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1.发明授权Colloidal dispersion of calcium phosphate tablets and method of obtaining the same 有权磷酸钙片剂的胶体分散体及其制备方法公开(公告)号：US07807724B2
公开(公告)日：2010-10-05
申请号：US10563167
申请日：2004-06-28
IPC分类号： B01J13/00
CPC分类号： C01B25/324 , B01J13/0013 , C01B25/32
摘要： The invention provides colloidal dispersions of calcium phosphate platelets comprising at least one polymer which complexes the calcium and in which the length of the platelets, L, is between 5 and 500 nm and in which the thickness of the platelets is between 0.5 and 20 nm.Another subject-matter of the invention is the calcium phosphate platelets obtained by drying the colloidal dispersion according to the invention.The invention also provides a process for preparing these colloidal dispersions of calcium phosphate platelets according to the invention.Finally, another subject-matter of the invention is the use of the abovementioned colloidal dispersions of platelets as food additive, reinforcing filler, thermal insulation filler, pharmaceutical excipient, polishing agent, building materials, additive for oral formulations, in particular dentifrices, or encapsulating agent.
摘要翻译： 本发明提供磷酸钙血小板的胶体分散体，其包含至少一种与钙复合的聚合物，其中血小板的长度L在5至500nm之间，其中血小板的厚度在0.5至20nm之间。 本发明的另一主题是通过干燥根据本发明的胶体分散体获得的磷酸钙血小板。 本发明还提供了制备本发明的磷酸钙血小板的这些胶体分散体的方法。 最后，本发明的另一主题是使用上述血小板的胶体分散体作为食品添加剂，增强填料，绝热填料，药物赋形剂，抛光剂，建筑材料，用于口服制剂的添加剂，特别是牙粉或包封 代理商
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2.发明授权Method of manufacturing hydroxyapatite and uses therefor in delivery of nucleic acids 有权制备羟基磷灰石的方法及其在核酸递送中的用途公开(公告)号：US07776600B2
公开(公告)日：2010-08-17
申请号：US11811992
申请日：2007-06-13
申请人： Prashant N. Kumta , Charles Sfeir , Jeffrey Owen Hollinger , Daiwon Chol , Lee Weiss , Phil Campbell
发明人： Prashant N. Kumta , Charles Sfeir , Jeffrey Owen Hollinger , Daiwon Chol , Lee Weiss , Phil Campbell
IPC分类号： C01B25/12 , A61L27/32 , A61F2/00 , A61K31/715 , C12N15/00
CPC分类号： C01B25/324
摘要： Provided is a method for production of nanocrystalline hydroxyapatite particles, and nanocrystalline hydroxyapatite particles produced according to the method. The nanocrystalline hydroxyapatite particles exhibit substantially superior cell transformation abilities as compared to known and commercially-available calcium phosphate kits. The nanocrystalline hydroxyapatite particles also find use in tissue engineering applications, for example bone and tooth engineering and repair applications.
摘要翻译： 本发明提供一种生产纳米晶体羟基磷灰石颗粒的方法和根据该方法制备的纳米晶体羟基磷灰石颗粒。 与已知和市售的磷酸钙试剂盒相比，纳米晶体羟基磷灰石颗粒表现出显着优异的细胞转化能力。 纳米晶体羟基磷灰石颗粒也用于组织工程应用，例如骨和牙齿工程和修复应用。
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公开(公告)号：US20070166217A1
公开(公告)日：2007-07-19
申请号：US10583735
申请日：2004-12-23
申请人： Mohamed Takhim
发明人： Mohamed Takhim
IPC分类号： C01B25/32
CPC分类号： C01B25/41 , C01B25/28 , C01B25/30 , C01B25/322 , C01B25/324 , C01B25/405
摘要： The inventive method for producing strong base phosphates consists in forming a pulp consisting of an aqueous phase which contains a water-soluble calcium phosphate and a solid impurity-containing phase, in separating said phases, transferring calcium ions to a liquid phase by a strong base ions associated with forming the aqueous solution of the pure phosphate(s) of said strong base and in precipitating a pure water-insoluble calcium phosphate. Said method also consists in mixing phosphoric ores and acid in such a way that a pasty triple superphosphate composition is obtained and in adding water thereto in order to produce said pulp.
摘要翻译： 用于生产强碱性磷酸盐的本发明的方法在于形成由含有水溶性磷酸钙和含固体杂质的相的水相组成的纸浆，在分离所述相中，通过强碱将钙离子转移到液相 与形成所述强碱的纯磷酸盐的水溶液和沉淀纯水不溶性磷酸钙有关的离子。 所述方法还包括以下方式混合磷矿石和酸，即获得糊状三重过磷酸钙组合物并向其中加入水以生产所述纸浆。
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公开(公告)号：US20070122326A1
公开(公告)日：2007-05-31
申请号：US10583344
申请日：2004-12-23
申请人： Mohamed Takhim
发明人： Mohamed Takhim
IPC分类号： C22B26/20
CPC分类号： C01B25/324 , C01B25/2212
摘要： The inventive method for etching phosphate ores involves a single-pass digesting of ores whose P2O5 content is greater than 20% in weight by at least 10% in weight of a hydrochloric aqueous acid solution associated with an etching solution formation and the separation of the insoluble solid phase and the aqueous phase of said etching solution. Said method consists in pre-neutralising the etching solution by a neutralising agent prior to said separation in such a way that the etching solution pH which is less than pH to which an important part of phosphate ions in solution precipitates in the form of calcium monohydrogen phosphate (DCP) is adjusted and in subsequently neutralising said separated aqueous phase in such a way that a pure DCP is precipitated.
摘要翻译： 用于蚀刻磷酸盐矿石的本发明的方法涉及矿石的单程消化，其中P 2 O 5 O 5含量大于20重量％，至少10重量％ 与蚀刻溶液形成相关的盐酸酸水溶液和所述蚀刻溶液的不溶性固相和水相的分离。 所述方法包括在所述分离之前通过中和剂预处理蚀刻溶液，使得蚀刻溶液pH小于pH，溶液中的重要部分磷酸根离子以磷酸一氢钙的形式沉淀 （DCP）并随后中和所述分离的水相，使得纯DCP沉淀。
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公开(公告)号：US06569396B1
公开(公告)日：2003-05-27
申请号：US09701193
申请日：2000-11-27
申请人： Shouhan Yanagi , Mamoru Senna , Tetsuhiko Isobe , Manabu Kanayama
发明人： Shouhan Yanagi , Mamoru Senna , Tetsuhiko Isobe , Manabu Kanayama
IPC分类号： C01B2532
CPC分类号： C01B25/32 , C01B25/324
摘要： The present invention provides a method of manufacturing calcium phosphate powder comprising the steps of preparing a mixed material by mixing calcium hydroxide (Ca(OH)2) powder and calcium hydrogenphosphate powder so that a molar ratio (Ca/P) of calcium to phosphor is set to a range of 1.45-1.72; conducting a mixing/milling treatment to the mixed material to cause a soft-mechanochemical compositing reaction thereby to prepare a calcium phosphate precursor; and conducting a heat treatment to thus obtained precursor at a temperature of 600° C. or more thereby to prepare calcium phosphate powder. According to the present invention, the manufacturing process is simple and the manufacturing cost can be remarkably reduced. In addition, fine calcium phosphate powder excellent in characteristics can be easily manufactured in a short time.
摘要翻译： 本发明提供一种磷酸钙粉末的制造方法，其特征在于，通过混合氢氧化钙（Ca（OH）2）粉末和磷酸氢钙粉末，使钙与磷的摩尔比（Ca / P）为 设定在1.45-1.72的范围内; 对混合材料进行混合/研磨处理以引起软化机械复合反应，从而制备磷酸钙前体; 在600℃以上的温度下进行如此得到的前体的热处理，制作磷酸钙粉末。 根据本发明，制造过程简单，制造成本显着降低。 另外，能够在短时间内容易地制造出特性优异的细小的磷酸钙粉末。
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公开(公告)号：US3427124A
公开(公告)日：1969-02-11
申请号：US3427124D
申请日：1965-06-18
发明人： BOYLAN DAVID R , FENG KUO KANG
CPC分类号： C01B25/324 , C05B11/08 , C05B11/10
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公开(公告)号：US1969951A
公开(公告)日：1934-08-14
申请号：US68897133
申请日：1933-09-11
申请人： SEYFRIED WARREN R
发明人： SEYFRIED WARREN R
CPC分类号： C05B11/12 , C01B25/324
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公开(公告)号：US20130338237A1
公开(公告)日：2013-12-19
申请号：US13993253
申请日：2010-12-31
申请人： Ahmet Cuneyt Tas
发明人： Ahmet Cuneyt Tas
CPC分类号： A61K47/02 , A61L24/02 , A61L27/12 , C01B25/322 , C01B25/324 , C01B25/325 , C01B25/385
摘要： Brushite (DCPD, dicalcium phosphate dihydrate, CaHPO4-2HH2O) and octacaicium phosphate (OCP, Ca8(HPO4)2(PO4)4-5H2O) granules in the millimetre size range were prepared by using calcium carbonate granules of marble-origin as the starting material. The method of the invention comprised of soaking the marble granules in aqueous solutions containing phosphate and/or calcium ions at temperatures between 20° and 75° C. The load-bearing DCPD and OCP granules of this invention are useful in maxillofacial and orthopedic void/bone defect filiing and grafting applications.
摘要翻译： 通过使用大理石原料的碳酸钙颗粒作为起始，制备了毫米尺寸范围内的褐铁矿（DCPD，磷酸二钙，CaHPO 4·2H 2 O）和磷酸八钙（OCP，Ca 8（HPO 4）2（PO 4） 材料。 本发明的方法包括将大理石颗粒浸泡在含有磷酸盐和/或钙离子的水溶液中，温度在20℃和75℃之间。本发明的承载DCPD和OCP颗粒可用于颌面和整形外科/ 骨缺损和移植应用。
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9.发明申请Colloidal dispersion of calcium phosphate tablets and method of obtaining the same 有权磷酸钙片剂的胶体分散体及其制备方法公开(公告)号：US20070179202A1
公开(公告)日：2007-08-02
申请号：US10563167
申请日：2004-06-28
CPC分类号： C01B25/324 , B01J13/0013 , C01B25/32
摘要： The invention provides colloidal dispersions of calcium phosphate platelets comprising at least one polymer which complexes the calcium and in which the length of the platelets, L, is between 5 and 500 nm and in which the thickness of the platelets is between 0.5 and 20 nm. Another subject-matter of the invention is the calcium phosphate platelets obtained by drying the colloidal dispersion according to the invention. The invention also provides a process for preparing these colloidal dispersions of calcium phosphate platelets according to the invention. Finally, another subject-matter of the invention is the use of the abovementioned colloidal dispersions of platelets as food additive, reinforcing filler, thermal insulation filler, pharmaceutical excipient, polishing agent, building materials, additive for oral formulations, in particular dentifrices, or encapsulating agent.
摘要翻译： 本发明提供磷酸钙血小板的胶体分散体，其包含至少一种与钙复合的聚合物，其中血小板的长度L在5至500nm之间，其中血小板的厚度在0.5至20nm之间。 本发明的另一主题是通过干燥根据本发明的胶体分散体获得的磷酸钙血小板。 本发明还提供了制备根据本发明的磷酸钙血小板的这些胶体分散体的方法。 最后，本发明的另一主题是使用上述血小板的胶体分散体作为食品添加剂，增强填料，绝热填料，药物赋形剂，抛光剂，建筑材料，用于口服制剂的添加剂，特别是牙粉，或包封 代理商
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10.发明授权Biocompatible cement containing reactive calcium phosphate nanoparticles and methods for making and using cement 失效含有反应性磷酸钙纳米粒子的生物相容性水泥及其制造和使用方法公开(公告)号：US07081161B2
公开(公告)日：2006-07-25
申请号：US10841885
申请日：2004-05-07
申请人： Brian R. Genge , Licia Wu , Glenn R. Sauer , Roy E. Wuthier , Ronald Genge
发明人： Brian R. Genge , Licia Wu , Glenn R. Sauer , Roy E. Wuthier , Ronald Genge
IPC分类号： C04B12/02
CPC分类号： C04B28/34 , A61K6/033 , A61K6/083 , A61L24/0063 , A61L24/0084 , A61L24/02 , C01B25/32 , C01B25/324 , C04B12/025 , C04B20/0036 , C04B28/344 , C04B28/346 , C04B2111/00189 , C04B2111/00637 , C04B2111/00836 , C08L33/02 , C04B22/10 , C04B22/16 , C04B24/2641 , C04B20/008 , C08L33/08 , C04B14/28
摘要： A cement powder is disclosed that contains reactive tricalcium phosphate nanoparticles and other ingredients required to form a cementous material. Methods of making the reactive tricalcium phosphate nanoparticles, the cement powder, the cement paste, and cured cement are also provided, as are methods and articles for using the cement.
摘要翻译： 公开了含有反应性磷酸三钙纳米颗粒和形成胶结材料所需的其它成分的水泥粉末。 还提供了制备反应性磷酸三钙纳米颗粒，水泥粉末，水泥浆和固化水泥的方法，以及使用该水泥的方法和制品。
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