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1.发明公开公开(公告)号：US20230172876A1
公开(公告)日：2023-06-08
申请号：US17946485
申请日：2022-09-16
发明人： Xinde Xu , Bin Shao , Yongjian Peng , Shengnan Wang
IPC分类号： A61K31/122 , C07C403/24 , A61K36/71 , A61Q19/00 , A23K20/179 , A23L33/105 , A61K8/9789
CPC分类号： A61K31/122 , C07C403/24 , A61K36/71 , A61Q19/00 , A23K20/179 , A23L33/105 , A61K8/9789 , A61K2800/10 , A61K2800/43 , C07C2601/16 , C07C2601/14 , A61K2236/33 , A61K2236/37 , A61K2236/51 , A61K2236/53
摘要： The present invention provides a high-content carotenoid compound from Adonis amurensis. The content of the total carotenoid of the carotenoid compound is higher than 95%. The content of all-trans (3S, 3′S)-carotenoid is higher than 80%. The carotenoid crystals have a high purity, and can be used in multiple forms in the fields of a dietary supplement of a human being, a food additive, a feed additive and a cosmetic product. In addition, the present invention also provides a method for manufacturing the compound.
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公开(公告)号：US11180445B2
公开(公告)日：2021-11-23
申请号：US15519552
申请日：2015-10-12
发明人： Yongjian Peng , Xinde Xu , Jinping Ma , Yanwen Zhang , Bin Shao
IPC分类号： C07C273/16 , C07C7/152 , C11C3/00 , C07C57/12 , C07C7/14 , C07C51/43 , C07C51/487
摘要： The present invention discloses a method for recycling urea in the process of separating and purifying unsaturated substances through a urea adduction method. The method comprises the following steps: liposoluble substances containing target unsaturated components are used as raw materials, and subjected to urea adduction, crystallization and filtration to produce a filtrate, from which the specific unsaturated components are obtained; the urea adduct is dissolved in a polar solvent, and after the adducted adducts are layered and released, adding a certain solvent to the urea solution to adjust the polarity, then cooling for crystallization, and recycling the urea. The method can realize complete release of the adducted components and recycling and reuse of urea, and the process is simple, the recovery rate is high, and the adduction effect is not influenced when recycling urea for reuse, and the production cost of the urea adduct is reduced, thus alleviating the adverse impact of urea discharges on the environment.
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公开(公告)号：US10011550B2
公开(公告)日：2018-07-03
申请号：US15511135
申请日：2015-09-17
发明人： Yongjian Peng , Xinde Xu , Bin Shao , Lihua Zhang
CPC分类号： C07C51/09 , C07C67/02 , C11B7/0041 , C11B7/0058 , C11C1/08 , C11C1/10 , C11C3/003 , C11C3/10 , G01N30/02 , G01N2030/027
摘要： A method for preparing high-content conjugated linoleic acid (CLA) through purification of vegetable oil includes alcoholysis, purification and isomerization of vegetable oil. Alcoholysis is for preparing corresponding methyl ester or ethyl ester with glyceride; purification of methyl ester or ethyl ester is for obtaining methyl linoleate or ethyl linoleate of content over 85% through silver-based silica gel column chromatography; high-content CLA is obtained after alkali-catalyzed conjugation of methyl linoleate or ethyl linoleate, and CLA products are prepared as needed. This invention changes the status quo of preparing high-content CLA with safflower oil alone, expands sources of CLA, and develops an efficient technology for separation and purification of linoleic acid. The CLA obtained is of high purity and meets applications in pharmaceutical, health care products and other industries.
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公开(公告)号：US20170240507A1
公开(公告)日：2017-08-24
申请号：US15519552
申请日：2015-10-12
发明人： Yongjian Peng , Xinde Xu , Jinping Ma , Yanwen Zhang , Bin Shao
IPC分类号： C07C273/16 , C07C7/14 , C07C7/152 , C07C51/43 , C07C51/487
CPC分类号： C07C273/16 , C07C7/14 , C07C7/152 , C07C51/43 , C07C51/487 , C07C57/12 , C11C3/00 , Y02P20/582
摘要： The present invention discloses a method for recycling urea in the process of separating and purifying unsaturated substances through a urea adduction method. The method comprises the following steps: liposoluble substances containing target unsaturated components are used as raw materials, and subjected to urea adduction, crystallization and filtration to produce a filtrate, from which the specific unsaturated components are obtained; the urea adduct is dissolved in a polar solvent, and after the adducted adducts are layered and released, adding a certain solvent to the urea solution to adjust the polarity, then cooling for crystallization, and recycling the urea. The method can realize complete release of the adducted components and recycling and reuse of urea, and the process is simple, the recovery rate is high, and the adduction effect is not influenced when recycling urea for reuse, and the production cost of the urea adduct is reduced, thus alleviating the adverse impact of urea discharges on the environment.
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