摘要:
The invention relates to an improved process for preparing triallyl cyanurate (TAC) by reacting cyanuric chloride with allyl alcohol in the presence of an alkali metal acid acceptor and in the absence of an organic solvent other than allyl alcohol. According to the invention, TAC is obtained in over 99% purity with an APHA colour number below 10 in a yield of over 90% when 3.9 to 6.0 mol of allyl alcohol and 3.0 to 3.2 equivalents of acid acceptor are used per mole of cyanuric chloride, cyanuric chloride and acid acceptor are added simultaneously or successively to anhydrous or at least 50% by weight aqueous allyl alcohol, and the reaction is performed in one or more stages at a temperature in the range of −5 to +50° C.
摘要:
Exemplary embodiments are directed to a test arrangement for testing surge voltage in electrical high voltage components with a surge voltage generator and a voltage distributor. The surge voltage generator and voltage distributor have a tower-like structure with a first and a second structure end. A rectangular container is connected to the first and second structure and includes a first and a second container end. At least one of the surge voltage generator and the voltage distributor are movable between a first substantially horizontal position inside the container and a substantially vertical position relative to the container. Each movement between the two positions involves a pivot motion about a rotational axis perpendicular to the longitudinal direction of the surge voltage generator.
摘要:
The present invention is directed towards a method for the production of 2,4,6-trimercapto-1,3,5-triazine (TMT-H3). In particular, the method of the subject matter relates to the operation of acidifying the salts of 2,4,6-trimercapto-1,3,5-triazine in aqueous solution and in a defined pH range.
摘要:
The direct handling of acrolein for the purpose of combatting microbial, vegetable and animal pests in water and soil is problematic on account of the potential for danger of acrolein. According to the invention a composition which releases acrolein upon contact with water at the site of use and is easy to handle is used. The composition in accordance with the invention contains an acrolein acetal, preferably 2-vinyl-1,3-dioxolane, and a compound hydrolyzable to an acid with a pK.sub.s value of less than 4, especially one from the series of organic acid anhydrides, organic acid halides and inorganic halogen compounds forming hydrogen halide upon hydrolysis.
摘要:
A method and apparatus are disclosed for implementing absolute interferometry with radiation generated by diode laser whereby relative or absolute distance measurement can be performed without need of a reference interferometer, with only a single detector, and with high precision determination of the length of the measurement distance. The method comprises modulating the radiation generated by the diode laser in such a way that the diode laser is frequency-modulated at at least one discrete frequency, which then is detected with a known phase-sensitive detection method. Due to the modulation of the original radiation of the diode laser, a second laser beam is in effect produced, with the result that a single beam path includes a measurement beam and a reference beam. Each of these beams, i.e. the measurement beam and the reference beam, is at a different frequency, but the two have parallel wave fronts, pass along exactly the same optical path in the unitary beam, and interfere at the single detector. The length of the measurement distance is then found by a determination of phase shift or determination of the phase change of the modulation signal. Alternatively, the modulation frequency of the diode laser can be changed until the detector shows that a predetermined phase shift between the original first beam of the diode laser and the second, modulation-produced beam, with altered frequency, exists or has been passed through. By determining the modulation frequency at which the predetermined phase shift is reached, and taking the difference between this and the initial modulation frequency, the absolute length of the measurement distance can be found.
摘要:
The invention relates to a process for preparing dodecamethylenebismelamine (DMB) by reacting 2,4-diamino-6-chloro-1,3,5-triazine with 1,12-diaminododecane in an alkaline aqueous suspension, to which the diamine has been added in a water-miscible solvent. The product is used to stabilize aqueous formaldehye solutions.
摘要:
Pentaerythritol is treated at a temperature of about 180.degree. to 220.degree. C. with a strongly alkaline acting material, e.g. calcium oxide. The thus treated pentaerythritol serves as a costabilizer e.g., with the salt of a polyvalent metal and a carboxylic acid, for a vinyl chloride resin, e.g. polyvinyl chloride and has outstanding properties as such.
摘要:
Pure hydroxypropyltheophylline is produced by the catalytic reaction of theophylline with glycidol in the presence of a hydroxide of a short chain alcoholate of an alkali metal or an alkali metal salt of a pseudohydrohalic acid which has a readily polarizable anion. The catalyst is suitably employed in an amount between 0.01 and 0.2 moles per mole of theophylline. The dihydroxypropyltheophylline is obtained directly in the reaction in a high purity.
摘要:
Guaiacol glycerine ether is obtained in very good yield and in very high purity by reacting glycidol with o-methyoxyphenol in the presence of an alkali hydroxide, an alkali alcoholate, an alkali cyanate or an alkali thiocyanate at 80.degree. to 150.degree. C. An especially effective purification of the crude product can be obtained by adding hydrogen peroxide, preferably prior to cooling.
摘要:
A system is provided for creating and/or collecting, storing and providing access to data from an electric power device which contains a cooling or operating liquid. A sensing device is mounted on the electric power device. The sensing device includes a microprocessor/microcontroller, a memory, a display panel, an input panel, and a tag read/write apparatus. A sampling container for holding a liquid sample to be taken from the electric power device has a container tag mounted thereon. The tag read/write apparatus uses a wireless communication link, when a sample has been taken, to transmit (i) administrative data denoting the electric power device, and (ii) diagnosis data denoting the sample taken to the container tag. The diagnosis data can be input directly using the input panel of the sensing device when a sample has been taken.