Method and device for obtaining stearin from animal or vegetable fats
    3.
    发明授权
    Method and device for obtaining stearin from animal or vegetable fats 有权
    从动物或植物脂肪中获得硬脂精的方法和装置

    公开(公告)号:US06169191A

    公开(公告)日:2001-01-02

    申请号:US09214735

    申请日:1999-01-11

    IPC分类号: C11B700

    CPC分类号: C11B7/0075 B04B1/12

    摘要: 1. Method and Apparatus for the production of stearin from fat of animal or plant origin. 2.1 A method is carried out such that during the duration of a production run, a sharp separation between the stearin phase and the oil phase is maintained at a constant rate, to achieve an optimum quality of stearin and stearin yield. 2.2. Crystallized oil of a temperature from 10 C to 40 C is fed into inlet (12) of a nozzle-type centrifuge (11) which is not self-emptying and is equipped with a stack of plates (15) and a stationary gripping device (16) for the oil phase. The solid phase is guided through flow chambers tapering towards the nozzles (20) and discharged through these nozzles. To realize a high degree of separation between the stearin phase and the oil phase, the ratio between the feed rate in I/h and the nozzle capacity in I/h is adjusted in the range between 2:1 and 4:1. 2.3 The method is used for stearin production from animal or plant fats. 3. FIG. 2.

    摘要翻译: 1.用于从动物或植物来源的脂肪生产硬脂精的方法和装置.1一种方法进行,使得在生产运行期间,硬脂酸相和油相之间的急剧分离保持恒定 速率,达到硬脂精和硬脂精产量的最佳质量。 将温度为10℃至40℃的结晶油进料到不自排空的喷嘴式离心机(11)的入口(12)中,并配备有一叠板(15)和固定夹紧装置( 16)为油相。 固相通过朝向喷嘴(20)逐渐变细的流动室引导并通过这些喷嘴排出。 为了实现硬脂酸相和油相之间的高度分离,I / h中的进料速率和I / h中的喷嘴容量之间的比率在2:1和4:1.2.3之间的范围内调节。 方法用于动物或植物脂肪的硬脂精生产。 图。 2。

    Recovery of polyunsaturated fatty acids from urea adducts
    4.
    发明授权
    Recovery of polyunsaturated fatty acids from urea adducts 失效
    从尿素加合物回收多不饱和脂肪酸

    公开(公告)号:US06528669B1

    公开(公告)日:2003-03-04

    申请号:US10031712

    申请日:2002-04-03

    IPC分类号: C11B700

    摘要: Polyunsaturated fatty acids, as free fatty acids, fatty acid esters or fatty acid amides, especially EPA and/or DHA, DPC 9/02, are recovered from urea adducts, such as obtained as by-products in the processing of fish and other oils, by treatment with a subcritical or supercritical fluid.

    摘要翻译: 多不饱和脂肪酸,作为游离脂肪酸,脂肪酸酯或脂肪酸酰胺,特别是EPA和/或DHA,DPC 9/02,从尿素加合物中回收,例如在鱼和其他油的加工中作为副产物获得 ,通过用亚临界或超临界流体处理。

    Liquid chromatography of high purity conjugated fatty acid
    6.
    发明授权
    Liquid chromatography of high purity conjugated fatty acid 失效
    高纯度共轭脂肪酸的液相色谱法

    公开(公告)号:US06410763B1

    公开(公告)日:2002-06-25

    申请号:US09721849

    申请日:2000-11-24

    申请人: Michael C. Seidel

    发明人: Michael C. Seidel

    IPC分类号: C11B700

    摘要: A method for providing a purified conjugated fatty acid is disclosed. The purified conjugated fatty acid is formed by separating by liquid chromatography a conjugated fatty acid formed by a novel synthesis of reacting an ester of a fatty acid having a four carbon chain such that carbon one bears one hydrogen and one hydroxyl group, carbon two bears two hydrogen atoms, and a double bond is positioned between carbon three and carbon four, with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of said ester, and reacting the tosylate or mesylate of said ester with diazabicyclo-undecene. Reacting an ester of a fatty acid having a four carbon chain such that carbon one bears one hydrogen and one hydroxyl group, carbon two bears two hydrogen atoms, a double bond is positioned between carbon three and carbon four, with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of said ester, and reacting the tosylate or mesylate of said ester with diazabicyclo-undecene forms a conjugated fatty acid having a purity greater than 50%, and separating by liquid chromatography forms a conjugated fatty acid having a purity greater than 90%. In one aspect, the liquid chromatography uses a strong acid macroreticular ion exchange resin. In one aspect, the liquid chromatography includes silver ion liquid chromatography.

    摘要翻译: 公开了提供纯化的共轭脂肪酸的方法。 纯化的共轭脂肪酸通过液相色谱法分离形成的共轭脂肪酸,其通过使具有四个碳链的脂肪酸的酯与碳一个氢和一个羟基反应的新合成形成,二碳二 氢原子和双键位于碳三和碳四之间,用甲苯磺酰氯或甲磺酰氯形成所述酯的甲苯磺酸酯或甲磺酸酯,并使所述酯的甲苯磺酸酯或甲磺酸酯与二氮杂双环十一碳烯反应。 反应具有四个碳链的脂肪酸的酯,使得碳一个具有一个氢和一个羟基,碳二具有两个氢原子,双键位于碳三和碳四之间,用甲苯磺酰氯或甲磺酰 氯化以形成所述酯的甲苯磺酸酯或甲磺酸酯,并使所述酯的甲苯磺酸酯或甲磺酸酯与二氮杂双环十一碳烯反应形成纯度大于50%的共轭脂肪酸,并通过液相色谱分离形成具有纯度的共轭脂肪酸 大于90%。 一方面,液相色谱法使用强酸性大网状离子交换树脂。 一方面,液相色谱法包括银离子液相色谱法。

    Method of solvent fractionation of fat
    7.
    发明授权
    Method of solvent fractionation of fat 有权
    脂肪溶剂分馏方法

    公开(公告)号:US06265595B1

    公开(公告)日:2001-07-24

    申请号:US09509689

    申请日:2000-03-30

    IPC分类号: C11B700

    CPC分类号: C11B7/0008

    摘要: A method of solvent fractionation of a fat by which a high fat concentration, a rise in refrigerant temperature, and a reduction in operation time, etc. can be attained and fractions are efficiently produced at a low cost, characterized by rapidly cooling a feedstock fat dissolved in a solvent to a temperature higher by 1 to 20° C. than the crystallization temperature used in a crystallizer in the step prior to introduction of the feedstock fat into the crystallizer.

    摘要翻译: 可以获得高脂肪浓度,制冷剂温度上升和操作时间降低等的脂肪的溶剂分馏方法,并且以低成本有效地生产级分,其特征在于快速冷却原料脂肪 溶解在溶剂中比在将原料脂肪引入结晶器之前的步骤中结晶器中使用的结晶温度高1至20℃的温度。