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    AN EFFICIENT PROCESS FOR THE PRODUCTION OF HIGH MOLECULAR WEIGHT POLYESTER
    1.
    发明申请
    AN EFFICIENT PROCESS FOR THE PRODUCTION OF HIGH MOLECULAR WEIGHT POLYESTER 审中-公开
    用于生产高分子量聚酯的有效方法

    公开(公告)号：WO2009060470A3

    公开(公告)日：2009-07-23

    申请号：PCT/IN2008000452

    申请日：2008-07-19

    Applicant: RELIANCE IND LTD ,  AGARWAL UDAY SHANKAR ,  BOON WYNDHAM HENRY ,  WADEKAR SHREERAM ASHOK ,  DUBEY RAJAN ,  TIBUDE AJAY RAMLAL

    Inventor： AGARWAL UDAY SHANKAR ,  BOON WYNDHAM HENRY ,  WADEKAR SHREERAM ASHOK ,  DUBEY RAJAN ,  TIBUDE AJAY RAMLAL

    IPC: C08G63/80 ,  C08G63/16 ,  C08G63/183 ,  C08G63/78

    CPC classification number: C08G63/80 ,  C08G63/183

    Abstract: The present invention discloses an efficient process for the production of high molecular weight polyester resin having IV of about 0.5 dl/g to about 1.2 dl/g from low molecular weight prepolymer having IV of about 0.2 dl/g to about 0.45 dl/g by adding a Lewis acid such as sulfonic acid at any steps during the esterification step or the melt polymerization step but before a particle former process to reduce the oligomer volatilization during solid state polymerization. The Lewis acid such as sulfonic acid is selected from methane sulfonic acid, para toluene sulfonic acid, toluene sulfonic acid, benzene sulfonic acid or xylene sulfonic acid. The present invention also discloses a low molecular weight crystalline prepolymer having IV of about 0.2 dl/g to about 0.45 dl/g and high molecular weight polyester resin having IV of about 0.5 dl/g to about 1.2 dl/g produced by the above process.

    Abstract translation: 本发明公开了一种制备高分子量聚酯树脂的有效方法，其具有IV为约0.5dl / g至约1.2dl / g的低分子量预聚物，其IV为约0.2dl / g至约0.45dl / g 在酯化步骤或熔融聚合步骤期间的任何步骤，但在固态聚合反应中减少低聚物挥发之前的颗粒形成剂方法之前，在任何步骤中加入路易斯酸如磺酸。 路易斯酸如磺酸选自甲磺酸，对甲苯磺酸，甲苯磺酸，苯磺酸或二甲苯磺酸。 本发明还公开了具有约0.2dl / g至约0.45dl / g的IV的低分子量结晶预聚物和通过上述方法制备的IV为约0.5dl / g至约1.2dl / g的高分子量聚酯树脂 。

    AN EFFICIENT PROCESS FOR THE PRODUCTION OF HIGH MOLECULAR WEIGHT POLYESTER
    4.
    发明申请
    AN EFFICIENT PROCESS FOR THE PRODUCTION OF HIGH MOLECULAR WEIGHT POLYESTER 审中-公开
    生产高分子量聚酯的有效工艺

    公开(公告)号：WO2009060470A2

    公开(公告)日：2009-05-14

    申请号：PCT/IN2008/000452

    申请日：2008-07-19

    Applicant: RELIANCE INDUSTRIES LIMITED ,  AGARWAL, Uday, Shankar ,  BOON, Wyndham, Henry ,  WADEKAR, Shreeram, Ashok ,  DUBEY, Rajan ,  TIBUDE, Ajay, Ramlal

    Inventor： AGARWAL, Uday, Shankar ,  BOON, Wyndham, Henry ,  WADEKAR, Shreeram, Ashok ,  DUBEY, Rajan ,  TIBUDE, Ajay, Ramlal

    IPC: C08G63/78 ,  C08G63/80 ,  C08G63/183

    CPC classification number: C08G63/80 ,  C08G63/183

    Abstract: The present invention discloses an efficient process for the production of high molecular weight polyester resin having IV of about 0.5 dl/g to about 1.2 dl/g from low molecular weight prepolymer having IV of about 0.2 dl/g to about 0.45 dl/g by adding a Lewis acid such as sulfonic acid at any steps during the esterification step or the melt polymerization step but before a particle former process to reduce the oligomer volatilization during solid state polymerization. The Lewis acid such as sulfonic acid is selected from methane sulfonic acid, para toluene sulfonic acid, toluene sulfonic acid, benzene sulfonic acid or xylene sulfonic acid. The present invention also discloses a low molecular weight crystalline prepolymer having IV of about 0.2 dl/g to about 0.45 dl/g and high molecular weight polyester resin having IV of about 0.5 dl/g to about 1.2 dl/g produced by the above process.

    Abstract translation: 本发明公开了一种有效的方法，用于由IV为约0.2dl / g至约1.2dl / g的低分子量预聚物生产具有约0.5dl / g至约1.2dl / g的IV的高分子量聚酯树脂， 通过在酯化步骤或熔融聚合步骤期间但在颗粒形成剂过程之前的任何步骤添加路易斯酸如磺酸以减少固态聚合过程中的低聚物挥发，从而提高至约0.45dl / g。 路易斯酸如磺酸选自甲烷磺酸，对甲苯磺酸，甲苯磺酸，苯磺酸或二甲苯磺酸。 本发明还公开了IV为约0.2dl / g至约0.45dl / g的低分子量结晶预聚物和由上述方法制得的IV为约0.5dl / g至约1.2dl / g的高分子量聚酯树脂

    ANTIMICROBIAL MATERIALS AND PREPARATION THEREOF
    7.
    发明申请
    ANTIMICROBIAL MATERIALS AND PREPARATION THEREOF 审中-公开
    抗微生物材料及其制备

    公开(公告)号：WO2009072144A3

    公开(公告)日：2009-07-30

    申请号：PCT/IN2008000553

    申请日：2008-09-01

    Applicant: RELIANCE IND LTD ,  AGARWAL UDAY SHANKAR ,  THAMPI SUMESH ,  JAIN ASHWIN KUMAR

    Inventor： AGARWAL UDAY SHANKAR ,  THAMPI SUMESH ,  JAIN ASHWIN KUMAR

    IPC: A01N55/02 ,  A01N41/04 ,  C07C309/00

    CPC classification number: C07C309/58 ,  A01N41/04 ,  C08G63/681 ,  D01F1/103 ,  D01F6/62 ,  A01N25/34 ,  A01N59/16 ,  A01N59/20 ,  A01N2300/00

    Abstract: The invention relates to a monomelic antimicrobial agent, to a copolymer and polymer compositions having antimicrobial activity and to articles and products prepared from them. The invention also relate to methods for preparing the anti microbial copolymer and polymer compositions. The monomeric antimicrobial agent of the invention has the general formula (R)j-(SO3MM)m(L)n where j, l, m is an integer from 1 to 6, n is an integer from 0 to 6, M is a metal selected from Ag, Cu or Zn, L is a nitrogen, phosphorus or sulphur containing ligand selected from ammonia, an amine, pyridine, imidazole, pyrazole, triaryl phosphine, trialkyl phosphine, triaryl phosphate, trialkyl phosphate or a thiol, R is a linear or branched unsubstituted or substituted alkyl or alkenyl, an aryl or a substituted aryl carrying at least one reactive functional group.

    Abstract translation: 本发明涉及单体抗微生物剂，涉及具有抗微生物活性的共聚物和聚合物组合物，以及由其制备的制品和产品。 本发明还涉及制备抗微生物共聚物和聚合物组合物的方法。 本发明的单体抗微生物剂具有通式（R）j-（SO 3 MM）m（L）n其中j，l，m是1至6的整数，n是0至6的整数，M是 选自Ag，Cu或Zn的金属，L是选自氨，胺，吡啶，咪唑，吡唑，三芳基膦，三烷基膦，三芳基磷酸酯，三烷基磷酸酯或硫醇的含氮，磷或硫的配体，R是 直链或支链的未取代或取代的烷基或链烯基，带有至少一个反应性官能团的芳基或取代的芳基。

    ANTIMICROBIAL MATERIALS AND PREPARATION THEREOF
    8.
    发明申请
    ANTIMICROBIAL MATERIALS AND PREPARATION THEREOF 审中-公开

    公开(公告)号：WO2009072144A4

    公开(公告)日：2009-06-11

    申请号：PCT/IN2008/000553

    申请日：2008-09-01

    Applicant: RELIANCE INDUSTRIES LIMITED ,  AGARWAL, Uday, Shankar ,  THAMPI, Sumesh ,  JAIN, Ashwin, Kumar

    Inventor： AGARWAL, Uday, Shankar ,  THAMPI, Sumesh ,  JAIN, Ashwin, Kumar

    IPC: A01N55/02 ,  A01N41/04 ,  C07C309/00

    Abstract: The invention relates to a monomelic antimicrobial agent, to a copolymer and polymer compositions having antimicrobial activity and to articles and products prepared from them. The invention also relate to methods for preparing the anti microbial copolymer and polymer compositions. The monomeric antimicrobial agent of the invention has the general formula (R) j -(SO 3 MM) m (L) n where j, l , m is an integer from 1 to 6, n is an integer from 0 to 6, M is a metal selected from Ag, Cu or Zn, L is a nitrogen, phosphorus or sulphur containing ligand selected from ammonia, an amine, pyridine, imidazole, pyrazole, triaryl phosphine, trialkyl phosphine, triaryl phosphate, trialkyl phosphate or a thiol, R is a linear or branched unsubstituted or substituted alkyl or alkenyl, an aryl or a substituted aryl carrying at least one reactive functional group.

    ANTIMICROBIAL MATERIALS AND PREPARATION THEREOF
    9.
    发明申请
    ANTIMICROBIAL MATERIALS AND PREPARATION THEREOF 审中-公开
    抗微生物材料及其制备

    公开(公告)号：WO2009072144A2

    公开(公告)日：2009-06-11

    申请号：PCT/IN2008000553

    申请日：2008-09-01

    Applicant: RELIANCE IND LTD ,  AGARWAL UDAY SHANKAR ,  THAMPI SUMESH ,  JAIN ASHWIN KUMAR

    Inventor： AGARWAL UDAY SHANKAR ,  THAMPI SUMESH ,  JAIN ASHWIN KUMAR

    IPC: A01N55/02 ,  A01N41/04 ,  C07C309/00

    CPC classification number: C07C309/58 ,  A01N41/04 ,  C08G63/681 ,  D01F1/103 ,  D01F6/62 ,  A01N25/34 ,  A01N59/16 ,  A01N59/20 ,  A01N2300/00

    Abstract: The invention relates to a monomelic antimicrobial agent, to a copolymer and polymer compositions having antimicrobial activity and to articles and products prepared from them. The invention also relate to methods for preparing the anti microbial copolymer and polymer compositions. The monomeric antimicrobial agent of the invention has the general formula (R)j-(SO3MM)m(L)n where j, l, m is an integer from 1 to 6, n is an integer from 0 to 6, M is a metal selected from Ag, Cu or Zn, L is a nitrogen, phosphorus or sulphur containing ligand selected from ammonia, an amine, pyridine, imidazole, pyrazole, triaryl phosphine, trialkyl phosphine, triaryl phosphate, trialkyl phosphate or a thiol, R is a linear or branched unsubstituted or substituted alkyl or alkenyl, an aryl or a substituted aryl carrying at least one reactive functional group.

    Abstract translation: 本发明涉及一种单体抗微生物剂，一种具有抗微生物活性的共聚物和聚合物组合物以及由它们制备的制品和产品。 本发明还涉及制备抗微生物共聚物和聚合物组合物的方法。 本发明的单体抗微生物剂具有通式（R）j-（SO3MM）m（L）n，其中j，l，m为1至6的整数，n为0至6的整数，M为 选自Ag，Cu或Zn的金属，L是选自氨，胺，吡啶，咪唑，吡唑，三芳基膦，三烷基膦，磷酸三芳基酯，磷酸三烷基酯或硫醇中的氮，磷或硫的配体，R是 直链或支链的未取代或取代的烷基或烯基，芳基或带有至少一个反应性官能团的取代芳基。

    CONTINUOUS POLYMERIC FILAMENTS HAVING ENHANCED UNIFORMITY OF DENIER AND TENACITY
    10.
    发明申请
    CONTINUOUS POLYMERIC FILAMENTS HAVING ENHANCED UNIFORMITY OF DENIER AND TENACITY 审中-公开
    连续聚合纤维具有增强的均匀度和耐久性

    公开(公告)号：WO2009063477A1

    公开(公告)日：2009-05-22

    申请号：PCT/IN2008/000081

    申请日：2008-02-07

    Applicant: RELIANCE INDUSTRIES LIMITED ,  AGARWAL, Uday, Shankar ,  THAMPI, Sumesh ,  RAGHA, Ramappa, Krishnappa ,  BALASUBRAMANIAN, Mathur, Ramakrishna ,  PATIL, Vasant, Krishnaji ,  ANEJA, Arun, Pal

    Inventor： AGARWAL, Uday, Shankar ,  THAMPI, Sumesh ,  RAGHA, Ramappa, Krishnappa ,  BALASUBRAMANIAN, Mathur, Ramakrishna ,  PATIL, Vasant, Krishnaji ,  ANEJA, Arun, Pal

    IPC: D01D5/08 ,  D01D5/092

    CPC classification number: D01F11/00 ,  D01D5/092

    Abstract: A method and quench apparatus for melt spinning of continuous polymeric filaments having enhanced uniformity of denier and tenacity. Polymeric filaments are extruded from a molten polymeric material (not shown) through the capillaries (not shown) of a spinneret (2). The filament bundle (12) emerging from the spinneret is passed through a quench apparatus (Ia) located underneath the spinneret so as to cool the filament bundle by a cooling gas. A finish agent is applied to the filament bundle by a finish applicator (14) located in the path of the filament bundle. The filament bundle exiting the quench apparatus is taken on a take up device (17). The entraining gas and filament bundle are guided towards the finish applicator by a baffle device (11) located in the path of the filament bundle spaced from the finish applicator so as to stabilize the filament bundle towards the finish applicator and improve finish coverage on the filament bundle and uniformity of denier and tenacity of the filaments (Fig 1).

    Abstract translation: 用于熔融纺丝连续聚合物长丝的方法和骤冷装置，其具有增强的旦尼尔和韧度均匀性。 聚合物长丝通过喷丝头（2）的毛细管（未示出）从熔融聚合材料（未示出）中挤出。 从喷丝头出来的丝束（12）通过位于喷丝板下面的骤冷装置（1a），以便通过冷却气体冷却丝束。 通过位于丝束的路径中的整理剂（14）将整理剂施加到丝束上。 退出淬火装置的丝束被带到卷取装置（17）上。 夹带气体和细丝束通过位于细丝束的路径中的挡板装置（11）被引导到涂抹器，该挡板装置（11）与整理剂施加器间隔开，以使细丝束朝向涂饰器稳定，并改善细丝上的完成覆盖 束的均匀性和长丝的强度（图1）。

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