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公开(公告)号：US06218578B1
公开(公告)日：2001-04-17
申请号：US09589350
申请日：2000-06-08
IPC分类号： C07C31900
CPC分类号： C09K19/38 , C09K19/542 , C09K2219/01 , C09K2219/03
摘要： The invention relates to a polymeric film composed of an optically anisotropic material made from a cross-linked synthetic resin composition comprising a polymer network, being obtainable by copolymerization of a mixture comprising (a) at least one monomer or oligomer, each of said monomers or oligomers having at least two polymerizable functional groups selected from the group consisting of (meth-)acrylate ester, epoxy and vinyl ether, (b) at least one achiral liquid crystalline monomer or oligomer, each of said monomersloligomers having mesogenic groups and one polymerizable functional group selected from the group consisting of (meth-)acrylate ester, epoxy and vinyl ether.
摘要翻译： 本发明涉及由包含聚合物网络的交联合成树脂组合物制成的光学各向异性材料组成的聚合物膜，该聚合物网络可通过使包含（a）至少一种单体或低聚物，每种所述单体的混合物或 具有至少两个选自（甲基）丙烯酸酯，环氧和乙烯基醚的可聚合官能团的低聚物，（b）至少一种非手性液晶单体或低聚物，所述单体单体具有介晶基团和一个可聚合官能团 选自（甲基）丙烯酸酯，环氧和乙烯基醚的基团。
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2.发明授权Derivatives of 4-sulfanylalkyl-3,5-dinitrobenzyl alcohol and method for preparing the same 失效4-硫烷基烷基-3,5-二硝基苄醇的衍生物及其制备方法公开(公告)号：US06815567B2
公开(公告)日：2004-11-09
申请号：US10727611
申请日：2003-12-05
申请人： Hyoyoung Lee , Mun Seok Jeong , Sung Yool Choi , Tae Hyoung Zyung
发明人： Hyoyoung Lee , Mun Seok Jeong , Sung Yool Choi , Tae Hyoung Zyung
IPC分类号： C07C31900
CPC分类号： C07C327/28 , C07C323/16
摘要： The present invention is directed to a novel 4-sulfanylalkyl-3,5-dinitro benzyl alcohol compound and its preparation method, more specifically, derivatives of 4-sulfanylalkyl-3,5-dinitro benzyl alcohol compound having the following formula 1 and its preparation method: wherein, R is hydrogen, alkyl group, or acetyl group, and n is an integer of 1 to 25. The organic compound of the present invention can be used as a material for molecular electronic device.
摘要翻译： 本发明涉及一种新的4-硫烷基烷基-3,5-二硝基苯甲醇化合物及其制备方法，更具体地，涉及具有下式1的4-硫烷基烷基-3,5-二硝基苄醇化合物及其制备方法 方法：其中R为氢，烷基或乙酰基，n为1至25的整数。本发明的有机化合物可用作分子电子器件的材料。
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3.发明授权公开(公告)号：US06610218B1
公开(公告)日：2003-08-26
申请号：US09366865
申请日：1999-08-04
申请人： Tod C. Duvall , Paul B. Adams , Gene K. Norris
发明人： Tod C. Duvall , Paul B. Adams , Gene K. Norris
IPC分类号： C07C31900
摘要： Halogen-containing polymer compositions comprising a latent mercaptan-containing heat stabilizer composition substantially free from the offensive odor typically associated with mercaptans are protected during processing by the degradation products of the latent (i.e., blocked) mercaptan which include a free mercaptan. Other products of the degradation are believed to include carbocations of the blocking moiety which are stabilized by a molecular structure in which the electron deficiency is shared by several groups. The latent mercaptan may be the sole heat stabilizer additive but the free mercaptan released during processing may also synergize the activity of metal-based heat stabilizers such as metal salts and organometallic stabilizers such as organotin carboxylates and mercaptides in the polymer composition. The odor of primary mercaptan-containing heat stabilizers in halogenated polymer compositions is masked by a small amount of a latent mercaptan. The latent mercaptans also serve as intermediates in the preparation of anti-oxidants, anti-microbial agents, photostabilizers, and primary heat stabilizers. Highly effective heat stabilizers are prepared by the condensation of formaldehyde and a para-phenol and further condensation of the crude product with a mercapto-containing compound.
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公开(公告)号：US06765116B2
公开(公告)日：2004-07-20
申请号：US10226902
申请日：2002-08-23
申请人： Charles Lee Edwards
发明人： Charles Lee Edwards
IPC分类号： C07C31900
CPC分类号： C07C41/03 , B01J27/1804 , C07C43/11
摘要： A process to prepare an improved fluid rare earth phosphate catalyst composition useful in preparing alkylene oxide adducts of organic compounds having active hydrogen atoms is provided. The catalyst is prepared by dissolving a rare earth salt in a C9-C30 active hydrogen containing organic compound and then adding phosphoric acid to the organic compound rare earth mixture.
摘要翻译： 提供了制备用于制备具有活性氢原子的有机化合物的环氧烷加合物的改进的流体稀土磷酸盐催化剂组合物的方法。 通过将稀土盐溶解在含C9-C30活性氢的有机化合物中，然后向有机化合物稀土混合物中加入磷酸制备催化剂。
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公开(公告)号：US06365781B2
公开(公告)日：2002-04-02
申请号：US09755369
申请日：2001-01-05
IPC分类号： C07C31900
CPC分类号： C07C319/14 , C08K5/375 , C08L21/00 , C07C323/16
摘要： There is disclosed an improved process for the preparation of a compound of the formula I wherein n is 0 or 1, R1 is C1-C12alkyl or —CH2SR3, R2 is C1-C12alkyl, C7-C9phenylalkyl, C7-C9-phenylalkyl substituted on the phenyl radical by from 1 to 3 C1-C4alkyl groups; or —CH2SR3, R3 is C6-C18alkyl, phenyl or benzyl, R4 is hydrogen or methyl, R5 is hydrogen or methyl, with the proviso that R4 and R5 are not simultaneously methyl, by reacting a compound of the formula II wherein n, R4 and R5 are as previously defined, R11 is hydrogen or C1-C12alkyl; and R12 is hydrogen, C1-C12alkyl, C7-C9phenylalkyl, C7-C9phenylalkyl substituted on the phenyl radical by from 1 to 3 C1-C4alkyl groups; with formaldehyde or a compound that liberates formaldehyde under the reaction conditions and with at least one compound of the formula III R3SH (III) wherein R3 is as previously defined, in the presence of a base, said base being mono- or dimethylamine or mono- or diethylamine, which process comprises treating afterwards the reaction product with a reducing agent.
摘要翻译： 公开了一种制备式I化合物的改进方法，其中n为0或1，R1为C1-C12烷基或-CH2SR3，R2为C1-C12烷基，C7-C9苯基烷基，C7-C9-苯基烷基取代苯基 由1至3个C 1 -C 4烷基基团; 或-CH 2 S R 3，R 3是C 6 -C 18烷基，苯基或苄基，R 4是氢或甲基，R 5是氢或甲基，条件是R 4和R 5不同时为甲基，通过使式II的化合物在n， R 5如前所定义，R 11为氢或C 1 -C 12烷基; 并且R 12是氢，C 1 -C 12烷基，C 7 -C 9苯基烷基，在苯基上被1至3个C 1 -C 4烷基取代的C 7 -C 9苯基烷基; 与甲醛或在反应条件下释放甲醛的化合物，以及至少一种式III的化合物，其中R 3如前所定义，在碱的存在下，所述碱是单或二甲胺或一或二乙胺，该方法 包括用还原剂处理反应产物。
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公开(公告)号：US06596905B1
公开(公告)日：2003-07-22
申请号：US09868823
申请日：2001-08-27
IPC分类号： C07C31900
CPC分类号： C07C319/14 , C07C323/29
摘要： The invention concerns a method for preparing aromatic diphenyl thioethers. More particularly the invention concerns the preparation of 4-chloro-4′-thiomethyldiphenylether. The inventive method for preparing an aromatic diphenyl thioether is characterised in that it consists in reacting in an aqueous medium a diazonium salt of an aromatic diphenyl compound with a disulphide sulphur compound, in the presence of an efficient amount of a coupling catalyst.
摘要翻译： 本发明涉及一种制备芳族二苯硫醚的方法。 更具体地，本发明涉及4-氯-4'-硫代甲基二苯醚的制备。 本发明的芳族二苯基硫醚的制备方法的特征在于，在有效量的偶联催化剂存在下，其在水性介质中使芳族二苯基化合物的重氮盐与二硫化物硫化合物反应。
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公开(公告)号：US06548709B2
公开(公告)日：2003-04-15
申请号：US09973606
申请日：2001-10-09
申请人： Margaret M. Wu , Philip Trotto , Shifang Luo , Jose G. Santiesteban , Hye Kyung C. Timken , Sandeep S. Dhingra , Simon C. Weston , Richard T. Spissell
发明人： Margaret M. Wu , Philip Trotto , Shifang Luo , Jose G. Santiesteban , Hye Kyung C. Timken , Sandeep S. Dhingra , Simon C. Weston , Richard T. Spissell
IPC分类号： C07C31900
CPC分类号： C10M135/28 , C07C319/14 , C07C321/30
摘要： The present invention relates to methods for production of arylsulfides wherein an aromatic compound is reacted with elemental sulfur in the presence of solid acid catalyst. The solid acid catalyst can be a zeolite. The methods are useful for producing alkylated diphenylsulfides from aromatic compounds and elemental sulfur.
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公开(公告)号：US06686506B1
公开(公告)日：2004-02-03
申请号：US09831914
申请日：2001-05-25
IPC分类号： C07C31900
CPC分类号： C07C319/24 , C07C321/14
摘要： The invention relates to a process for the preparation of organic disulfides by oxidation of mercaptans with sulfur dissolved in an organic disulfide using an amine as catalyst, where the mercaptans are used as “crude mercaptan stream” from a reaction of alcohols with hydrogen sulfide over a catalyst suitable for mercaptan synthesis. Furthermore, the invention relates to the use of the organic disulfides for the preparation of alkanesulfonic acids.
摘要翻译： 本发明涉及一种通过使用胺作为催化剂将硫溶解在有机二硫化物中的硫醇硫化制备有机二硫化物的方法，其中硫醇用作“硫醇粗品”的醇与硫化氢的反应， 适用于硫醇合成的催化剂。 此外，本发明涉及有机二硫化物用于制备链烷磺酸的用途。
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9.发明授权Latent mercaptans as multi-functional additives for halogen-containing polymer compositions 失效潜在的硫醇作为含卤聚合物组合物的多功能添加剂公开(公告)号：US06326518B1
公开(公告)日：2001-12-04
申请号：US09366879
申请日：1999-08-04
申请人： Tod C. Duvall , Paul B. Adams , Gene K. Norris
发明人： Tod C. Duvall , Paul B. Adams , Gene K. Norris
IPC分类号： C07C31900
摘要： Halogen-containing polymer compositions comprising a latent mercaptan-containing heat stabilizer composition substantially free from the offensive odor typically associated with mercaptans are protected during processing by the degradation products of the latent (i.e., blocked) mercaptan which include a free mercaptan. Other products of the degradation are believed to include carbocations of the blocking moiety which are stabilized by a molecular structure in which the electron deficiency is shared by several groups. The latent mercaptan may be the sole heat stabilizer additive but the free mercaptan released during processing may also synergize the activity of metal-based heat stabilizers such as metal salts and organometallic stabilizers such as organotin carboxylates and mercaptides in the polymer composition. The odor of primary mercaptan-containing heat stabilizers in halogenated polymer compositions is masked by a small amount of a latent mercaptan. The latent mercaptans also serve as intermediates in the preparation of anti-oxidants, anti-microbial agents, photostabilizers, and primary heat stabilizers. Highly effective heat stabilizers are prepared by the condensation of formaldehyde and a para-phenol and further condensation of the crude product with a mercapto-containing compound.
摘要翻译： 包含含有含硫醇的热稳定剂组合物的含卤素聚合物组合物通常与硫醇通常相关的令人反感的气味在加工过程中受到包含游离硫醇的潜在（即封闭的）硫醇的降解产物的保护。 认为降解的其它产物包括通过分子结构稳定的阻挡部分的碳阳离子，其中电子缺乏被几个基团共享。 潜在的硫醇可以是唯一的热稳定剂添加剂，但在加工过程中释放的游离硫醇也可以在金属基热稳定剂如金属盐和有机金属稳定剂例如聚合物组合物中的羧酸有机羧酸盐和硫醇中起作用。 卤代聚合物组合物中含一级硫醇的热稳定剂的气味被少量的潜硫酚掩蔽。 潜在的硫醇也用作制备抗氧化剂，抗微生物剂，光稳定剂和初级热稳定剂的中间体。 通过甲醛和对苯酚的缩合以及粗产物与含巯基化合物的进一步缩合来制备高效热稳定剂。
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