst
    3.
    发明授权
    Alkoxylation catalyst 失效
    烷氧基化催化剂

    公开(公告)号：US06365541B1

    公开(公告)日：2002-04-02

    申请号：US09257630

    申请日：1999-02-25

    申请人： Ignaz Wimmer ,  Hildegard Freundl

    发明人： Ignaz Wimmer ,  Hildegard Freundl

    IPC分类号： B01J3100

    CPC分类号： C08G65/2642 ,  B01J31/04 ,  B01J2231/4288 ,  C07C41/03 ,  C07C67/26 ,  C07C69/24 ,  C07C43/11 ,  C07C43/1785

    摘要： An alkoxylation catalyst is prepared by a) reaction of one mol of a dicarboxylic acid with from 1.5 to 8 mol of an alkoxylated alcohol to form the corresponding dicarboxylic monoester, b) formation of an alkaline earth metal salt of the dicarboxylic monoester by addition of water and from 0.45 to 0.55 mol of a basic alkaline earth metal compound per mol of dicarboxylic acid originally used, c) partial neutralization of the alkaline earth metal salt by addition of from 0.25 to 0.7 mol of H2SO4 per mol of basic alkaline earth metal compound originally used and d) removal of the water present at a temperature of less than 100° C. The catalyst prepared in this way makes it possible to prepare colorless alkoxylates having a narrow homologue distribution.

    摘要翻译： 通过a）使一摩尔二羧酸与1.5至8摩尔烷氧基化醇反应形成相应的二羧酸单酯来制备烷氧基化催化剂，b）通过加入水形成二羧酸单酯的碱土金属盐;和 原始使用的每摩尔二羧酸为0.45〜0.55摩尔的碱土金属化合物，c）通过加入0.25〜0.7摩尔H 2 SO 4 /摩尔碱性碱土金属化合物，最初使用的部分中和 和d）去除在低于100℃的温度下存在的水。以这种方式制备的催化剂使得可以制备具有窄的同系物分布的无色烷氧基化物。

    Process for the preparation of ether carboxylic acids with low residual alcohol content
    4.
    发明授权
    Process for the preparation of ether carboxylic acids with low residual alcohol content 失效
    具有低残留酒精含量的醚羧酸的制备方法

    公开(公告)号：US06326514B1

    公开(公告)日：2001-12-04

    申请号：US09596418

    申请日：2000-06-19

    申请人： Peter Klug ,  Rainer Kupfer ,  Ignaz Wimmer ,  Rüdiger Winter

    发明人： Peter Klug ,  Rainer Kupfer ,  Ignaz Wimmer ,  Rüdiger Winter

    IPC分类号： C07C59125

    CPC分类号： C07C51/367 ,  C07C59/125

    摘要： The invention provides a process for the preparation of ether carboxylic acids or alkali metal or ammonium salts thereof with low residual alcohol content, which comprises firstly converting a mono- or polyhydric alcohol into the corresponding alkoxide using a substoichiometric amount between 5 and 95 mol % of a basic compound, and then reacting the alkoxide with alkylene oxides, and, if necessary after distilling off the residual alcohol which remains, alkylating the highly alkaline reaction mixture, which comprises more than 5 mol % of alkoxylated alkoxides, directly with a chloroacetic acid derivative, and, if necessary, converting the alkylated product into the free ether carboxylic acid by acidification with mineral acid.

    摘要翻译： 本发明提供了制备具有低残留醇含量的醚羧酸或其碱金属或铵盐的方法，其包括首先将一元醇或多元醇转化为相应的醇盐，其中使用亚化学计量为5-95mol％ 碱性化合物，然后使烷氧基与环氧烷反应，并且如果需要，蒸馏剩余的残余醇后，直接用氯乙酸衍生物烷基化高碱性反应混合物（其包含大于5mol％的烷氧基化的醇盐） ，如果需要，通过用无机酸酸化将烷基化产物转化成游离醚羧酸。

    Poly(alkoxy ether) mixed formals
    9.
    发明授权
    Poly(alkoxy ether) mixed formals 失效
    聚（烷氧基醚）混合物

    公开(公告)号：US4992595A

    公开(公告)日：1991-02-12

    申请号：US274698

    申请日：1988-11-23

    申请人： Rolf Kleber ,  Siegfried Billenstein ,  Lothar Jaeckel ,  Ignaz Wimmer

    发明人： Rolf Kleber ,  Siegfried Billenstein ,  Lothar Jaeckel ,  Ignaz Wimmer

    IPC分类号： C07C41/00 ,  C07C41/50 ,  C07C43/315 ,  C07C67/00 ,  C08G65/32

    CPC分类号： C07C43/315

    摘要： Compounds of the formula ##STR1## where R.sub.1 denotes a group of the formula ##STR2## R.sub.2 denotes C.sub.1 -C.sub.4 -alkyl, R.sub.3 denotes hydrogen or methyl, n denotes a number from 5 to 100, m denotes an integer from 0 to 4 and x denotes the number of free valences of the particular R.sub.1 radical, a process for the preparation thereof, and the use thereof as fiber spin finishes.

    摘要翻译： 其中R 1表示下式的基团的化合物：其中R 1表示下式的基团：其中R 1表示C 1 -C 4烷基，R 3表示氢或甲基，n表示5〜 100，m表示0至4的整数，x表示特定的R 1基团的游离价数，其制备方法及其作为纤维旋涂的用途。