PROCESS FOR SYNTHESIZING METAL BOROHYDRIDES
    1.
    发明申请
    PROCESS FOR SYNTHESIZING METAL BOROHYDRIDES 审中-公开
    合成金属硼酸盐的方法

    公开(公告)号:US20090026416A1

    公开(公告)日:2009-01-29

    申请号:US12180452

    申请日:2008-07-25

    申请人: Yu Zhou

    发明人: Yu Zhou

    IPC分类号: C01B6/15 C09K3/00

    CPC分类号: C01B6/17 C01B6/15

    摘要: A process for synthesizing metal borohydride especially sodium borohydride directly from borax by the use of proton H at room temperature and pressure. Said process comprising the steps of: Providing proton H by the use of metals or alloys that can form hydrides with hydrogen. In this case, the metals or alloys are the carriers of proton H Proton H also can be provided from hydrogen gas by the use of catalysts located on the surface of carriers. Making the proton H enters the lattice of boron oxides Removing the oxygen from the lattice of boron oxides by the use of the carriers.

    摘要翻译: 通过在室温和压力下使用质子H从硼砂直接合成金属硼氢化物,特别是硼氢化钠的方法。 所述方法包括以下步骤:通过使用可与氢形成氢化物的金属或合金来提供质子H. 在这种情况下,金属或合金是质子H的载体。质子H也可以通过使用位于载体表面上的催化剂由氢气提供。 使质子H进入氧化硼的晶格通过使用载体从氧化硼晶格中除去氧。

    Process for synthesizing metal borohydrides
    2.
    发明授权
    Process for synthesizing metal borohydrides 有权
    合成金属硼氢化物的方法

    公开(公告)号:US07429368B2

    公开(公告)日:2008-09-30

    申请号:US09778997

    申请日:2001-02-08

    申请人: Yu Zhou

    发明人: Yu Zhou

    IPC分类号: C01B6/15

    CPC分类号: C01B6/17 C01B6/15

    摘要: A process for synthesizing metal borohydride especially sodium borohydride directly from borax by the use of proton H at room temperature and pressure. Said process comprising the steps of:Providing proton H by the use of metals or alloys that can form hydrides with hydrogen. In this case, the metals or alloys are the carriers of proton HProton H also can be provided from hydrogen gas by the use of catalysts located on the surface of carriers.Making the proton H enters the lattice of boron oxidesRemoving the oxygen from the lattice of boron oxides by the use of the carriers.

    摘要翻译: 通过在室温和压力下使用质子H从硼砂直接合成金属硼氢化物,特别是硼氢化钠的方法。 所述方法包括以下步骤:通过使用可与氢形成氢化物的金属或合金来提供质子H. 在这种情况下,金属或合金是质子H的载体。质子H也可以通过使用位于载体表面上的催化剂由氢气提供。 使质子H进入氧化硼的晶格通过使用载体从氧化硼晶格中除去氧。

    Inorganic magnesium solid electrolyte, magnesium battery, and method for producing inorganic magnesium solid electrolyte
    3.
    发明授权
    Inorganic magnesium solid electrolyte, magnesium battery, and method for producing inorganic magnesium solid electrolyte 有权
    无机镁固体电解质,镁电池和无机镁固体电解质的制备方法

    公开(公告)号:US09017880B2

    公开(公告)日:2015-04-28

    申请号:US13890647

    申请日:2013-05-09

    摘要: A magnesium battery 10 according to the present invention includes a positive electrode 12, a negative electrode 14 having a magnesium-containing negative electrode active material, and an inorganic magnesium solid electrolyte 16 that is interposed between the positive electrode 12 and the negative electrode 14, has a complex ion structure that contains magnesium and hydrogen, and conducts magnesium ions. The inorganic magnesium solid electrolyte 16 may contain a compound having at least one selected from boron and nitrogen. The inorganic magnesium solid electrolyte may be produced by a production method that includes a heat-treatment step of mixing and heating Mg(BH4)2 and Mg(NH2)2 to form a compound having a complex ion structure that contains magnesium and hydrogen.

    摘要翻译: 根据本发明的镁电池10包括正极12,具有含镁负极活性物质的负极14和插在正极12和负极14之间的无机镁固体电解质16, 具有复杂的离子结构,其含有镁和氢,并传导镁离子。 无机镁固体电解质16可以含有选自硼和氮中的至少一种的化合物。 无机镁固体电解质可以通过包括混合并加热Mg(BH 4)2和Mg(NH 2)2)以形成具有含有镁和氢的复合离子结构的化合物的热处理步骤的制备方法来制备。

    METHODS FOR PREPARING COMPOSITIONS WHICH COMPRISE MAGNESIUM BOROHYDRIDE, AND RELATED MATERIALS
    5.
    发明申请
    METHODS FOR PREPARING COMPOSITIONS WHICH COMPRISE MAGNESIUM BOROHYDRIDE, AND RELATED MATERIALS 有权
    制备含有硼氢化镁的组合物的方法及相关材料

    公开(公告)号:US20080014136A1

    公开(公告)日:2008-01-17

    申请号:US11767067

    申请日:2007-06-22

    IPC分类号: C01B6/15

    CPC分类号: C01B3/04 C01B6/21 Y02E60/364

    摘要: Disclosed herein is a method for preparing magnesium borohydride. The method includes the step of reacting a metal borohydride with a metal salt composition in a solvent, to form a reaction mixture. The metal salt composition comprises at least one magnesium salt. The metal borohydride and the metal salt composition are insoluble in the solvent. The method further includes the step of grinding the reaction mixture to produce a composition that includes magnesium borohydride; and removing the solvent from the composition. Another embodiment of this invention relates to a new material. The material is an orthorhombic crystal phase of magnesium borohydride.

    摘要翻译: 本文公开了一种制备硼氢化镁的方法。 该方法包括使金属硼氢化物与金属盐组合物在溶剂中反应以形成反应混合物的步骤。 金属盐组合物包含至少一种镁盐。 金属硼氢化物和金属盐组合物不溶于溶剂。 该方法还包括研磨反应混合物以产生包括硼氢化镁的组合物的步骤; 并从组合物中除去溶剂。 本发明的另一个实施例涉及一种新的材料。 该材料是硼氢化镁的斜方晶相。

    Boron compounds
    6.
    发明授权
    Boron compounds 失效
    硼化合物

    公开(公告)号:US6143264A

    公开(公告)日:2000-11-07

    申请号:US91580

    申请日:1998-08-26

    IPC分类号: C07F5/02 C01B6/15

    CPC分类号: C07F5/022

    摘要: Process for the preparation of undecahydrododecaborate anions [B.sub.12 H.sub.(12-n) (XCN).sub.n ].sup.2- or [B.sub.12 H.sub.11 XH].sup.2- or a nonahydrodecaborate anions [B.sub.10 H.sub.(12-n) (XCN).sub.n ].sup.2- or [B.sub.10 H.sub.9 XH].sup.2- or anions of formula [B.sub.12 H.sub.11 SC(NR.sup.1 R.sup.2).sub.2 ].sup.-1 wherein X=O, S, or Se.

    摘要翻译: PCT No.PCT / GB96 / 03115 Sec。 371日期:1998年8月26日 102(e)1998年8月26日PCT 1996年12月17日PCT PCT。 第WO97 / 23487号公报 日期1997年7月3日十氢十二硼酸盐阴离子的制备方法[B12H(12-n)(XCN)n] 2-或[B12H11XH] 2-或非氢化十硼酸盐阴离子[B10H(12-n)(XCN)n] 或[B10H9XH] 2-或式[B12H11SC(NR1R2)2] - ]的阴离子,其中X = O,S或Se。

    Borides and boride precursors deposited from solution
    9.
    发明授权
    Borides and boride precursors deposited from solution 失效
    从溶液中沉积硼化物和硼化物前体

    公开(公告)号:US5364607A

    公开(公告)日:1994-11-15

    申请号:US836304

    申请日:1992-03-04

    CPC分类号: C01B35/04 C01B6/10

    摘要: Zirconium and hafnium boride precursor complexes are prepared by deposition from solution, and yield metal borides upon heating at mild temperatures and ambient pressure.

    摘要翻译: PCT No.PCT / US89 / 03883 Sec。 371日期:1992年3月4日 102(e)1992年3月4日PCT PCT 1989年9月8日PCT公布。 出版物WO91 / 03420 1991年3月21日,锆和硼化铪前体复合物通过从溶液中沉积制备,并在温和的温度和环境压力下加热产生金属硼化物。