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    TRANSAMINATION OF NITROGEN-CONTAINING COMPOUNDS TO HIGH MOLECULAR WEIGHT POLYALKYLENEAMINES
    4.
    发明申请
    TRANSAMINATION OF NITROGEN-CONTAINING COMPOUNDS TO HIGH MOLECULAR WEIGHT POLYALKYLENEAMINES 有权
    含氮化合物向高分子量聚氨基甲酸铵的分解

    公开(公告)号：US20130225864A1

    公开(公告)日：2013-08-29

    申请号：US13884477

    申请日：2011-10-20

    申请人： Stephen W. King

    发明人： Stephen W. King

    IPC分类号： C07C209/54

    CPC分类号： C07C209/54 ,  C07C209/64 ,  C07C211/14

    摘要： A process for preparing high molecular weight acyclic polyamines comprising providing a reaction mixture that includes at least a first component comprising a first organic, nitrogen-containing compound that contains at least two non-tertiary amine groups separated from one another by a ternary or higher carbon atom spacing that can be transaminated in the presence of a hydrogenation/dehydrogenation catalyst to form a mixture of higher molecular weight, acyclic polyamines while minimizing the formation of cyclic polyamines.

    摘要翻译： 一种制备高分子量无环多胺的方法，包括提供反应混合物，该反应混合物包括至少第一组分，其包含第一有机含氮化合物，其含有通过三元或更高碳彼此分离的至少两个非叔胺基团 原子间隔可以在氢化/脱氢催化剂存在下进行转氨以形成较高分子量的无环多胺的混合物，同时最小化环状多胺的形成。

    Process for the continuous preparation of 3,3'-dichloro-benzidine dihydrochloride
    5.
    发明授权
    Process for the continuous preparation of 3,3'-dichloro-benzidine dihydrochloride 失效
    连续制备3,3'-二氯苯胺二氯化物的方法

    公开(公告)号：US5208376A

    公开(公告)日：1993-05-04

    申请号：US856063

    申请日：1992-06-08

    申请人： Kurt Habig ,  Konrad Baessler ,  Klaus Warning

    发明人： Kurt Habig ,  Konrad Baessler ,  Klaus Warning

    IPC分类号： C07C209/42 ,  C07C209/54 ,  C07C211/52

    CPC分类号： C07C209/54

    摘要： A process for the continuous preparation of 3,3'-dichlorobenzidine dihydrochloride from 2,2'-dichlorohydrazobenzene by treatment with aqueous sulfuric acid, which comprises treating the 2,2'-dichlorohydrazobenzene, dissolved in a water-immiscible aromatic solvent, continuously at temperatures of from about 20.degree. to about 50.degree. C. in the presence of an alkali metal salt of an alkyl (C.sub.8 -C.sub.23)polyglycol ether sulfate, with such an amount of from about 50 to about 80 % strength aqueous sulfuric acid that the suspension formed remains conveyable, subsequently diluting the suspension emerging from the reaction zone with water, again continuously, and subsequently heating the suspension to a temperature of from about 90.degree. to about 95.degree. C. until a solution is obtained, separating off the aromatic solvent from the hot, sulfuric acid aqueous phase, and precipitating the 3,3'-dichlorobenzidine dihydrochloride by adding hydrochloric acid to the sulfuric acid solution which remains and filtering off this product.

    摘要翻译： PCT No.PCT / EP90 / 01844 Sec。 371日期：1992年6月8日 102（e）日期1992年6月8日PCT 1990年11月3日PCT PCT。 第WO91 / 07377号公报 日本1991年5月30日。一种通过用硫酸水溶液连续制备3,3'-二氯联苯胺二盐酸盐的方法，该方法包括处理溶于水中的2,2'-二氯代苯， 不饱和的芳族溶剂，在约20至约50℃的温度下，在烷基（C 8 -C 23）聚乙二醇醚硫酸盐的碱金属盐存在下，其量为约50至约80％ 形成的悬浮液的强度硫酸水溶液仍然是可输送的，随后再次用水稀释从反应区出来的悬浮液，随后将悬浮液加热到约90℃至约95℃的温度，直至获得溶液 ，从热硫酸水相中分离芳族溶剂，并通过向硫酸溶液中加入盐酸沉淀出3,3'-二氯联苯胺二盐酸盐，其中r 发出并过滤掉本产品。

    Process for preparing di(aminophenyl)methanes
    6.
    发明授权
    Process for preparing di(aminophenyl)methanes 失效
    制备二（氨基苯基）甲烷的方法

    公开(公告)号：US4039580A

    公开(公告)日：1977-08-02

    申请号：US598794

    申请日：1975-07-24

    申请人： Floro F. Frulla ,  Adnan A. R. Sayigh ,  Henri Ulrich ,  Peter J. Whitman

    发明人： Floro F. Frulla ,  Adnan A. R. Sayigh ,  Henri Ulrich ,  Peter J. Whitman

    IPC分类号： C08G12/00 ,  B01J21/00 ,  C07B61/00 ,  C07C67/00 ,  C07C209/00 ,  C07C209/54 ,  C07C209/60 ,  C07C209/78 ,  C07C211/50 ,  C07C211/53 ,  C07C241/00 ,  C07C265/14 ,  C08G12/08 ,  C08G18/76 ,  C07C85/08

    CPC分类号： C08G18/7664

    摘要： A process is described for the preparation of polymethylene polyphenyl polyamines containing from 40 to 60 percent by weight of diamine and also containing markedly less high molecular weight polyamines than products hitherto available. Phosgenation of the polyamines gives the corresponding mixture of polymethylene polyphenyl polyisocyanates of markedly lower viscosity and lighter color than products hitherto available, and yielding polymer foams which are substantially white in color.The process comprises condensing aniline and formaldehyde (molar ratio 4-10:1) in the absence of catalyst, separating water from the resulting aminal mixture, contacting the aminals at 20.degree. C to 60.degree. C with a solid catalyst (diatomaceous earths, clays, zeolites) until formation of benzylamines is substantially complete, distilling aniline from the resulting benzylamines under reduced pressure and below 150.degree. C until the aniline content is 3 to 22 percent by weight, and contacting the resulting product with a solid catalyst (diatomaceous earths, clays, zeolites) at 100.degree. C to 190.degree. C until conversion to polymethylene polyphenyl polyamines is complete.

    摘要翻译： 描述了一种制备含有40至60重量％二胺的聚亚甲基多苯基多胺的方法，并且与目前可获得的产品相比，含有显着较少的高分子量多胺。 多胺的光气化产生与目前可获得的产品相比显着低粘度和较浅颜色的聚亚甲基多苯基多异氰酸酯的相应混合物，并产生基本上为白色的聚合物泡沫。

    {66 {11 , {60 -adamantane acetic acid
    7.
    发明授权
    {66 {11 , {60 -adamantane acetic acid 失效
    {66 {11，{60 -ADAMANTANE ACETIC ACID

    公开(公告)号：US3624126A

    公开(公告)日：1971-11-30

    申请号：US3624126D

    申请日：1970-05-04

    申请人： SQUIBB & SONS INC

    发明人： NARAYANAN VENKATACHALA L

    IPC分类号： B01J19/12 ,  C07C53/138 ,  C07C57/28 ,  C07C67/00 ,  C07C209/00 ,  C07C209/50 ,  C07C209/54 ,  C07C211/19 ,  C07D209/58 ,  C07C61/28 ,  C07C69/74

    CPC分类号： C07D209/58 ,  C07C53/138 ,  C07C57/28

    摘要： 1-Azacyclopentano(1,2-a)adamantane compounds and derivatives thereof which have antiviral and anti-inflammatory properties and which are useful cardiovascular agents may be prepared starting from 2-adamantanones or substituted 2-adamantanones and proceeding through a series of intermediate compounds to the corresponding 1-azacyclopentano(1,2-a)-adamantanes. Derivatives may be obtained by reacting the latter with an alkyl or alkenyl halide, haloalkylamine or a haloalkyl substituted amine, a haloalkylcarboxylic acid, an aralkyl halide of up to 10 carbon atoms, or a haloalkyladamantylamine or haloalkyl substituted adamantylamine. The 2-adamantane alkylamine intermediates for the 1-azacyclopentano-(1,2-a)adamantane compounds also have antiviral and anti-inflammatory properties and are useful cardiovascular agents.

    Transamination of nitrogen-containing compounds to high molecular weight polyalkyleneamines
    9.
    发明授权
    Transamination of nitrogen-containing compounds to high molecular weight polyalkyleneamines 有权
    含氮化合物转化成高分子量聚亚烷基胺

    公开(公告)号：US09000217B2

    公开(公告)日：2015-04-07

    申请号：US13884477

    申请日：2011-10-20

    申请人： Stephen W. King

    发明人： Stephen W. King

    IPC分类号： C07C209/60 ,  C07C209/54 ,  C07C209/64

    CPC分类号： C07C209/54 ,  C07C209/64 ,  C07C211/14

    摘要： A process for preparing high molecular weight acyclic polyamines comprising providing a reaction mixture that includes at least a first component comprising a first organic, nitrogen-containing compound that contains at least two non-tertiary amine groups separated from one another by a ternary or higher carbon atom spacing that can be transaminated in the presence of a hydrogenation/dehydrogenation catalyst to form a mixture of higher molecular weight, acyclic polyamines while minimizing the formation of cyclic polyamines.

    摘要翻译： 一种制备高分子量无环多胺的方法，包括提供反应混合物，该反应混合物包括至少第一组分，其包含第一有机含氮化合物，其含有通过三元或更高碳彼此分离的至少两个非叔胺基团 原子间隔可以在氢化/脱氢催化剂存在下进行转氨以形成较高分子量的无环多胺的混合物，同时最小化环状多胺的形成。