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公开(公告)号：US20110040015A1
公开(公告)日：2011-02-17
申请号：US12937844
申请日：2009-04-13
申请人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
发明人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
CPC分类号： C08F299/0492 , C01B33/44 , H01L31/0392 , Y02E10/50
摘要： This invention relates to a method for producing a transparent composite material comprising a first step of subjecting a synthetic smectite having a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300 to organizing treatment with an organic quaternary ammonium salt and/or an organic quaternary phosphonium salt; a second step of mixing the synthetic smectite subjected to organizing treatment and a curable resin to prepare a resin composition containing the synthetic smectite in an amount of 10 to 40 mass %; a third step of curing the resin composition to obtain a cured product; and a forth step of removing the organic volatile components remaining in the cured product. According to the method, a transparent composite material which is flexible and has a low coefficient of thermal expansion can be obtained which is reduced in outgassing at high temperature under vacuum as in vapor deposition of a conductive thin film.
摘要翻译： 本发明涉及一种透明复合材料的制造方法，其特征在于，包括：将数均粒径为10〜300nm，纵横比为10〜300的合成蒙脱石进行有机季铵化处理的第1工序 盐和/或有机季鏻盐; 混合经过组织处理的合成蒙皂石和固化性树脂的第二步骤，制备含有10〜40质量％的合成蒙皂石的树脂组合物; 固化树脂组合物以获得固化产物的第三步骤; 以及除去保留在固化物中的有机挥发成分的第四工序。 根据该方法，可以获得柔性且具有低热膨胀系数的透明复合材料，这在真空下在高温下在导电薄膜的气相沉积中减少脱气。
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公开(公告)号：US08163842B2
公开(公告)日：2012-04-24
申请号：US12937844
申请日：2009-04-13
申请人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
发明人： Yasushi Kadowaki , Kenji Shimamura , Ryoji Toita
IPC分类号： C08L83/02
CPC分类号： C08F299/0492 , C01B33/44 , H01L31/0392 , Y02E10/50
摘要： This invention relates to a method for producing a transparent composite material comprising a first step of subjecting a synthetic smectite having a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300 to organizing treatment with an organic quaternary ammonium salt and/or an organic quaternary phosphonium salt; a second step of mixing the synthetic smectite subjected to organizing treatment and a curable resin to prepare a resin composition containing the synthetic smectite in an amount of 10 to 40 mass %; a third step of curing the resin composition to obtain a cured product; and a forth step of removing the organic volatile components remaining in the cured product. According to the method, a transparent composite material which is flexible and has a low coefficient of thermal expansion can be obtained which is reduced in outgassing at high temperature under vacuum as in vapor deposition of a conductive thin film.
摘要翻译： 本发明涉及一种透明复合材料的制造方法，该方法包括：将数均粒径为10〜300nm，长径比为10〜300的合成蒙脱石进行有机季铵化处理的第1工序 盐和/或有机季鏻盐; 混合经过组织处理的合成蒙皂石和固化性树脂的第二步骤，制备含有10〜40质量％的合成蒙皂石的树脂组合物; 固化树脂组合物以获得固化产物的第三步骤; 以及除去保留在固化物中的有机挥发成分的第四工序。 根据该方法，可以获得柔性且具有低热膨胀系数的透明复合材料，这在真空下在高温下在导电薄膜的气相沉积中减少脱气。
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公开(公告)号：US08460501B2
公开(公告)日：2013-06-11
申请号：US12937939
申请日：2009-04-13
申请人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
发明人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
CPC分类号： H01M14/005 , C08J5/18 , C08J2333/06 , H01L31/0392 , H01L31/03926 , H01L31/048 , Y02E10/50 , Y10T428/31935
摘要： This invention relates to a method for producing a cured film, which comprises a first step of applying a curable resin composition onto a surface of a first substrate and a surface of a second substrate respectively; a second step of bonding the curable resin composition layers provided on each surface of the first and second substrates to each other; and a third step of curing the curable resin composition layer between the first and the second substrates. The present invention enables production of a cured film in which the amount of thermal deformation such as warpage upon heating/cooling is suppressed, and the film can be suitably used as a plastic substrate for a display such as a liquid crystal display device and an organic EL display device, a substrate for a display, such as a substrate for electronic paper and the like, and a substrate for a solar cell.
摘要翻译： 本发明涉及一种固化膜的制造方法，该方法包括：分别在第一基板和第二基板的表面上施加固化性树脂组合物的第一工序; 将设置在第一和第二基板的每个表面上的可固化树脂组合物层彼此接合的第二步骤; 以及在所述第一和第二基板之间固化所述可固化树脂组合物层的第三步骤。 本发明能够制造其中热变形如加热/冷却时的翘曲量被抑制的固化膜的生产，并且该膜可以适合用作液晶显示装置和有机物等显示器的塑料基板 EL显示装置，用于电子纸等的显示器用基板和太阳能电池用基板。
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公开(公告)号：US20110039117A1
公开(公告)日：2011-02-17
申请号：US12937939
申请日：2009-04-13
申请人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
发明人： Yasushi Kadowaki , Ryoji Toita , Kenji Shimamura
CPC分类号： H01M14/005 , C08J5/18 , C08J2333/06 , H01L31/0392 , H01L31/03926 , H01L31/048 , Y02E10/50 , Y10T428/31935
摘要： This invention relates to a method for producing a cured film, which comprises a first step of applying a curable resin composition onto a surface of a first substrate and a surface of a second substrate respectively; a second step of bonding the curable resin composition layers provided on each surface of the first and second substrates to each other; and a third step of curing the curable resin composition layer between the first and the second substrates. The present invention enables production of a cured film in which the amount of thermal deformation such as warpage upon heating/cooling is suppressed, and the film can be suitably used as a plastic substrate for a display such as a liquid crystal display device and an organic EL display device, a substrate for a display, such as a substrate for electronic paper and the like, and a substrate for a solar cell.
摘要翻译： 本发明涉及一种固化膜的制造方法，该方法包括：分别在第一基板和第二基板的表面上施加固化性树脂组合物的第一工序; 将设置在第一和第二基板的每个表面上的可固化树脂组合物层彼此接合的第二步骤; 以及在所述第一和第二基板之间固化所述可固化树脂组合物层的第三步骤。 本发明能够制造其中热变形如加热/冷却时的翘曲量被抑制的固化膜的生产，并且该膜可以适合用作液晶显示装置和有机物等显示器的塑料基板 EL显示装置，用于电子纸等的显示器用基板和太阳能电池用基板。
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公开(公告)号：US20090324922A1
公开(公告)日：2009-12-31
申请号：US12373977
申请日：2007-07-20
申请人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
发明人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
CPC分类号： B82Y30/00 , C08G63/21 , C08J5/005 , C08J5/18 , C08J2333/04 , C08J2367/07 , C08L51/10 , C09D151/10 , C08L2666/02
摘要： The invention provides a transparent composite material comprising a cured product of a three-dimensionally crosslinkable resin composition containing tabular inorganic substance having a number-average particle size of 10 to 300 nm and an aspect ratio of 10 to 300 dispersed therein, which material has a small coefficient of thermal expansion against surrounding temperature changes and can be suitably applicable as substrate for display devices, to thereby overcome disadvantages in substrate for display devices using conventional materials that differences in thermal shrinkage between a substrate and an transparent electrode cause cracks in the transparent electrode, resulting in increasing resistance and causing disconnection, and further can provide a display device with high durability.
摘要翻译： 本发明提供了一种透明复合材料，其包含三维可交联树脂组合物的固化产物，该组合物含有数均粒径为10-300nm，长宽比为10-300的片状无机物，其中该材料具有 相对于周围温度变化小的热膨胀系数可以适用于显示装置的基板，从而克服了使用常规材料的显示装置的基板的缺点，即基板和透明电极之间的热收缩差异导致透明电极中的裂纹 导致电阻增加并导致断开，并且还可以提供具有高耐久性的显示装置。
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公开(公告)号：US08518524B2
公开(公告)日：2013-08-27
申请号：US12373977
申请日：2007-07-20
申请人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
发明人： Yasushi Kadowaki , Kazufumi Kai , Ryoji Toita
CPC分类号： B82Y30/00 , C08G63/21 , C08J5/005 , C08J5/18 , C08J2333/04 , C08J2367/07 , C08L51/10 , C09D151/10 , C08L2666/02
摘要： The invention provides a transparent composite material comprising a cured product of a three-dimensionally crosslinkable resin composition containing tabular inorganic substance having a number-average particle size of 10 to 300 nm and an aspect ratio of 10 to 300 dispersed therein, which material has a small coefficient of thermal expansion against surrounding temperature changes and can be suitably applicable as substrate for display devices, to thereby overcome disadvantages in substrate for display devices using conventional materials that differences in thermal shrinkage between a substrate and an transparent electrode cause cracks in the transparent electrode, resulting in increasing resistance and causing disconnection, and further can provide a display device with high durability.
摘要翻译： 本发明提供了一种透明复合材料，其包含三维可交联树脂组合物的固化产物，该组合物含有数均粒径为10-300nm，长宽比为10-300的片状无机物，其中该材料具有 相对于周围温度变化小的热膨胀系数可以适用于显示装置的基板，从而克服了使用常规材料的显示装置的基板的缺点，即基板和透明电极之间的热收缩差异导致透明电极中的裂纹 导致电阻增加并导致断开，并且还可以提供具有高耐久性的显示装置。
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公开(公告)号：US20100292378A1
公开(公告)日：2010-11-18
申请号：US12864109
申请日：2009-01-30
申请人： Ryoji Toita , Kenji Shimamura
发明人： Ryoji Toita , Kenji Shimamura
CPC分类号： C08K9/04 , H01L31/0392 , H01L31/03926 , Y02E10/50 , C08L67/07
摘要： This invention relates to: (1) a transparent composite material comprising a cured product of a resin composition having from 60 to 90% by mass of a vinyl ester resin composition which has a vinyl ester resin being synthesized from an aliphatic epoxy compound and from 10 to 40% by mass of synthetic smectite that is organized with a quaternary ammonium salt and/or a quaternary phosphonium salt and has a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300, the composition being cured, (2) a method for producing the transparent composite material, wherein the raw material composition for the composite material before curing is cured with an electron beam (EB), an ultraviolet ray (UV) or heat, and (3) a display device and a substrate for a solar cell comprising the transparent composite material as a substrate.
摘要翻译： 本发明涉及：（1）一种透明复合材料，其包含具有60〜90质量％的由脂肪族环氧化合物合成的乙烯基酯树脂和10重量份的乙烯基酯树脂组合物的树脂组合物的固化物， 至40质量％的由季铵盐和/或季鏻盐组成的数均粒径为10〜300nm，纵横比为10〜300的合成蒙脱石，组合物固化 （2）一种透明复合材料的制造方法，其中，将固化前的复合材料的原料组合物用电子束（EB），紫外线（UV）或热固化，（3）显示装置 以及包含该透明复合材料作为基板的太阳能电池用基板。
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公开(公告)号：US20120034397A1
公开(公告)日：2012-02-09
申请号：US13260716
申请日：2010-03-26
申请人： Miyo Mukobayashi , Ryoji Toita
发明人： Miyo Mukobayashi , Ryoji Toita
CPC分类号： C08F2/44 , C08F299/028 , C08F2220/281 , C08G59/24 , C08G59/42 , C08J7/18 , C08J2463/10 , C08L33/14 , C08L63/10 , G02F1/133305 , Y10T428/1086 , Y10T428/25
摘要： This invention relates to a transparent composite material having a low linear expansion coefficient and excellent transparency, flexibility and workability, which is formed by curing a resin composition containing epoxy(meth)acrylate synthesized from lactone modified (meth)acrylate, acid anhydride and epoxy resin, in which 10 to 55% by mass of synthetic smectite that is organized with a quaternary ammonium salt and/or a quaternary phosphonium salt and has a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300 is dispersed; and a transparent composite sheet using the material.
摘要翻译： 本发明涉及通过使由内酯改性（甲基）丙烯酸酯，酸酐和环氧树脂合成的环氧（甲基）丙烯酸酯）的树脂组合物固化而形成的具有低线膨胀系数和优异的透明性，柔软性和可加工性的透明复合材料 ，其中使用季铵盐和/或季鏻盐组合的数均粒径为10〜300nm，纵横比为10〜300的合成蒙脱石为10〜55质量％ 分散的 和使用该材料的透明复合片材。
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公开(公告)号：US20120022191A1
公开(公告)日：2012-01-26
申请号：US13260718
申请日：2010-03-26
申请人： Ryoji Toita , Miyo Mukobayashi
发明人： Ryoji Toita , Miyo Mukobayashi
CPC分类号： C08F2/44 , C08F299/065 , C08G18/672 , C08J7/18 , C08K3/346 , C08K2201/016 , C08L75/16 , C09J151/08 , G02F1/133305 , G02F2201/54 , C08G18/44
摘要： This invention relates to a transparent composite material having a low coefficient of liner thermal expansion and excellent transparency and flexibility, which is formed by curing a resin composition containing urethane (meth)acrylate, in which 10 to 40% by mass of synthetic smectite that is organized with a quaternary ammonium salt and/or a quaternary phosphonium salt and has a number average particle diameter of from 10 to 300 nm and an aspect ratio of from 10 to 300 is dispersed; and a transparent composite sheet using the material.
摘要翻译： 本发明涉及通过固化含有氨基甲酸酯（甲基）丙烯酸酯的树脂组合物而形成的具有低内衬热膨胀系数和优异的透明性和柔软性的透明复合材料，其中10〜40质量％的合成蒙皂石为 用季铵盐和/或季鏻盐组合，其数均粒径为10〜300nm，纵横比为10〜300分散; 和使用该材料的透明复合片材。
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