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    Method For Producing Pure Alpha-Alkoxy-Omega-Hydroxy-Polyalkylene Glycols
    2.
    发明申请
    Method For Producing Pure Alpha-Alkoxy-Omega-Hydroxy-Polyalkylene Glycols 有权
    纯α-烷氧基-ω-羟基 - 聚亚烷基二醇的生产方法

    公开(公告)号：US20080076947A1

    公开(公告)日：2008-03-27

    申请号：US11792768

    申请日：2005-11-25

    申请人： Klaus Poellmann ,  Anton Strasser ,  Reinhard Vybiral ,  Rainer Wagner

    发明人： Klaus Poellmann ,  Anton Strasser ,  Reinhard Vybiral ,  Rainer Wagner

    IPC分类号： C07C29/10 ,  C07C33/02

    CPC分类号： C08G65/2609 ,  C08G65/2648 ,  C08G65/2651

    摘要： The invention relates to a method for producing pure alpha-alkoxy-Ω-hydroxy-polyalkylene glycols, creating small impurities of the product on high-molecular a-Ω-di-hydroxy-polyalkylene glycols. The method is based on the use of high-boiling initiator alcohols of the following general structure R2—(OCH2CHR)k—OH wherein R2 represents an alkyl radical comprising between 1 and 4 C atoms, preferably R2=CH3, k represents a number between 1 and 10, preferably between 1 and 4, and R represents H, CH3 or an alkyl radical comprising between 2 and 4 C atoms, preferably R=H, CH3. The use of the cited initiator alcohols enables the mixture of a basic catalyst and an initiator alcohol to be dried in such a way that it has a very low water content, and thus to produce very low concentrations of unwanted a-Ω-di-hydroxy-polyalkylene glycol impurities.

    摘要翻译： 本发明涉及一种生产纯α-烷氧基 - 羟基 - 羟基 - 聚亚烷基二醇的方法，在高分子α-ω-二羟基 - 聚亚烷基二醇上产生产物的小杂质。 该方法基于使用以下通式结构的高沸点引发剂醇R 2 - （OCH 2 CH 2）n -OH 其中R 2表示包含1至4个C原子的烷基，优选R 2 = CH 3，k表示1和 10，优选1至4，R表示H，CH 3或包含2至4个C原子，优选R = H，CH 3 3的烷基。 使用所引发的引发剂醇使得碱性催化剂和引发剂醇的混合物以使其具有非常低的水含量的方式被干燥，从而产生非常低浓度的不想要的α-二羟基 - 聚亚烷基二醇杂质。

    Method for producing pure α-alkoxy-Ω-hydroxy-polyalkylene glycols
    3.
    发明授权
    Method for producing pure α-alkoxy-Ω-hydroxy-polyalkylene glycols 有权
    纯α-烷氧基 - 羟基 - 聚亚烷基二醇的制备方法

    公开(公告)号：US07435857B2

    公开(公告)日：2008-10-14

    申请号：US11792768

    申请日：2005-11-25

    申请人： Klaus Poellmann ,  Anton Strasser ,  Reinhard Vybiral ,  Rainer Wagner

    发明人： Klaus Poellmann ,  Anton Strasser ,  Reinhard Vybiral ,  Rainer Wagner

    IPC分类号： C07C43/13

    CPC分类号： C08G65/2609 ,  C08G65/2648 ,  C08G65/2651

    摘要： The invention relates to a method for producing pure alpha-alkoxy-Ω-hydroxy-polyalkylene glycols, creating small impurities of the product on high-molecular a-Ω-di-hydroxy-polyalkylene glycols. The method is based on the use of high-boiling initiator alcohols of the following general structure R2—(OCH2CHR)k—OH wherein R2 represents an alkyl radical comprising between 1 and 4 C atoms, preferably R2═CH3, k represents a number between 1 and 10, preferably between 1 and 4, and R represents H, CH3 or an alkyl radical comprising between 2 and 4 C atoms, preferably R═H, CH3. The use of the cited initiator alcohols enables the mixture of a basic catalyst and an initiator alcohol to be dried in such a way that it has a very low water content, and thus to produce very low concentrations of unwanted a-Ω-di-hydroxy-polyalkylene glycol impurities.

    摘要翻译： 本发明涉及一种生产纯α-烷氧基 - 羟基 - 羟基 - 聚亚烷基二醇的方法，在高分子α-ω-二羟基 - 聚亚烷基二醇上产生产物的小杂质。 该方法基于使用以下通式结构的高沸点引发剂醇R 2 - （OCH 2 CH 2）n -OH 其中R 2代表包含1至4个C原子的烷基，优选R 2 -CH 3，k表示1至 10，优选1至4，R表示H，CH 3或包含2至4个C原子，优选RH，CH 3 3的烷基。 使用所引发的引发剂醇使得碱性催化剂和引发剂醇的混合物以使其具有非常低的水含量的方式被干燥，从而产生非常低浓度的不想要的α-二羟基 - 聚亚烷基二醇杂质。

    Amidopropyl-N-alkyl-polylhydroxyalkylamine compounds, processes for their preparation and their use
    4.
    发明授权
    Amidopropyl-N-alkyl-polylhydroxyalkylamine compounds, processes for their preparation and their use 失效
    氨基丙基-N-烷基 - 多羟基烷基胺化合物，其制备方法及其应用

    公开(公告)号：US5925775A

    公开(公告)日：1999-07-20

    申请号：US691469

    申请日：1996-08-02

    申请人： Gunter Prossel ,  Reinhard Vybiral ,  Werner Skrypzak ,  Hans Jurgen Scholz

    发明人： Gunter Prossel ,  Reinhard Vybiral ,  Werner Skrypzak ,  Hans Jurgen Scholz

    IPC分类号： A61K8/00 ,  A61K8/42 ,  A61Q5/02 ,  A61Q19/10 ,  B01F17/00 ,  B01F17/22 ,  C07C231/02 ,  C07C233/36 ,  C07C233/38 ,  C11D1/52 ,  C07C233/00

    CPC分类号： A61Q19/10 ,  A61K8/42 ,  A61Q5/02 ,  B01F17/0042 ,  C07C233/36 ,  C11D1/528

    摘要： Amidopropyl-N-alkyl-polyhydroxyalkylamines of the following formula (1) ##STR1## in which Z is a linear polyhydroxyhydrocarbon radical having at least 2 free or oxyalkylated hydroxyl groups, R.sup.1 is a C.sub.1 to C.sub.7 -alkyl radical or C.sub.2 to C.sub.4 -hydroxyalkyl radical and COR is an aliphatic acyl radical having 6 to 22 carbon atoms, and salts thereof from an inorganic or organic acid are described. They are prepared by a) reaction of a compound of the formula (2) ##STR2## with acrylonitrile to give the compound of the formula (3) ##STR3## b) hydrogenation of the product obtained in step a) to give the compound of the formula (4) ##STR4## and c) monoacylation of the product obtained in step b) in the melt to give the compound of the formula (1) mentioned. The compounds according to the invention are readily soluble in water and water/alcohol mixtures and are advantageous co-surfactants for use in detergents and cleaning compositions and in cosmetic preparations for cleansing the hair and skin.

    摘要翻译： Z为具有至少2个游离或烷氧基化羟基的直链多羟基烃基的下式（1）的氨基丙基-N-烷基 - 多羟基烷基胺，R 1为C 1至C 7 - 烷基或C 2至C 4 - 羟基烷基，COR 是具有6至22个碳原子的脂族酰基，并且描述了其来自无机或有机酸的盐。 它们通过以下步骤制备：a）式（2）化合物与丙烯腈的反应，得到式（3）化合物b）氢化步骤a）得到的产物得到式（4）化合物和 c）在步骤b）中获得的产物在熔体中的单酰化，得到所述式（1）的化合物。 根据本发明的化合物易溶于水和水/醇混合物，并且是用于洗涤剂和清洁组合物和用于清洁头发和皮肤的化妆品制剂中的有利的辅助表面活性剂。

    Polyalkylene glycol lubricant base oils with narrow molar mass distribution
    5.
    发明申请
    Polyalkylene glycol lubricant base oils with narrow molar mass distribution 审中-公开
    具有窄摩尔质量分布的聚亚烷基二醇润滑油基础油

    公开(公告)号：US20070191647A1

    公开(公告)日：2007-08-16

    申请号：US11705944

    申请日：2007-02-13

    申请人： Klaus Poellmann ,  Anton Strasser ,  Guido Scholz ,  Reinhard Vybiral

    发明人： Klaus Poellmann ,  Anton Strasser ,  Guido Scholz ,  Reinhard Vybiral

    IPC分类号： C07C31/18

    CPC分类号： C08G65/2609 ,  C08G65/2645 ,  C08G65/2663

    摘要： The present invention provides a process for preparing polyalkylene glycols by reacting a mixture of a mono- or polyhydric alcohol and a polyalkylene glycol prepolymer with a C2- to C4-alkylene oxide or a mixture of such alkylene oxides in the presence of a catalyst which comprises Zn3[Co(CN)6]2, the mono- or polyhydric alcohol having a molecular weight of up to 500 g/mol and containing from 1 to 20 carbon atoms and from 1 to 10 hydroxyl groups, and the polyalkylene glycol prepolymer being the addition product of a C2- to C4-alkylene oxide or of a mixture of such alkylene oxides in an amount of at least 500 g/mol to a mono- or polyhydric alcohol having from 1 to 20 carbon atoms and from 1 to 10 hydroxyl groups.

    摘要翻译： 本发明提供了通过将一元或多元醇和聚亚烷基二醇预聚物的混合物与C 2〜C 4 - 亚烷基亚烷基 氧化物或这种环氧烷烃的混合物，在包含Zn 3 Co（CN）6 N 2 N 2的催化剂存在下，单 - 或分子量高达500g / mol且含有1至20个碳原子和1至10个羟基的多元醇，并且聚亚烷基二醇预聚物是C 2 N 2的加成产物 或者至少为500g / mol的这种环氧烷的混合物与具有1至20个碳原子的一元或多元醇和1个 至10个羟基。

    Process for the preparation of pure aqueous betaine solutions
    6.
    发明授权
    Process for the preparation of pure aqueous betaine solutions 失效
    制备纯甜菜碱水溶液的方法

    公开(公告)号：US5371250A

    公开(公告)日：1994-12-06

    申请号：US120281

    申请日：1993-09-13

    申请人： Hubert Seitz ,  Reinhard Vybiral

    发明人： Hubert Seitz ,  Reinhard Vybiral

    IPC分类号： B01F17/28 ,  C07C227/08 ,  C07C227/40 ,  C07C227/44 ,  C07C229/12 ,  C07C231/12 ,  C07C233/36 ,  C07C231/100

    CPC分类号： C07C227/08 ,  C07C231/12

    摘要： The process described relates to the preparation of aqueous betaine solutions by reaction of a tertiary amine with an .omega.-monohalocarboxylic acid, preferably monochloroacetic acid, and an alkali metal hydroxide in the presence of water, which solutions are said to be highly pure particularly in respect of the tertiary starting amine and .omega.-monohalocarboxylic acid. This is achieved by first reacting the three reaction components in a certain molar ratio with the aim of obtaining a betaine solution which comprises only a tolerated amount of starting amine. This aqueous betaine solution is then treated with a sulfonating agent, preferably with an alkali metal sulfite, alkali metal pyrosulfite or alkali metal bisulfite, for conversion of the .omega.-monohalocarboxylic acid present into the corresponding sulfocarboxylic acid, which is not troublesome. The process described is simple to carry out and leads to the highly pure aqueous betaine solutions mentioned.

    摘要翻译： 所描述的方法涉及通过叔胺与ω-单卤代羧酸（优选一氯乙酸）和碱金属氢氧化物在水存在下反应来制备甜菜碱水溶液，该溶液被认为是高度纯的，特别是在这方面 的叔起始胺和ω-单卤代羧酸。 这通过首先使三种反应组分以一定摩尔比反应，以获得仅包含耐受量的起始胺的甜菜碱溶液来实现。 然后用磺化剂，优选用碱金属亚硫酸盐，碱金属焦亚硫酸盐或碱金属亚硫酸氢盐处理这种甜菜碱水溶液，用于将存在的ω-单卤代羧酸转化成相应的磺基羧酸，这是不麻烦的。 所描述的方法很容易进行并导致所提及的高纯度的甜菜碱水溶液。