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    Sulfited fats
    3.
    发明授权
    Sulfited fats 失效
    饱和脂肪

    公开(公告)号：US4800045A

    公开(公告)日：1989-01-24

    申请号：US53998

    申请日：1987-05-26

    申请人： Hans-Herbert Friese ,  Friedrich Pieper ,  Reinhard Bosse

    发明人： Hans-Herbert Friese ,  Friedrich Pieper ,  Reinhard Bosse

    IPC分类号： C11C3/00 ,  C07B45/02 ,  C14C9/02 ,  C07C143/90

    CPC分类号： C07B45/02 ,  C14C9/02

    摘要： Sulfited fats prepared by oxidation of fats with oxygen-containing gas mixtures and simultaneous or subsequent sulfitation using alkali and/or ammonium hydrogen sulfites, wherein the fats used are mixtures containing(A) fats having iodine numbers below about 100 and(B) fatty acid esters having iodine numbers of from about 60 to about 100 and containing from 12 to 24 carbon atoms in the linear or branched, natural and/or synthetic fatty acid residue and from 1 to 5 carbon atoms in the monofunctional alcohol residue,the ratio by weight of (A) to (B) being from about 9:1 to about 1:4.

    摘要翻译： 用含氧气体混合物氧化脂肪制备的硫酸脂肪，以及使用碱和/或亚硫酸氢铵的同时或随后的硫酸化，其中使用的脂肪是含有（A）碘值低于约100的脂肪和（B）脂肪酸 在单官能醇残基中直链或支链，天然和/或合成的脂肪酸残基和1至5个碳原子的碘值为约60至约100且含有12至24个碳原子的酯，重量比 （A）至（B）为约9:1至约1:4。

    Process for the continuous sulphonation of alkyl aromatic hydrocarbons
    5.
    发明授权
    Process for the continuous sulphonation of alkyl aromatic hydrocarbons 失效
    烷基芳烃连续磺化的方法

    公开(公告)号：US4036875A

    公开(公告)日：1977-07-19

    申请号：US583319

    申请日：1975-06-02

    申请人： Anders Brostrom

    发明人： Anders Brostrom

    IPC分类号： B01J19/18 ,  C07B45/02 ,  C07C303/00 ,  C07C309/08 ,  C07C309/28 ,  C07C143/24

    CPC分类号： C07C303/00 ,  B01J19/18 ,  C07B45/02 ,  C07C303/06 ,  C07C303/24 ,  B01J2219/00085 ,  B01J2219/00189 ,  B01J2219/185

    摘要： An improved process is provided for the continuous sulphonation and/or sulphation of organic substances with sulphur trioxide gas mixed with an inert gaseous diluent, at an increased production rate without impairment of product quality, while minimizing discoloration of the product, and the amounts of unsulphonated product in the product, and of unreacted sulphur trioxide in the residual gaseous mixture, by limiting the amount of sulphur trioxide introduced ab initio into the organic liquid to be sulphonated and/or sulphated to not exceeding 7%, and preferably within the range from about 0.25 to about 5%, of the stoichiometric amount required for the desired sulphonated or sulphated product, introducing the remaining sulphur trioxide over from about 20 to about 80%, preferably from about 25 to about 50%, of the remainder of the length of the reaction zone.

    摘要翻译： 提供了一种改进的方法，用于连续磺化和/或硫酸化有机物质与三氧化硫气体混合惰性气体稀释剂，以增加的生产率，而不损害产品质量，同时最小化产品的变色，以及未磺​​化的量 产物和残余气体混合物中未反应的三氧化硫，通过将从头进入磺化和/或硫酸化的有机液体中的三氧化硫的量限制在不超过7％，优选在约 将所需磺化或硫酸化产物所需的化学计量量为0.25至约5％，将剩余的三氧化硫引入剩余长度的约20至约80％，优选约25至约50％ 反应区。

    Sulfonation of aromatic compounds
    6.
    发明授权
    Sulfonation of aromatic compounds 失效
    芳香化合物的磺化

    公开(公告)号：US3946037A

    公开(公告)日：1976-03-23

    申请号：US411054

    申请日：1973-10-30

    申请人： Adolf Koebner

    发明人： Adolf Koebner

    IPC分类号： C07D333/04 ,  C07B31/00 ,  C07B45/02 ,  C07C67/00 ,  C07C301/00 ,  C07C303/06 ,  C07C309/01 ,  C07C309/28 ,  C07D333/00 ,  C07D333/34 ,  C07C143/24

    CPC分类号： C07C309/00 ,  C07B45/02

    摘要： A process for the sulfonation of aromatic compounds wherein an aromatic substance consisting of one or more aromatic compounds is brought to boiling at a temperature not greater than 100.degree.C under a pressure of from 0.1 mm Hg to atmospheric pressure, gaseous sulfur trioxide is introduced thereinto, thereby causing it to continue to boil, the aromatic substance thus volatilized is reconverted to liquid in a heat-exchanger and is recycled to the reaction chamber, and the pressure in the reaction chamber and the rate at which the gaseous sulfur trioxide is introduced into the aromatic substance are controlled to ensure that the amount of liquid aromatic substance present in the reaction chamber and available for participation in the sulfonation reaction is always in excess of that amount of said aromatic substance capable of reacting with the gaseous sulfur trioxide in contact with the aromatic substance in the reaction chamber and that the temperature of the reaction mixture is a temperature of 100.degree.C or below.

    摘要翻译： 芳族化合物的磺化方法，其中将由一种或多种芳族化合物组成的芳族物质在不大于100℃的温度下在0.1mmHg至大气压的压力下沸腾，将气态三氧化硫引入其中 ，从而使其继续沸腾，由此挥发的芳族物质在热交换器中再转化为液体并再循环至反应室，反应室中的压力和引入气态三氧化硫的速率 控制芳香物质以确保存在于反应室中并且可用于参与磺化反应的液体芳族物质的量总是超过能够与与三氯化硫接触的气态三氧化硫反应的所述芳族物质的量 芳族物质，反应混合物的温度是一个温度 100℃以下。

    Isothermal sulfonation process
    7.
    发明授权
    Isothermal sulfonation process 失效
    等温磺化工艺

    公开(公告)号：US3925441A

    公开(公告)日：1975-12-09

    申请号：US40908873

    申请日：1973-10-24

    申请人： LION FAT OIL CO LTD

    发明人： TOYODA SADAO ,  OGOSHI TOSHIAKI ,  MARUYAMA MINORU ,  MIYAWAKI YOZO

    IPC分类号： C07B45/02 ,  C07C303/00 ,  C07C141/02 ,  C07C143/16

    CPC分类号： C07B45/02 ,  C07C303/06 ,  C07C303/24 ,  C07C309/20 ,  C07C309/10 ,  C07C309/31 ,  C07C305/06

    摘要： In the process for sulfonation by contacting a falling thin film stream of organic compound with a stream of SO3-inert gas in parallel, an improved process for isothermal sulfonation producing sulfonates of high quality, which comprises making a SO3-containing cooling gas (wherein the SO3 content is 1 to 20 wt.% relative to the whole amount of SO3 to be employed) in the amount of about 2 to 12 times (by volume) as much as the total amount of said stream of SO3-inert gas flow in parallel between said falling thin film stream of organic compound and said stream of SO3-inert gas.

    摘要翻译： 在通过使有机化合物的下降薄膜流与SO 3惰性气体流并联接触来进行磺化的方法中，改进了等温磺化生产高质量磺酸盐的方法，其包括制备含SO 3的冷却气体（其中 SO 3含量相对于所使用的SO 3的总量为1〜20重量％）为所述SO 3 - 惰性气体流平行流量的总量的2〜12倍（体积） 在所述下降的有机化合物薄膜流和所述SO 3惰性气体流之间。

    Polynuclear amines and process for the preparation thereof
    8.
    发明授权
    Polynuclear amines and process for the preparation thereof 失效
    多核苷及其制备方法

    公开(公告)号：US3646005A

    公开(公告)日：1972-02-29

    申请号：US3646005D

    申请日：1967-03-10

    申请人： UGINE KUHLMANN

    发明人： ROE RENE PIERRE VICTOR ,  INFERIEURE SEINE ,  THIROT GERARD

    IPC分类号： C07B45/02 ,  C07D231/56 ,  C07D249/18 ,  C07D263/56 ,  C07D263/58 ,  C07D277/68 ,  C09B43/02 ,  C07C143/60 ,  C07C143/66

    CPC分类号： C09B43/02 ,  C07B45/02 ,  C07D231/56 ,  C07D249/18 ,  C07D263/56 ,  C07D263/58 ,  C07D277/68

    摘要： GROUPS.

    -N(-R1)-R2

    WHEREIN A REPRESENTS THE RESIDUE OF A DIZAOTISABLE AROMATIC OR HETEROCYCLIC AMINE, B REPRESENTS THE RESIDUE OF A COUPLING COMPOUND, R1 REPRESENTS A HYDROGEN ATOM OR AN ALKYL OR ARYL RESIDU, R2 REPRESENTS A HYDROGEN ATOM OR AN ALKYL RESIDUE, AND X'' AND Y'' EACH REPRESENT HYDROGEN OR HALOGEN ATOMS OR HYDROXY, ALKOXY, CARBOXY, SULPHO OR

    1-(B-N=N-),4-(HO3S-),(HO3S-),X'',Y''-DECALIN

    1,2,3,4,4A,7,8,8A-OCTAHYDRONAPHTHALENE

    1-(R1-N(-R2)-),2-(A-N=N-),3,4-DI(HO3S-),X'',Y''-

    THE PRESENT INVENTION RELATES TO A PROCESS FOR THE SULPHONOATION OF AN AROMATIC OR HETEROCYCLIC POLYNUCLEAR AMINE WHICH COMPRISES TREATING THE AMINE, DISPERSED OR DISSOLVED IN AN AQUEOUS SOLUTION OF A WATER-SOLUBLE SALT OF SULPHUROUS ACID, WITH AN OXIDISING AGENT OF WHICH THE OXIDATION POTENTIAL, MEASURED AT 20*C, AND PH( WITH RESPECT TO THE NORMAL HYDROGEN ELECTRODE, IS BETWEEN +0.4 AND +0.7 VOLT, THE PH OF THE MEDUM BEING MAINTAINED APPROXIMATELY CONSTANT AT A VALUE BETWEEN 3 AND 9.5. IT ALSO RELATES TO NEW SULPHONATED POLYNUCLEAR AMINES AND TO AZO DYESTUFFS HAVING ONE OF THE FORMULAE: