摘要:
An immersion fixed bed reactor intensified by liquid flow contains a cylindrical tank internally installed with an annular cylindrical catalyst bed (ACCB) packed with solid catalysts is provided. The inner and outer walls of the ACCB are composed of two layers of stainless steel sheets with holes. The outer layer of stainless steel perforated with holes. The inner layer of catalyst contacting stainless steel is covered with stainless steel waved mesh in circumferential direction. The bottom of AACB is sealed with a steel plate by welding or a blind plate and the top of ACCB is fixed to cylindrical tank with a flange. The solid catalysts are packed in the ACCB.
摘要:
A process of integrated system formed by coupling of fixed bed, jetting floating bed, and separating unit, aimed to provide a new process and equipment of higher efficiency, which integrates multi-type reactors and separation is provided. Reaction materials undergo preliminary reaction in fixed bed reactor and intensified reaction in jetting floating bed reactor, and then separation in the subsequent separation system. Unreacted materials will be returned to the raw material intermediate storage tank for mixing with fresh materials, as raw materials for continued reaction. During this process, materials first pass the fixed bed reactor once to achieve certain conversion rate, and then enter the jetting floating bed reactor for intensified reaction. When the product reaches required concentration, the materials will enter subsequent separation equipment for separation.
摘要:
An anti-thermosensitization rectification tower comprising a rectification tower, a T-shaped condenser, a baffle plate, a tower bottom, a falling-film reboiler and a recirculation system, wherein the T-shaped condenser is secured exactly on the top of the rectification tower without any pipeline in between, and the circular baffle plate is installed in the T-shaped condenser; an annular sump located between the rectification tower and the T-shaped condenser for collecting the liquid condensed in the T-shaped condenser and channeling it out of the rectification tower into a liquid-collecting tank, and a centrifugal pump utilized to connect together the tower bottom and the falling-film reboiler to form a high-speed circulation system, wherein the tower bottom is an elongated conduit and the falling-film reboiler is in the form of a stout shell-and-tube heat exchanger is provided.
摘要:
A multiphase catalytic tower-shaped impinging-stream reactor in the form of a tower, the upper part of which is a plate or packed tower 4 and the lower part of which is a multiphase catalytic impinging-stream reaction kettle 2; the upper part and the lower part are separated by a flow channel plate 14 which has a plurality of round holes serving as flow channels 62; at the top of the reaction kettle 2 exists an upper ejector 3 and at the bottom of the reaction kettle 2 exists a lower ejector 8; near to the side wall of the reaction kettle 2 stands a baffle plate 5, which separates a static liquid zone within the reaction kettle 2 is disclosed.
摘要:
A multiphase catalytic tower-shaped impinging-stream reactor in the form of a tower, the upper part of which is a plate or packed tower 4 and the lower part of which is a multiphase catalytic impinging-stream reaction kettle 2; the upper part and the lower part are separated by a flow channel plate 14 which has a plurality of round holes serving as flow channels 62; at the top of the reaction kettle 2 exists an upper ejector 3 and at the bottom of the reaction kettle 2 exists a lower ejector 8; near to the side wall of the reaction kettle 2 stands a baffle plate 5, which separates a static liquid zone within the reaction kettle 2 is disclosed.
摘要:
An anti-thermosensitization rectification tower comprising a rectification tower, a T-shaped condenser, a baffle plate, a tower bottom, a falling-film reboiler and a recirculation system, wherein the T-shaped condenser is secured exactly on the top of the rectification tower without any pipeline in between, and the circular baffle plate is installed in the T-shaped condenser; an annular sump located between the rectification tower and the T-shaped condenser for collecting the liquid condensed in the T-shaped condenser and channeling it out of the rectification tower into a liquid-collecting tank, and a centrifugal pump utilized to connect together the tower bottom and the falling-film reboiler to form a high-speed circulation system, wherein the tower bottom is an elongated conduit and the falling-film reboiler is in the form of a stout shell-and-tube heat exchanger is provided.
摘要:
A green treatment process for cleaning exhaust gas generated in the air oxidation of benzene homologs is disclosed. It takes the hot pressurized exhaust gas generated in the benzene homolog air oxidation process as driving power and heating source: firstly, introducing the said exhaust gas into a turbine refrigerator so that it can drive the refrigerator to generate the cooling capacity that will be utilized for condensing the gas phase in the upper part of the flash evaporator and for trapping organics entrained in the exhaust gas; then, leading the exhaust gas with lowered temperature and pressure into corresponding heat exchangers to provide a part of heating source for the flash evaporator and to preheat the reaction raw materials. Furthermore, introducing the condensed exhaust gas into a water absorption scrubber for further removal of trace organics entrained therein.
摘要:
A green treatment process for cleaning exhaust gas generated in the air oxidation of benzene homologs is disclosed. It takes the hot pressurized exhaust gas generated in the benzene homolog air oxidation process as driving power and heating source: firstly, introducing the said exhaust gas into a turbine refrigerator so that it can drive the refrigerator to generate the cooling capacity that will be utilized for condensing the gas phase in the upper part of the flash evaporator and for trapping organics entrained in the exhaust gas; then, leading the exhaust gas with lowered temperature and pressure into corresponding heat exchangers to provide a part of heating source for the flash evaporator and to preheat the reaction raw materials. Furthermore, introducing the condensed exhaust gas into a water absorption scrubber for further removal of trace organics entrained therein.
摘要:
A catalytic reaction-rectification integrated process and a catalytic reaction-rectification integrated column (T-01), the specialized device of such process. The process comprises that the reactants are preheated and mixed with catalysts, and then fed into a jet agitation reaction section (6) located in the middle of the catalytic reaction-rectification integrated column (T-01) from a feeding inlet. The jet agitation reaction section (6) is a kettle-like reactor located in the middle of the catalytic reaction-rectification integrated column (T-01). After pressurized by a centrifugal pump (21), the reactant materials are admitted into a subsonic or transonic agitator (33) located within the reaction section (6). The reactant materials are ejected into the jet agitation reaction section (6) at high speed, to efficiently mix the solid and liquid phases in the reaction section (6) and to reinforce heat and mass transfer efficiency during the reaction. The liquid reaction mixture is separated and purified directly in the catalytic reaction-rectification integrated column (T-01). This process may be used for esterification, the production of alcohols from olefins and water, and the production of ethers from olefins and alcohols.
摘要:
A floating valve providing a parent-and-subsidiary flow-guided floating valve of low pressure drop, high throughput and highly flexible operation maintaining high efficiency within a wide range of gaseous load changes is disclosed. Furthermore, a parent-and-subsidiary flow-guided floating valve having at least two legs, wherein the body of the parent valve is a symmetrical plane figure with the central axis line as the symmetrical line, the central axis line to the overflow cofferdam along the direction in which the liquid flows is also provided.