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    Energy efficient synthesis of boranes
    2.
    发明授权
    Energy efficient synthesis of boranes 有权
    能量高效合成硼烷

    公开(公告)号：US08101786B2

    公开(公告)日：2012-01-24

    申请号：US12914595

    申请日：2010-10-28

    申请人： David L Thorn ,  William Tumas ,  Daniel E Schwarz ,  Anthony K Burrell

    发明人： David L Thorn ,  William Tumas ,  Daniel E Schwarz ,  Anthony K Burrell

    IPC分类号： C01B6/24 ,  C08G79/08

    CPC分类号： C01B6/15 ,  C01B6/19 ,  C01B35/061

    摘要： The reaction of halo-boron compounds (B—X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B—H compounds, compounds having one or more B—H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si—H) react with B—X compounds to form B—H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface-bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn—H bond) to form boranes and halostannanes (tin compounds having a Sn—X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCl3, the B—H compound is B2H6, and where the reducing potential is provided electrochemically or by the thermolysis of formate.

    摘要翻译： 卤代硼化合物（B-X化合物，具有一个或多个硼 - 卤键的化合物）与硅烷的反应提供硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。 无机氢化物，例如表面结合的硅烷氢化物（Si-H）与B-X化合物反应以形成B-H化合物和表面结合的卤代硅烷。 表面结合的卤代硅烷在电化学上转化回表面结合的硅烷。 卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代烷（具有Sn-X键的锡化合物）。 卤代烷腈通过电化学方法或通过Sn-甲酸酯化合物的热解转化回锡烷。 当卤代硼化合物为BCl 3时，B-H化合物为B 2 H 6，并且其电还原电位或通过甲酸盐的热解提供还原电位。

    ENERGY EFFICIENT SYNTHESIS OF BORANES
    3.
    发明申请
    ENERGY EFFICIENT SYNTHESIS OF BORANES 有权
    能量有效地合成硼

    公开(公告)号：US20110105706A1

    公开(公告)日：2011-05-05

    申请号：US12914595

    申请日：2010-10-28

    申请人： David L. Thorn ,  William Tumas ,  Daniel E. Schwarz ,  Anthony K. Burrell

    发明人： David L. Thorn ,  William Tumas ,  Daniel E. Schwarz ,  Anthony K. Burrell

    IPC分类号： C08F130/04 ,  C07F5/02 ,  C07F7/22

    CPC分类号： C01B6/15 ,  C01B6/19 ,  C01B35/061

    摘要： The reaction of halo-boron compounds (B—X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B—H compounds, compounds having one or more B—H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si—H) react with B—X compounds to form B—H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface-bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn—H bond) to form boranes and halostannanes (tin compounds having a Sn—X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCl3, the B—H compound is B2H6, and where the reducing potential is provided electrochemically or by the thermolysis of formate.

    摘要翻译： 卤代硼化合物（B-X化合物，具有一个或多个硼 - 卤键的化合物）与硅烷的反应提供硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。 无机氢化物，例如表面结合的硅烷氢化物（Si-H）与B-X化合物反应以形成B-H化合物和表面结合的卤代硅烷。 表面结合的卤代硅烷在电化学上转化回表面结合的硅烷。 卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代烷（具有Sn-X键的锡化合物）。 卤代烷腈通过电化学方法或通过Sn-甲酸酯化合物的热解转化回锡烷。 当卤代硼化合物为BCl 3时，B-H化合物为B 2 H 6，并且其还原电位通过电化学方法或通过甲酸盐的热解提供。

    Inorganic magnesium solid electrolyte, magnesium battery, and method for producing inorganic magnesium solid electrolyte
    4.
    发明授权
    Inorganic magnesium solid electrolyte, magnesium battery, and method for producing inorganic magnesium solid electrolyte 有权
    无机镁固体电解质，镁电池和无机镁固体电解质的制备方法

    公开(公告)号：US09017880B2

    公开(公告)日：2015-04-28

    申请号：US13890647

    申请日：2013-05-09

    申请人： Kabushiki Kaisha Toyota Chuo Kenkyusho

    发明人： Shougo Higashi ,  Masakazu Aoki

    IPC分类号： H01M10/0562 ,  H01M10/054 ,  C01B21/092 ,  C01B6/00 ,  C01B6/15

    CPC分类号： H01M10/0562 ,  C01B6/003 ,  C01B6/15 ,  C01B21/092 ,  C01P2002/72 ,  H01M10/054 ,  H01M2300/0068

    摘要： A magnesium battery 10 according to the present invention includes a positive electrode 12, a negative electrode 14 having a magnesium-containing negative electrode active material, and an inorganic magnesium solid electrolyte 16 that is interposed between the positive electrode 12 and the negative electrode 14, has a complex ion structure that contains magnesium and hydrogen, and conducts magnesium ions. The inorganic magnesium solid electrolyte 16 may contain a compound having at least one selected from boron and nitrogen. The inorganic magnesium solid electrolyte may be produced by a production method that includes a heat-treatment step of mixing and heating Mg(BH4)2 and Mg(NH2)2 to form a compound having a complex ion structure that contains magnesium and hydrogen.

    摘要翻译： 根据本发明的镁电池10包括正极12，具有含镁负极活性物质的负极14和插在正极12和负极14之间的无机镁固体电解质16， 具有复杂的离子结构，其含有镁和氢，并传导镁离子。 无机镁固体电解质16可以含有选自硼和氮中的至少一种的化合物。 无机镁固体电解质可以通过包括混合并加热Mg（BH 4）2和Mg（NH 2）2）以形成具有含有镁和氢的复合离子结构的化合物的热处理步骤的制备方法来制备。

    INORGANIC MAGNESIUM SOLID ELECTROLYTE, MAGNESIUM BATTERY, AND METHOD FOR PRODUCING INORGANIC MAGNESIUM SOLID ELECTROLYTE
    7.
    发明申请
    INORGANIC MAGNESIUM SOLID ELECTROLYTE, MAGNESIUM BATTERY, AND METHOD FOR PRODUCING INORGANIC MAGNESIUM SOLID ELECTROLYTE 有权
    无机磁固体电解质，镁电池及其制造无机固体电解质的方法

    公开(公告)号：US20130316249A1

    公开(公告)日：2013-11-28

    申请号：US13890647

    申请日：2013-05-09

    申请人： KABUSHIKI KAISHA TOYOTA CHUO KENKYUSHO

    发明人： Shougo HIGASHI ,  Masakazu AOKI

    IPC分类号： H01M10/0562 ,  H01M10/054

    CPC分类号： H01M10/0562 ,  C01B6/003 ,  C01B6/15 ,  C01B21/092 ,  C01P2002/72 ,  H01M10/054 ,  H01M2300/0068

    摘要： A magnesium battery 10 according to the present invention includes a positive electrode 12, a negative electrode 14 having a magnesium-containing negative electrode active material, and an inorganic magnesium solid electrolyte 16 that is interposed between the positive electrode 12 and the negative electrode 14, has a complex ion structure that contains magnesium and hydrogen, and conducts magnesium ions. The inorganic magnesium solid electrolyte 16 may contain a compound having at least one selected from boron and nitrogen. The inorganic magnesium solid electrolyte may be produced by a production method that includes a heat-treatment step of mixing and heating Mg(BH4)2 and Mg(NH2)2 to form a compound having a complex ion structure that contains magnesium and hydrogen.

    摘要翻译： 根据本发明的镁电池10包括正极12，具有含镁负极活性物质的负极14和插在正极12和负极14之间的无机镁固体电解质16， 具有复杂的离子结构，其含有镁和氢，并传导镁离子。 无机镁固体电解质16可以含有选自硼和氮中的至少一种的化合物。 无机镁固体电解质可以通过包括混合并加热Mg（BH 4）2和Mg（NH 2）2）以形成具有含有镁和氢的复合离子结构的化合物的热处理步骤的制备方法来制备。

    Complex hydrides for hydrogen storage
    8.
    发明授权
    Complex hydrides for hydrogen storage 有权
    用于氢存储的复杂氢化物

    公开(公告)号：US07094387B2

    公开(公告)日：2006-08-22

    申请号：US10700001

    申请日：2003-11-03

    申请人： Ragaiy Zidan

    发明人： Ragaiy Zidan

    IPC分类号： C01B6/00 ,  C01B6/02 ,  C01B6/04 ,  C01B6/24 ,  C01B3/04

    CPC分类号： C01B3/0031 ,  C01B6/15 ,  C01B6/24 ,  Y02E60/327 ,  Y02E60/364

    摘要： A hydrogen storage material and process of forming the material is provided in which complex hydrides are combined under conditions of elevated temperatures and/or elevated temperature and pressure with a titanium metal such as titanium butoxide. The resulting fused product exhibits hydrogen desorption kinetics having a first hydrogen release point which occurs at normal atmospheres and at a temperature between 50° C. and 90° C.

    摘要翻译： 提供了一种储氢材料和形成该材料的方法，其中使用钛金属如丁醇钛在高温和/或升高的温度和压力条件下将复合氢化物组合。 所得的熔融产物表现出氢解吸动力学，其具有在正常气氛下和在50℃和90℃之间的温度下发生的第一氢释放点。