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公开(公告)号：US10130895B2
公开(公告)日：2018-11-20
申请号：US15535795
申请日：2015-12-15
申请人： CAP III B.V.
IPC分类号： B01D3/00 , C07C45/82 , B01D3/12 , B01D3/10 , B01D3/14 , C07C27/28 , C07C35/08 , C07C45/00 , C07C49/403
摘要： A process for the construction of a second chemical plant, which second chemical plant is suitable for the separation of cyclohexanone from a second mixture, which second mixture comprises reaction products from the hydrogenation of phenol. The process comprises providing a first chemical plant, which first chemical plant is suitable for the separation of cyclohexanone from a first mixture, and a second chemical plant comprising a distillation column suitable for distilling overhead cyclohexanone reused from the first chemical plant.
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2.发明授权Process for separating solids from valuable or harmful liquids by vaporisation 有权通过蒸发从有价值或有害液体中分离固体的方法公开(公告)号：US08652304B2
公开(公告)日：2014-02-18
申请号：US12997717
申请日：2009-06-15
申请人： Craig Nazzer
发明人： Craig Nazzer
摘要： The present invention is directed to an enhanced process for separating dissolved and suspended solids from valuable or harmful liquids and more particularly to improving the operational aspects and separation efficiency of treating certain water miscible fluids including those used for oil and gas processing such as glycols, as well as automobile and aircraft fluids, that have become contaminated with dissolved and/or suspended solid matter.
摘要翻译： 本发明涉及一种用于从有价值或有害液体中分离溶解和悬浮固体的改进方法，更具体地涉及改善处理某些水混溶性流体（包括用于油和气体处理的那些水混溶性流体如乙二醇）的操作方面和分离效率，如 以及被溶解和/或悬浮固体物质污染的汽车和飞机液体。
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公开(公告)号：US20120142977A1
公开(公告)日：2012-06-07
申请号：US13369255
申请日：2012-02-08
申请人： Jorge Miller , Louisa Kling Miller
发明人： Jorge Miller , Louisa Kling Miller
CPC分类号： C07C29/147 , C07C17/06 , C07C17/07 , C07C17/10 , C07C27/16 , C07C29/095 , C07C29/48 , C07C29/54 , C07C67/10 , C07C67/11 , C07C67/39 , C07C69/24 , C07C69/78 , C07C31/04 , C07C31/08 , C07C19/075
摘要： A method of making alcohols involves forming of alcohol esters from liquid alkane halides and a solution of metallic salts of organic acids to produce gaseous alcohol esters for reaction with magnesium or metal hydroxides to form the alcohol and the metal salt of the organic acids. In an improvement method liquid phase alcohol esters instead of gaseous alcohol esters are produced from liquid alkane halides and a solution of metal salts of organic acids whose alkane esters are less soluble in water than that of the alkane halide and treating of the alcohol ester formed with magnesium or metal hydroxides to form the alcohol and the metal salt of the organic acids.
摘要翻译： 制备醇的方法包括从液体烷烃卤化物和有机酸的金属盐形成醇酯以产生用于与镁或金属氢氧化物反应以形成醇和有机酸的金属盐的气态醇酯。 在改进方法中，液相醇酯代替气态醇酯由液态烷烃卤化物和烷烃酯在水中比烷烃卤化物溶解度较低的有机酸的金属盐溶液产生，并处理与 镁或金属氢氧化物以形成醇和有机酸的金属盐。
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公开(公告)号：US08052847B2
公开(公告)日：2011-11-08
申请号：US11901247
申请日：2007-09-14
申请人： Matthew Koban , Phillip Rowland , Michael Harvey , Peter Demakos
发明人： Matthew Koban , Phillip Rowland , Michael Harvey , Peter Demakos
CPC分类号： B01D3/02 , B01D53/1425 , B01D53/263 , Y10S159/901
摘要： A system and method for removing water from a liquid desiccant such as a glycol used to dry cooled air in order to restore the desiccant to a purity up to around 97% in a closed continuous flow process. Liquid desiccant can be sprayed into cooled air in a conditioner where it gains moisture. The wet or gained desiccant can be optionally preheated in an economizing heat exchanger and then routed into a concentrator. Desiccant pure to around 97% can be removed from the concentrator, passed through an economizing heat exchanger to provide the preheating and returned to the conditioner holding area. The concentrator can be heated by steam or other means such as natural gas to boil the wet desiccant causing mixed vapor to enter a vertical distillation column where most of the glycol condenses out on the column packing or plates and returns to the concentrator. Almost pure water vapor normally passes out of the top of the column and can be condensed in a water-cooled (or otherwise cooled) condenser and collected or discarded as liquid water. A portion of the water can be piped back into the top of the column as a reflux stream that scrubs the column packing or plates of desiccant. In this way, the desiccant can be purified to around 97%.
摘要翻译： 用于从用于干燥冷却空气的二醇等液体干燥剂中除去水的系统和方法，以便在封闭的连续流动过程中将干燥剂恢复至高达约97％的纯度。 液体干燥剂可以在其中获得水分的调理剂中喷入冷却的空气中。 湿的或获得的干燥剂可以任选地在节约的热交换器中预热，然后被路由到浓缩器中。 干燥剂纯度达到97％左右，可以从集中器中取出，通过节约型换热器提供预热并返回到调理器的保持区域。 浓缩器可以通过蒸汽或其它方式加热，例如天然气，以将湿干燥剂煮沸，使混合蒸气进入立式蒸馏塔，其中大部分乙二醇在柱填料或板上冷凝并返回浓缩器。 几乎纯净的水蒸气通常从塔的顶部流出，并可以在水冷（或冷却的）冷凝器中冷凝，并以液态水的形式收集或丢弃。 一部分水可以作为回流而被回管到塔的顶部，该回流可以洗涤干燥剂的柱填料或板。 以这种方式，干燥剂可以纯化至约97％。
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公开(公告)号：US06964728B2
公开(公告)日：2005-11-15
申请号：US10147621
申请日：2002-05-16
CPC分类号： B01D3/34 , Y10S203/11 , Y10S203/14
摘要： Bisphenol-A-bis(neopentylglycolphosphate) products of enhanced properties and processes for preparing them are described. One of the processes includes (a) mixing and reacting neopentyl glycol and bisphenol-A-bis(dichlorophosphate) in an inert polar organic solvent which (1) if mixed by itself with an equal volume of water at 25° C., will form a separate phase, (2) the solvent by itself will dissolve at least about 10 wt % of bisphenol-A-bis(neopentylglycolphosphate) at a temperature in the range of 25 to 50° C., and optionally but preferably (3) the solvent by itself can be completely vaporized at a temperature below about 180° C.; (b) washing bisphenol-A-bis(neopentylglycolphosphate) product formed in a) while dissolved in inert organic solvent having such characteristics at least once with an aqueous alkaline washing solution; and (c) optionally but preferably, recovering bisphenol-A-bis(neopentylglycolphosphate) product from organic solvent having such characteristics. The reaction of (a) can be conducted in an inert non-polar solvent if that solvent is replaced by an inert polar organic solvent satisfying (1) and (2), and preferably (3). A solvent satisfying (1), (2), and (3) is used when (c) is conducted by distilling or vaporizing off the solvent to recover the bisphenol-A-bis(neopentylglycolphosphate) product as such. The product has a low acid number or a high thermal stability, and usually both.
摘要翻译： 描述了增强性能的双酚A双（新戊二醇磷酸酯）产物及其制备方法。 其中一个方法包括（a）在惰性极性有机溶剂中将新戊二醇和双酚-A-双（二氯磷酸盐）混合和反应，（1）如果在25℃下与等体积的水自身混合，将形成 单独的相，（2）溶剂本身将在25至50℃的温度范围内溶解至少约10重量％的双酚A-双（新戊基乙二醇酯磷酸酯），并且任选但优选（3） 溶剂本身可以在低于约180℃的温度下完全蒸发; （b）洗涤a）中形成的双酚-A-双（新戊基乙二醇磷酸酯）产物，同时用碱性洗涤液溶解至少一次具有这种特性的惰性有机溶剂; 和（c）任选地但优选地，从具有这种特性的有机溶剂中回收双酚A-双（新戊基乙二醇磷酸酯）产物。 （a）的反应可以在惰性非极性溶剂中进行，如果该溶剂被满足（1）和（2），优选（3）的惰性极性有机溶剂代替。 （c）通过蒸馏除去溶剂进行蒸发以回收双酚A-双（新戊基乙二醇酯磷酸酯）产物时，使用满足（1），（2）和（3）的溶剂。 该产品具有低酸值或高热稳定性，通常两者都是。
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6.发明授权
公开(公告)号：US5985100A
公开(公告)日：1999-11-16
申请号：US11700
申请日：1998-02-17
申请人： Maik Aron , Harald Rust
发明人： Maik Aron , Harald Rust
CPC分类号： C07C41/42 , C07C29/80 , Y10S203/20
摘要： Butanol and dibutyl ether are separated from a mixture containing water, dibutyl ether and n-butanol, 2-butanol and/or isobutanol by a process in whicha) the mixture is introduced into a first distillation column, essentially butanol is separated off at the bottom of this distillation column and the mixture taken off at the top of the distillation columnb) is introduced into a second distillation column and essentially dibutyl ether is separated off at the bottom of this second distillation column and the mixture formed at the top of the second distillation column is removed,c) the second distillation column being operated at a higher pressure than the first distillation column and at least one of the two mixtures taken off via the top of the distillation columns being subjected to phase separation, only the organic phase separated off being fed to the second distillation column in the case of phase separation downstream of the first distillation column, and separation into an aqueous and an organic phase also being effected in the case of phase separation downstream of the second distillation column, a part stream being recycled from the top or rectification section of the second distillation column to the first distillation column.
摘要翻译： PCT No.PCT / EP96 / 03762 Sec。 371日期1998年2月17日 102（e）1998年2月17日PCT 1995年8月26日PCT PCT。 公开号WO97 / 08120 日期1997年3月6日丁醇和二丁醚由含有水，二丁醚和正丁醇，2-丁醇和/或异丁醇的混合物分离，其中a）将混合物引入第一蒸馏塔，基本上为丁醇 在该蒸馏塔的底部分离，将在蒸馏塔b）顶部排出的混合物引入第二蒸馏塔中，并且在该第二蒸馏塔的底部基本上分离出二丁基醚，并形成混合物 在第二蒸馏塔的顶部被除去，c）第二蒸馏塔在比第一蒸馏塔高的压力下操作，并且通过蒸馏塔的顶部排出的两种混合物中的至少一种经受相分离 在第一蒸馏塔下游相分离的情况下，仅分离出分离的有机相进入第二蒸馏塔，分离 在第二蒸馏塔下游的相分离的情况下也进行水和有机相的离子化，将一部分物流从第二蒸馏塔的顶部或精馏段再循环到第一蒸馏塔。
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公开(公告)号：US20230050575A1
公开(公告)日：2023-02-16
申请号：US17794388
申请日：2021-01-21
发明人： Kokoro HAMACHI , Satoshi SHIMIZU
摘要： Provided are a method for producing an organic substance and an apparatus for producing an organic substance that are capable of efficiently cooling a synthesis gas and converting the synthesis gas to an organic substance at a high conversion efficiency using a microbial catalyst. A method for producing an organic substance includes a step of passing a synthesis gas G1 discharged from a gasifier 2 through a heat exchanger 20 to cool the synthesis gas G1, a step of passing the synthesis gas G1 cooled with the heat exchanger 20 through a gas cooling tower 21 to cool the synthesis gas G1 with water sprayed in the gas cooling tower 21 and a step of bringing the synthesis gas G1 that has passed through at least the heat exchanger 20 and the gas cooling tower 21 into contact with a microbial catalyst to generate an organic substance.
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8.发明授权公开(公告)号：US07527712B2
公开(公告)日：2009-05-05
申请号：US10521784
申请日：2003-07-22
CPC分类号： B01D3/141 , B01D3/143 , B01D3/4222 , C07D301/12 , Y10S203/20 , Y10S203/24
摘要： Process for the continuously operated purification by distillation of the methanol used as solvent in the synthesis of propylene oxide by reaction of a hydroperoxide with propylene, with the methoxypropanols being separated off simultaneously, wherein the solvent mixture obtained in the synthesis is separated in a dividing wall column into a low-boiling fraction including methanol, an intermediate-boiling fraction containing the methoxypropanols as azeotrope with water and a high-boiling fraction including water and propylene glycol.
摘要翻译： 通过蒸馏通过氢过氧化物与丙烯的反应合成环氧丙烷的甲醇作为溶剂进行连续操作纯化的方法，同时将甲氧基丙醇分离出来，其中合成中得到的溶剂混合物在分隔壁 加入包含甲醇的低沸点馏分，含有与水共沸的甲氧基丙醇的中间沸点馏分和包含水和丙二醇的高沸点馏分。
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公开(公告)号：US6117277A
公开(公告)日：2000-09-12
申请号：US894601
申请日：1997-08-22
CPC分类号： C07C29/80
摘要： The invention relates to a process for the purification of C.sub.3 -C.sub.10 -alcohols by distillation, by distilling the alcohols at 150 to 200.degree. C. in the presence of 10 to 1000 ppm of alkali metal hydroxide.
摘要翻译： PCT No.PCT / EP96 / 00633 Sec。 371日期1997年8月22日 102（e）日期1997年8月22日PCT 1996年2月14日PCT PCT。 公开号WO96 / 26173 日期：1996年8月29日本发明涉及通过蒸馏在10〜1000ppm碱金属氢氧化物存在下，在150〜200℃下蒸馏醇来纯化C 3 -C 10醇的方法。
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10.发明授权
公开(公告)号：US5734075A
公开(公告)日：1998-03-31
申请号：US570773
申请日：1995-12-12
IPC分类号： C07C27/00 , C07C27/28 , C07C29/80 , C07C31/02 , C07C51/44 , C07C51/487 , C07C57/04 , C07C57/055 , C07C57/07 , C07C67/08 , C07C67/327 , C07C67/54 , C07C67/60 , C07C69/54 , C07C67/48 , C07C51/42
CPC分类号： C07C51/487 , C07C51/44 , C07C67/327 , C07C67/60
摘要： To recover these noble products consisting of acrylic acid monomer, acrylic ester monomers and alcohols, a thermal cracking is performed in the absence of catalyst on a mixture of heavy distillation residues originating, on the one hand, from the manufacture of acrylic acid and, on the other hand, from the manufacture of the esters, the light fraction originating from the dissociation reactions is continuously vaporized during the cracking operation and this light fraction is distilled in order to recover, after condensation, the required products. The process according to the invention may consist in conducting the cracking of the mixture of heavy residues, optionally preheated, in a reactor (R1); feeding a distillation column (C1) with the light cracking products; recovering the required mixture of light noble products at the head of column (C1); recycling the flow recovered at the foot of column (C1) into the reactor (R1); recovering the heavy residue from the reactor (R1) and sending it to a removal treatment, if appropriate after having diluted it with a part of the flow recovered at the foot of column (C1), the remainder of the said flow being recycled into the reactor (R1). Figure to be published: FIG. 1
摘要翻译： 为了回收由丙烯酸单体，丙烯酸酯单体和醇组成的这些贵重产物，在不存在催化剂的情况下，在重馏分残余物的混合物上进行热裂解，一方面源于丙烯酸的制备， 另一方面，从酯的制造出发，解离反应中的轻馏分在裂解操作期间被连续蒸发，并将该轻馏分蒸馏以在冷凝后回收所需产物。 根据本发明的方法可以包括在反应器（R1）中进行任选预热的重残余物混合物的裂化; 向轻馏分产物中加入蒸馏塔（C1）; 在色谱柱（C1）的头部回收所需的淡色产物混合物; 将在柱（C1）的脚处回收的流回收到反应器（R1）中; 从反应器（R1）中回收重质残余物，并将其送入去除处理（如果适用），将其用塔（C1）底部回收的一部分流体稀释后，将其余的所述流回收到 反应器（R1）。 图将被公布：
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