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    DEVICE AND METHOD FOR EVALUATING ORGANIC MATERIAL FOR ORGANIC SOLAR CELL
    1.
    发明申请
    DEVICE AND METHOD FOR EVALUATING ORGANIC MATERIAL FOR ORGANIC SOLAR CELL 有权
    用于评估有机太阳能电池有机材料的装置和方法

    公开(公告)号：US20140213800A1

    公开(公告)日：2014-07-31

    申请号：US14126683

    申请日：2012-06-21

    申请人： Zhenfeng Zhang ,  Tsuneo Imamoto ,  Ken Tamura

    发明人： Zhenfeng Zhang ,  Tsuneo Imamoto ,  Ken Tamura

    IPC分类号： C07F9/28

    CPC分类号： C07F9/28 ,  C07B53/00 ,  C07C231/18 ,  C07F9/65517 ,  C07F15/0073 ,  C07C233/47

    摘要： Provided are a novel 1,2-bis(dialkylphosphino)-4,5-(methylenedioxy)benzene derivative that forms a metal complex having particularly high asymmetry induction capacity and catalytic activity on β-dehydroamino acids, a method for manufacturing the same, a metal complex having this 1,2-bis(dialkylphosphino)-4,5-(methylenedioxy)benzene derivative as a ligand, and an asymmetric hydrogenation method using this metal complex. A 1,2-bis(dialkylphosphino)-4,5-(methylenedioxy)benzene derivative represented by general formula (1). (In the formula, R1 and R2 represent an alkyl group having 1-10 carbon atoms, and R1 and R2 have different numbers of carbon atoms.)

    摘要翻译： 提供了形成具有特别高的不对称诱导能力和对 - 脱氨基酸的催化活性的金属络合物的新型1,2-双（二烷基膦基）-4,5-（亚甲二氧基）苯衍生物，其制造方法， 具有该1,2-二（二烷基膦基）-4,5-（亚甲二氧基）苯衍生物作为配体的金属络合物和使用该金属络合物的不对称氢化法。 由通式（1）表示的1,2-双（二烷基膦基）-4,5-（亚甲二氧基）苯衍生物。 （式中，R 1，R 2表示碳原子数1〜10的烷基，R 1和R 2的碳原子数不同。）

    Device and method for evaluating organic material for organic solar cell
    2.
    发明授权
    Device and method for evaluating organic material for organic solar cell 有权
    有机太阳能电池有机材料评估装置及方法

    公开(公告)号：US09029571B2

    公开(公告)日：2015-05-12

    申请号：US14126683

    申请日：2012-06-21

    申请人： Zhenfeng Zhang ,  Tsuneo Imamoto ,  Ken Tamura

    发明人： Zhenfeng Zhang ,  Tsuneo Imamoto ,  Ken Tamura

    IPC分类号： C07F9/28 ,  C07F9/655 ,  C07B53/00 ,  C07F15/00 ,  C07C231/18

    CPC分类号： C07F9/28 ,  C07B53/00 ,  C07C231/18 ,  C07F9/65517 ,  C07F15/0073 ,  C07C233/47

    摘要： Provided are a novel 1,2-bis(dialkylphosphino)-4,5-(methylenedioxy)benzene derivative that forms a metal complex having particularly high asymmetry induction capacity and catalytic activity on β-dehydroamino acids, a method for manufacturing the same, a metal complex having this 1,2-bis(dialkylphosphino)-4,5-(methylenedioxy)benzene derivative as a ligand, and an asymmetric hydrogenation method using this metal complex. A 1,2-bis(dialkylphosphino)-4,5-(methylenedioxy)benzene derivative represented by general formula (1). (In the formula, R1 and R2 represent an alkyl group having 1-10 carbon atoms, and R1 and R2 have different numbers of carbon atoms.)

    摘要翻译： 提供了形成具有特别高的不对称诱导能力和对 - 脱氨基酸的催化活性的金属络合物的新型1,2-双（二烷基膦基）-4,5-（亚甲二氧基）苯衍生物，其制造方法， 具有该1,2-二（二烷基膦基）-4,5-（亚甲二氧基）苯衍生物作为配体的金属络合物和使用该金属络合物的不对称氢化法。 由通式（1）表示的1,2-双（二烷基膦基）-4,5-（亚甲二氧基）苯衍生物。 （式中，R 1，R 2表示碳原子数1〜10的烷基，R 1和R 2的碳原子数不同。）

    2, 2'-BIS (DIALKYLPHOSPHINO) BIPHENYL COMPOUND, PRODUCTION METHOD THEREOF, AND METAL COMPLEX COMPRISING THE COMPOUND AS LIGAND
    3.
    发明申请
    2, 2'-BIS (DIALKYLPHOSPHINO) BIPHENYL COMPOUND, PRODUCTION METHOD THEREOF, AND METAL COMPLEX COMPRISING THE COMPOUND AS LIGAND 失效
    2，2-BIS（二乙基磷酰）联苯胺化合物，其生产方法和包含化合物的金属复合物

    公开(公告)号：US20100234626A1

    公开(公告)日：2010-09-16

    申请号：US12719252

    申请日：2010-03-08

    申请人： Ken Tamura ,  Masashi Sugiya ,  Tsuneo Imamoto

    发明人： Ken Tamura ,  Masashi Sugiya ,  Tsuneo Imamoto

    IPC分类号： C07F15/00 ,  C07F9/535

    CPC分类号： C07F15/008 ,  B01J31/2409 ,  B01J2231/645 ,  B01J2531/822 ,  C07F9/5027

    摘要： It is an object of the present invention to provide a novel phosphine compound capable of forming a metal complex useful as a catalyst for various asymmetric synthesis reactions, a production method thereof, and a metal complex comprising the aforementioned compound as a ligand.A 2,2′-bis(dialkylphosphino)biphenyl compound represented by the formula (A-1). A compound represented by the formula (1) is appropriate as a catalyst for an asymmetric synthesis reaction. The biphenyl compound represented by the formula (A-1) can be obtained by subjecting a compound represented by the formula (A-2) to a coupling reaction to obtain an intermediate represented by the formula (A-3), and then subjecting the intermediate to a deboranation reaction. In the formula (A-1), R1 and R2 each independently represent a C1-C10 alkyl group, R3 represents a monovalent substituent, and n represents an integer of 0 to 4. In the formula (1), R1 represents a C2-C10 alkyl group, R2 represents an alkyl group containing fewer carbon atoms than R1, R3 represents a monovalent substituent, and n represents an integer of 0 to 4.

    摘要翻译： 本发明的目的是提供能够形成可用作各种不对称合成反应的催化剂的金属络合物，其制备方法和包含上述化合物作为配体的金属络合物的新型膦化合物。 由式（A-1）表示的2,2'-双（二烷基膦基）联苯化合物。 由式（1）表示的化合物作为不对称合成反应的催化剂是合适的。 由式（A-1）表示的联苯化合物可以通过使式（A-2）表示的化合物进行偶联反应，得到式（A-3）表示的中间体，然后使 中间体到脱硼反应。 在式（A-1）中，R 1和R 2各自独立地表示C1-C10烷基，R3表示一价取代基，n表示0〜4的整数。式（1）中，R1表示C2- C10烷基，R2表示比R1少的碳原子的烷基，R3表示一价取代基，n表示0〜4的整数。

    METHOD FOR PRODUCING OPTICALLY ACTIVE 1,2-BIS(DIALKYLPHOSPHINO)BENZENE DERIVATIVE
    4.
    发明申请
    METHOD FOR PRODUCING OPTICALLY ACTIVE 1,2-BIS(DIALKYLPHOSPHINO)BENZENE DERIVATIVE 有权
    用于生产光学活性的1,2-双（对羟基苯基）苯甲醛衍生物的方法

    公开(公告)号：US20130172597A1

    公开(公告)日：2013-07-04

    申请号：US13808692

    申请日：2011-07-03

    申请人： Ken Tamura ,  Masashi Sugiya ,  Tsuneo Imamoto

    发明人： Ken Tamura ,  Masashi Sugiya ,  Tsuneo Imamoto

    IPC分类号： C07F9/54

    CPC分类号： C07F9/5449 ,  B01J31/2409 ,  B01J2231/645 ,  B01J2531/822 ,  C07B53/00 ,  C07B2200/07 ,  C07C67/303 ,  C07C231/12 ,  C07C231/18 ,  C07D207/337 ,  C07D307/54 ,  C07F9/5022 ,  C07F9/5027 ,  C07F15/0073 ,  C07C69/34 ,  C07C233/47

    摘要： An industrially advantageous method for producing an optically active 1,2-bis(dialkylphosphino)benzene derivative of the present invention is provided. The method is characterized in that a phosphine-borane compound represented by the following general formula (1) is subjected to a deboronation reaction, followed by lithiation, then the reaction product is subjected to reaction with an alkyldihalogenophosphine represented by RaPX′2, and thereafter the reaction product is subjected to reaction with a Grignard reagent represented by RbMgX″ to produce an optically active 1,2-bis(dialkylphosphino)benzene derivative (A). R1 and R2 respectively represent an alkyl group having 1 to 8 carbon atoms, and the number of carbon atoms is different between R1 and R2. Ra is either R1 or R2 and Rb is the other of R1 and R2. X, X′, and X″ each represent a halogen atom.

    摘要翻译： 提供了用于制备本发明的光学活性1,2-双（二烷基膦基）苯衍生物的工业上有利的方法。 该方法的特征在于将由以下通式（1）表示的膦 - 硼烷化合物进行脱硼反应，然后进行锂化，然后使反应产物与由RaPX'2表示的烷基二卤代膦反应，然后 使反应产物与由RbMgX“表示的格氏试剂反应，生成光学活性的1,2-双（二烷基膦基）苯衍生物（A）。 R1和R2分别表示碳原子数1〜8的烷基，R1和R2之间的碳原子数不同。 R a是R 1或R 2，R b是R 1和R 2中的另一个。 X，X'和X“各自表示卤素原子。

    Pressurized coal gasifier and coal gasification combined cycle power plant
    7.
    发明申请
    Pressurized coal gasifier and coal gasification combined cycle power plant 审中-公开
    加压煤气化炉和煤气化联合循环发电厂

    公开(公告)号：US20080115479A1

    公开(公告)日：2008-05-22

    申请号：US11600729

    申请日：2006-11-17

    申请人： Ken Tamura

    发明人： Ken Tamura

    IPC分类号： F02B43/00 ,  C10J3/68

    CPC分类号： C10J3/78 ,  C10J3/526 ,  C10J3/84 ,  C10J3/86 ,  C10J2300/093 ,  C10J2300/1606 ,  C10J2300/165 ,  C10J2300/1671 ,  C10J2300/1675 ,  C10K1/101 ,  Y02E20/16 ,  Y02E20/18 ,  Y02P20/13

    摘要： Provided is a pressurized coal gasifier in which a general low head pump can be used, abrasion damage of a control valve and pump due to flushing can be prevented and maintenance cost and device cost can be reduced. Also, provided is a coal gasification combined cycle power plant that can efficiently use gas generated by the pressurized coal gasifier for power generation. In a pressurized coal gasifier for thermally processing a coal material under pressure to be gasified, the gasifier having a bottom portion thereof provided with a water tank (4) for water-granulating a slag, the water tank being connected with one end of a feed water pipe (5) and one end of a drain pipe (6), the other ends of the feed water pipe and drain pipe are connected so as to communicate with each other to form a circulating channel (7) of closed system and the circulating channel is provided with a cooler (8) and circulating pump (9) of circulating water.

    摘要翻译： 提供一种加压煤气化炉，其中可以使用通用的低头泵，可以防止由于冲洗而导致的控制阀和泵的磨损，并且可以降低维护成本和装置成本。 另外，提供了一种能够有效地利用由加压煤气化炉产生的气体用于发电的煤气化联合循环发电厂。 在用于在加压气化的煤材中进行热处理的加压煤气化炉中，具有底部的气化器设置有水箱（4），用于对渣进行水粒化，水箱与进料的一端连接 水管（5）和排水管（6）的一端，供水管和排水管的另一端连接成相互连通，形成封闭系统的循环通道（7），循环 通道设置有循环水的冷却器（8）和循环泵（9）。

    Extractants for palladium and method of rapidly separating and recovering palladium using the same
    10.
    发明授权
    Extractants for palladium and method of rapidly separating and recovering palladium using the same 有权
    用于钯的萃取剂和使用其进行快速分离和回收钯的方法

    公开(公告)号：US07918918B2

    公开(公告)日：2011-04-05

    申请号：US12318824

    申请日：2009-01-09

    申请人： Hirokazu Narita ,  Mikiya Tanaka ,  Ken Tamura

    发明人： Hirokazu Narita ,  Mikiya Tanaka ,  Ken Tamura

    IPC分类号： C22B11/00 ,  C01G55/00 ,  C07C323/41

    CPC分类号： C07C323/60 ,  C22B3/0008 ,  C22B3/10 ,  C22B7/007 ,  C22B11/048 ,  Y02P10/214 ,  Y02P10/234

    摘要： Provided is a novel extractant for palladium capable of improving an extraction rate compared to the conventional extractant, DHS, and also capable of back-extracting palladium using an ammonia solution, and a method of separating and recovering palladium using the novel extractant. The present invention provides a method for obtaining an aqueous solution containing palladium only by: bringing an acidic aqueous solution containing at least palladium into contact with an organic solution containing a sulfide-containing monoamide as an active integredient represented by the following structural formula (I), where R1, R2, and R3 each represent a group selected from a chain hydrocarbon group having 1 to 18 carbon atoms which may be branched, an alicyclic hydrocarbon group having 1 to 10 carbon atoms, and an aromatic hydrocarbon group having 1 to 14 carbon atoms, and n represents an integer of 1 to 4; extracting palladium into the organic solution; and conducting the back-extraction of the palladium extracted in the organic solution to an aqueous solution using an ammonia solution.

    摘要翻译： 提供了一种新型的能够提高萃取速率的钯萃取剂，与常规萃取剂DHS相比，并且还能够使用氨溶液反萃取钯，以及使用新的萃取剂分离和回收钯的方法。 本发明提供一种获得含钯水溶液的方法，其方法是：使至少含有钯的酸性水溶液与含有硫化物的单酰胺作为活性成分的有机溶液接触，所述有机溶液为下述结构式（I）所示的活性成分， 其中R 1，R 2和R 3各自表示选自可具有支链的碳原子数1〜18的链状烃基，碳原子数1〜10的脂环族烃基和碳原子数1〜14的芳香族烃基 原子，n表示1〜4的整数。 将钯提取到有机溶液中; 并使用氨溶液将在有机溶液中提取的钯进行背萃取至水溶液。