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公开(公告)号：US08163842B2
公开(公告)日：2012-04-24
申请号：US12937844
申请日：2009-04-13
申请人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
发明人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
IPC分类号： C08L83/02
CPC分类号： C08F299/0492 , C01B33/44 , H01L31/0392 , Y02E10/50
摘要： This invention relates to a method for producing a transparent composite material comprising a first step of subjecting a synthetic smectite having a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300 to organizing treatment with an organic quaternary ammonium salt and/or an organic quaternary phosphonium salt; a second step of mixing the synthetic smectite subjected to organizing treatment and a curable resin to prepare a resin composition containing the synthetic smectite in an amount of 10 to 40 mass %; a third step of curing the resin composition to obtain a cured product; and a forth step of removing the organic volatile components remaining in the cured product. According to the method, a transparent composite material which is flexible and has a low coefficient of thermal expansion can be obtained which is reduced in outgassing at high temperature under vacuum as in vapor deposition of a conductive thin film.
摘要翻译： 本发明涉及一种透明复合材料的制造方法，该方法包括：将数均粒径为10〜300nm，长径比为10〜300的合成蒙脱石进行有机季铵化处理的第1工序 盐和/或有机季鏻盐; 混合经过组织处理的合成蒙皂石和固化性树脂的第二步骤，制备含有10〜40质量％的合成蒙皂石的树脂组合物; 固化树脂组合物以获得固化产物的第三步骤; 以及除去保留在固化物中的有机挥发成分的第四工序。 根据该方法，可以获得柔性且具有低热膨胀系数的透明复合材料，这在真空下在高温下在导电薄膜的气相沉积中减少脱气。
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公开(公告)号：US20110040015A1
公开(公告)日：2011-02-17
申请号：US12937844
申请日：2009-04-13
申请人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
发明人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
CPC分类号： C08F299/0492 , C01B33/44 , H01L31/0392 , Y02E10/50
摘要： This invention relates to a method for producing a transparent composite material comprising a first step of subjecting a synthetic smectite having a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300 to organizing treatment with an organic quaternary ammonium salt and/or an organic quaternary phosphonium salt; a second step of mixing the synthetic smectite subjected to organizing treatment and a curable resin to prepare a resin composition containing the synthetic smectite in an amount of 10 to 40 mass %; a third step of curing the resin composition to obtain a cured product; and a forth step of removing the organic volatile components remaining in the cured product. According to the method, a transparent composite material which is flexible and has a low coefficient of thermal expansion can be obtained which is reduced in outgassing at high temperature under vacuum as in vapor deposition of a conductive thin film.
摘要翻译： 本发明涉及一种透明复合材料的制造方法，其特征在于，包括：将数均粒径为10〜300nm，纵横比为10〜300的合成蒙脱石进行有机季铵化处理的第1工序 盐和/或有机季鏻盐; 混合经过组织处理的合成蒙皂石和固化性树脂的第二步骤，制备含有10〜40质量％的合成蒙皂石的树脂组合物; 固化树脂组合物以获得固化产物的第三步骤; 以及除去保留在固化物中的有机挥发成分的第四工序。 根据该方法，可以获得柔性且具有低热膨胀系数的透明复合材料，这在真空下在高温下在导电薄膜的气相沉积中减少脱气。
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公开(公告)号：US08460501B2
公开(公告)日：2013-06-11
申请号：US12937939
申请日：2009-04-13
申请人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
发明人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
CPC分类号： H01M14/005 , C08J5/18 , C08J2333/06 , H01L31/0392 , H01L31/03926 , H01L31/048 , Y02E10/50 , Y10T428/31935
摘要： This invention relates to a method for producing a cured film, which comprises a first step of applying a curable resin composition onto a surface of a first substrate and a surface of a second substrate respectively; a second step of bonding the curable resin composition layers provided on each surface of the first and second substrates to each other; and a third step of curing the curable resin composition layer between the first and the second substrates. The present invention enables production of a cured film in which the amount of thermal deformation such as warpage upon heating/cooling is suppressed, and the film can be suitably used as a plastic substrate for a display such as a liquid crystal display device and an organic EL display device, a substrate for a display, such as a substrate for electronic paper and the like, and a substrate for a solar cell.
摘要翻译： 本发明涉及一种固化膜的制造方法，该方法包括：分别在第一基板和第二基板的表面上施加固化性树脂组合物的第一工序; 将设置在第一和第二基板的每个表面上的可固化树脂组合物层彼此接合的第二步骤; 以及在所述第一和第二基板之间固化所述可固化树脂组合物层的第三步骤。 本发明能够制造其中热变形如加热/冷却时的翘曲量被抑制的固化膜的生产，并且该膜可以适合用作液晶显示装置和有机物等显示器的塑料基板 EL显示装置，用于电子纸等的显示器用基板和太阳能电池用基板。
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公开(公告)号：US20110039117A1
公开(公告)日：2011-02-17
申请号：US12937939
申请日：2009-04-13
申请人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
发明人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
CPC分类号： H01M14/005 , C08J5/18 , C08J2333/06 , H01L31/0392 , H01L31/03926 , H01L31/048 , Y02E10/50 , Y10T428/31935
摘要： This invention relates to a method for producing a cured film, which comprises a first step of applying a curable resin composition onto a surface of a first substrate and a surface of a second substrate respectively; a second step of bonding the curable resin composition layers provided on each surface of the first and second substrates to each other; and a third step of curing the curable resin composition layer between the first and the second substrates. The present invention enables production of a cured film in which the amount of thermal deformation such as warpage upon heating/cooling is suppressed, and the film can be suitably used as a plastic substrate for a display such as a liquid crystal display device and an organic EL display device, a substrate for a display, such as a substrate for electronic paper and the like, and a substrate for a solar cell.
摘要翻译： 本发明涉及一种固化膜的制造方法，该方法包括：分别在第一基板和第二基板的表面上施加固化性树脂组合物的第一工序; 将设置在第一和第二基板的每个表面上的可固化树脂组合物层彼此接合的第二步骤; 以及在所述第一和第二基板之间固化所述可固化树脂组合物层的第三步骤。 本发明能够制造其中热变形如加热/冷却时的翘曲量被抑制的固化膜的生产，并且该膜可以适合用作液晶显示装置和有机物等显示器的塑料基板 EL显示装置，用于电子纸等的显示器用基板和太阳能电池用基板。
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公开(公告)号：US08518524B2
公开(公告)日：2013-08-27
申请号：US12373977
申请日：2007-07-20
申请人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
发明人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
CPC分类号： B82Y30/00 , C08G63/21 , C08J5/005 , C08J5/18 , C08J2333/04 , C08J2367/07 , C08L51/10 , C09D151/10 , C08L2666/02
摘要： The invention provides a transparent composite material comprising a cured product of a three-dimensionally crosslinkable resin composition containing tabular inorganic substance having a number-average particle size of 10 to 300 nm and an aspect ratio of 10 to 300 dispersed therein, which material has a small coefficient of thermal expansion against surrounding temperature changes and can be suitably applicable as substrate for display devices, to thereby overcome disadvantages in substrate for display devices using conventional materials that differences in thermal shrinkage between a substrate and an transparent electrode cause cracks in the transparent electrode, resulting in increasing resistance and causing disconnection, and further can provide a display device with high durability.
摘要翻译： 本发明提供了一种透明复合材料，其包含三维可交联树脂组合物的固化产物，该组合物含有数均粒径为10-300nm，长宽比为10-300的片状无机物，其中该材料具有 相对于周围温度变化小的热膨胀系数可以适用于显示装置的基板，从而克服了使用常规材料的显示装置的基板的缺点，即基板和透明电极之间的热收缩差异导致透明电极中的裂纹 导致电阻增加并导致断开，并且还可以提供具有高耐久性的显示装置。
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公开(公告)号：US20090324922A1
公开(公告)日：2009-12-31
申请号：US12373977
申请日：2007-07-20
申请人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
发明人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
CPC分类号： B82Y30/00 , C08G63/21 , C08J5/005 , C08J5/18 , C08J2333/04 , C08J2367/07 , C08L51/10 , C09D151/10 , C08L2666/02
摘要： The invention provides a transparent composite material comprising a cured product of a three-dimensionally crosslinkable resin composition containing tabular inorganic substance having a number-average particle size of 10 to 300 nm and an aspect ratio of 10 to 300 dispersed therein, which material has a small coefficient of thermal expansion against surrounding temperature changes and can be suitably applicable as substrate for display devices, to thereby overcome disadvantages in substrate for display devices using conventional materials that differences in thermal shrinkage between a substrate and an transparent electrode cause cracks in the transparent electrode, resulting in increasing resistance and causing disconnection, and further can provide a display device with high durability.
摘要翻译： 本发明提供了一种透明复合材料，其包含三维可交联树脂组合物的固化产物，该组合物含有数均粒径为10-300nm，长宽比为10-300的片状无机物，其中该材料具有 相对于周围温度变化小的热膨胀系数可以适用于显示装置的基板，从而克服了使用常规材料的显示装置的基板的缺点，即基板和透明电极之间的热收缩差异导致透明电极中的裂纹 导致电阻增加并导致断开，并且还可以提供具有高耐久性的显示装置。
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公开(公告)号：US08119039B2
公开(公告)日：2012-02-21
申请号：US12296245
申请日：2007-04-05
申请人： Yasushi Kadowaki , Kazufumi Kai
发明人： Yasushi Kadowaki , Kazufumi Kai
IPC分类号： H01B1/06
CPC分类号： C08J5/18 , C08J2367/06 , C08J2367/07 , Y10T428/31663 , Y10T428/31667 , Y10T442/3415
摘要： A transparent conductive substrate using allyl ester heat-curable resin, including a compound having a group represented by formula (2) as terminus and a group represented by formula (3) as repeating unit, where R3, A2, and A3 in the formulae have the same meanings as defined in the specification.
摘要翻译： 使用具有由式（2）表示的基团作为末端的化合物和由式（3）表示的基团作为重复单元的烯丙基酯热固性树脂的透明导电基材，其中式中的R3，A2和A3具有 与本说明书中定义的含义相同。
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公开(公告)号：US20090166589A1
公开(公告)日：2009-07-02
申请号：US12296245
申请日：2007-04-05
申请人： Yasushi Kadowaki , Kazufumi Kai
发明人： Yasushi Kadowaki , Kazufumi Kai
IPC分类号： H01B1/12
CPC分类号： C08J5/18 , C08J2367/06 , C08J2367/07 , Y10T428/31663 , Y10T428/31667 , Y10T442/3415
摘要： The invention provides a transparent conductive substrate using allyl ester heat-curable resin, comprising a compound having a group represented by formula (2) as terminus and a group represented by formula (3) as repeating unit, (In the formulae, R3 A2 and A3 have the same meanings as defined in the Description). The transparent conductive substrate is useful as a plastic substrate for display device, characterized by excellent heat resistance and chemical resistance, a low average linear expansion coefficient and high transparency, where warpage, deformation, crack of wiring are hard to occur in a process of thin film device formation.
摘要翻译： 本发明提供一种使用烯丙基酯热固性树脂的透明导电性基材，其包含具有式（2）表示的基团作为末端的化合物和由式（3）表示的基团作为重复单元）（式中，R3A2和 A3具有与说明中定义相同的含义）。 透明导电性基板作为显示装置的塑料基板是有用的，其特征在于优异的耐热性和耐化学性，低平均线膨胀系数和高透明度，其中在薄的过程中难以发生翘曲，变形，布线裂纹 胶片装置形成。
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9.发明授权Production process of 3-alkoxy-1-propanols, and 3-alkoxy-1-propanols obtained by the production process 失效通过制备方法得到的3-烷氧基-1-丙醇和3-烷氧基-1-丙醇的制备方法公开(公告)号：US07754926B2
公开(公告)日：2010-07-13
申请号：US10588085
申请日：2005-02-04
CPC分类号： C07C41/06 , C07C29/10 , C07C31/205 , C07C43/13 , C07C43/178
摘要： The present invention reacts an allyl alcohol with an alcohol compound in the presence of a catalyst containing at least one element selected from the group consisting of elements of the group III, lanthanoid elements and actinoid elements of the Periodic Table, as depicted in the following reaction and provides a method for efficiently producing 3-alkoxy-1-propanol in a single step using an alcohol as a starting material.
摘要翻译： 本发明在含有选自元素周期表第III族，镧系元素和锕系元素中的至少一种元素的催化剂存在下，使烯丙醇与醇化合物反应，如下述反应 并且提供了使用醇作为原料在一个步骤中有效生产3-烷氧基-1-丙醇的方法。
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10.发明授权Catalyst for producing both end-hydroxyl group-terminated diols, process for producing the catalyst, process for producing the diols by using the catalyst, and both end-hydroxyl group-terminated diols obtained by the process 失效用于制备端羟基封端的二醇的催化剂，用于制备催化剂的方法，通过使用催化剂制备二醇的方法，以及通过该方法获得的端羟基封端的二醇公开(公告)号：US07230145B2
公开(公告)日：2007-06-12
申请号：US10876687
申请日：2004-06-28
申请人： Yasushi Kadowaki , Masato Kaneda , Hiroshi Uchida
发明人： Yasushi Kadowaki , Masato Kaneda , Hiroshi Uchida
IPC分类号： C07C29/151 , C07C29/15 , C07C31/20
CPC分类号： B01J37/0201 , B01J21/08 , B01J23/70 , B01J23/75 , B01J23/755 , B01J25/00 , B01J25/02 , C07C29/132 , C07C31/205
摘要： A process for producing a both end-hydroxyl group-terminated diol, wherein an epoxy alcohol represented by the general formula (1) is subjected to a hydrogenolysis reaction in the presence of a catalyst for producing both end-hydroxyl group terminated diols, which catalyst contains at least one element selected from the group consisting of Group V elements, Group VI elements, Group VII elements, Group VIII elements, Group IX elements, Group X elements, and Group XI elements in the periodic table, in the presence of at least one solvent selected from the group consisting of ethers, esters, aromatic hydrocarbon compounds, alicyclic hydrocarbon compounds and aliphatic hydrocarbon compounds, to thereby obtain a both end-hydroxyl group-terminated diol represented by general formula (2). General formula (1) and (2) are as described in the specification.
摘要翻译： 在用于制备端羟基封端的二醇的催化剂的存在下，将由通式（1）表示的环氧醇进行氢解反应的两末端羟基封端的二醇的制备方法，该催化剂 包含至少一种选自元素周期表中的V族元素，VI族元素，VII族元素，VIII族元素，IX族元素，X族元素和XI族元素的元素， 一种选自醚，酯，芳烃化合物，脂环族烃化合物和脂族烃化合物的溶剂，从而获得由通式（2）表示的两端羟基封端的二醇。 通式（1）和（2）如说明书中所述。
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