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1.发明申请VESSEL FOR PERFORMING MICROWAVE-ASSISTED CHEMISTRY ON SMALL VOLUMES OF REAGENTS 审中-公开用于在小容量试剂上进行微波辅助化学物质的容器
公开(公告)号：WO2004054706A1
公开(公告)日：2004-07-01
申请号：PCT/SE2003/001996
申请日：2003-12-18
IPC分类号： B01J19/12
CPC分类号： B01J19/126 , B01J19/0093 , B01J2219/00788 , B01J2219/00941 , B01J2219/1215 , B01J2219/1227 , B01J2219/1233 , B01J2219/1236 , B01J2219/1254 , B01L3/5082 , B01L2300/042 , B01L2300/1866 , H05B6/6408 , H05B6/806
摘要： A micro vial assembly for performing microwave-assisted chemical reactions on small reaction mixture volumes is disclosed, wherein a reaction vessel (10) is sealed through a diaphragm (30) that is capped over an open end of the reaction vessel. The reaction vessel mouths in an end plane of a sleeve (20) surrounding the reaction vessel, the diaphragm being clamped for sealing the open end of the vessel by means of a cap (40) which is secured to the sleeve. The sleeve provides a radial extension of the reaction vessel in order to bridge the radial distance between a wall of the reaction vessel and other components in a system for performing microwave-assisted chemical reactions.
摘要翻译： 公开了一种用于在小反应混合物体积上进行微波辅助化学反应的微型小瓶组件，其中反应容器（10）通过覆盖在反应容器开口端的隔膜（30）密封。 反应容器在围绕反应容器的套筒（20）的端面中开口，隔膜被夹紧，借助于固定到套筒上的盖（40）密封容器的开口端。 套筒提供反应容器的径向延伸，以便在用于进行微波辅助化学反应的系统中桥接反应容器的壁与其它组分之间的径向距离。
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公开(公告)号：WO2003041856A1
公开(公告)日：2003-05-22
申请号：PCT/SE2002/001885
申请日：2002-10-16
发明人： FAGRELL, Magnus
IPC分类号： B01J19/12
CPC分类号： H05B6/806 , B01J19/0013 , B01J19/126 , B01J19/2415 , B01J2219/00063 , B01J2219/00141 , B01J2219/00159 , B01J2219/002 , B01J2219/00213 , B01J2219/00238 , B01J2219/0875 , B01J2219/0877 , G05D23/1935
摘要： Continuous flow heating system and a method of performing chemical reactions in a process fluid carried out in the system. The system includes fluid transporting and containing means (2) and a number of sections (4, 10, 16) adapted to control the temperature of the process fluid according to a predetermined temperature profile. The system comprises at least one heat-up section (4) provided with a microwave heating means and at least one constant temperature section (10 provided with a heating means, adapted to hold the temperature of the process fluid passing through it at a substantially constant temperature T C .
摘要翻译： 连续流加热系统和在系统中进行的过程流体中进行化学反应的方法。 该系统包括流体输送和容纳装置（2）和适于根据预定温度分布控制过程流体的温度的多个部分（4,10,16）。 该系统包括至少一个加热部分（4），其设有微波加热装置和至少一个恒温部分（10），其设置有加热装置，适于保持通过其的工艺流体的温度基本恒定 温度TC。
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公开(公告)号：WO2003040630A3
公开(公告)日：2003-05-15
申请号：PCT/SE2002/002004
申请日：2002-11-05
IPC分类号： H05B6/70
摘要： The present invention relates to a microwave applicator for heating loads being a waveguide transition between the rectangular TE 10 and TE 20 modes comprising a TE 10 mode section and a TE 20 mode section. The location of the load (4) being inside said TE 20 mode section and with its major axis perpendicularly to the major propagation direction of the TE 20 mode, close to a shorting wall (3) of said TE 20 mode section and also close to the centreline of said propagation direction.
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公开(公告)号：WO2002052279A3
公开(公告)日：2002-07-04
申请号：PCT/SE2001/002876
申请日：2001-12-21
发明人： ULIN, Johan
IPC分类号： G01N1/44
摘要： A seal mechanism, apparatus and method are suggested for confining a chemical reaction in a reaction vessel (1) that is accessible through a self-sealing diaphragm (5). A movable plunger (7) is reversibly operable between a retracted position where the diaphragm is accessible for injection and/or extraction of reagents, and an operational position wherein the plunger is controlled to apply an external pressure in direct contact with the self-sealing diaphragm.
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公开(公告)号：WO2004105443A1
公开(公告)日：2004-12-02
申请号：PCT/SE2004/000669
申请日：2004-04-30
IPC分类号： H05B6/70
CPC分类号： H05B6/806 , H05B6/6402 , H05B6/70 , H05B6/704
摘要： Microwave heating device intended for heating load(s) and comprising a cylinder-shaped cavity (2) enclosed by a periphery wall, said cavity is provided with a microwave feeding means (10). The heating device comprises a dielectric wall structure (8) arranged inside said cavity between said periphery wall and said load(s), wherein said microwave feeding means is arranged to generate a microwave field being an arch surface hybrid mode having TE and TM type properties inside said cavity in order to heat the load(s).
摘要翻译： 微波加热装置，用于加热负载并且包括由周围壁包围的圆柱形空腔（2），所述空腔设置有微波馈送装置（10）。 加热装置包括布置在所述外围壁和所述负载之间的所述空腔内的电介质壁结构（8），其中所述微波馈送装置被布置成产生具有TE和TM型性质的拱形表面混合模式的微波场 在所述腔内部，以加热负载。
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公开(公告)号：WO2003034790A3
公开(公告)日：2003-04-24
申请号：PCT/SE2002/001813
申请日：2002-10-04
IPC分类号： H05B6/70
摘要： Microwave heating apparatus comprising a dielectric microwave applicator provided with a microwave coupling means adapted to feed microwave energy to the applicator. The applicator is provided with a load chamber 8 extending coaxially with regard to the centre axis of the applicator from an upper end to a predetermined distance from a lower end of the applicator, said load chamber is adapted to receive a load to be heated. The dielectric applicator comprises two sections, an upper section 4 provided with the load chamber and a lower section 6 for impedance matching between the coupling means and upper section. In a preferred embodiment the lower section has an increasing crosssectional area from the coupling means to the intersection to the upper section.
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公开(公告)号：WO2002048072A3
公开(公告)日：2002-06-20
申请号：PCT/EP2001/014596
申请日：2001-12-12
申请人： PERSONAL CHEMISTRY I UPPSALA AB , KAISER, Nils-Fredrik , LARHED, Mats , HALLBERG, Anders , ALTERMAN, Mathias , WAN, Yiqian
IPC分类号： C07B43/06
摘要： A method of performing a one-pot organic reaction including carbon monoxide as reactant without the use of an external CO gas source is described wherein a reaction mixture containing a solid or liquid CO releasing compound, a non-metal substrate and a metal catalyst is exposed to an energy source to release carbon monoxide from the CO releasing compound and wherein carbon atoms of the released carbon monoxide form a bond with the non-metal substrate compound. A method of preparing chemical libraries and a kit for organic reactions are also described.
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公开(公告)号：WO2003101933A1
公开(公告)日：2003-12-11
申请号：PCT/SE2003/000827
申请日：2003-05-22
发明人： WESTMAN, Jacob , LUNDIN, Ronny
IPC分类号： C07C225/16
CPC分类号： C07C225/16 , C07B2200/11 , C07C229/34
摘要： Novel solid supported intermediate products of the general formula I coupled to a solid polymeric support through one or both of the R&supl; groups or through the R4 group which are suitable for synthesis of heterocyclic compounds are disclosed. Methods for preparing such intermediate products are also disclosed and also the use of the intermediate products in simple and fast methods on solid phase for synthesis of heterocycles.
摘要翻译： 通式I的新型固体支撑的中间产物通过R 1和R 2中的一个或两个与固体聚合物载体偶联， 基团或通过适合于杂环化合物合成的R 4基团。 还公开了制备这种中间产物的方法，并且还公开了用于合成杂环的固相中简单且快速的中间产物的用途。
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公开(公告)号：WO2004054707A1
公开(公告)日：2004-07-01
申请号：PCT/SE2003/002009
申请日：2003-12-18
发明人： HELLMAN, Bo
IPC分类号： B01J19/12
CPC分类号： B01J19/126 , B01J2219/0871 , B01J2219/0877 , H05B6/80 , H05B6/806
摘要： This invention relates to a method and apparatus for performing microwave assisted chemical reactions, in particular for performing microwave assisted organic synthesis reactions under nearly ideal heating and cooling conditions. The method according to the present invention comprises, supplying substances for a chemical reaction into a reaction chamber, which is adapted to withstand high temperature and pressure, applying microwave heating to initiate the chemical reaction and reach a desired temperature, and cooling the reaction mixture to a desired lower temperature by using adiabatic cooling. The invention also relates to an apparatus for performing the method and use of the method and apparatus for performing organic synthesis reactions.
摘要翻译： 本发明涉及用于进行微波辅助化学反应的方法和装置，特别是用于在几乎理想的加热和冷却条件下进行微波辅助有机合成反应。 根据本发明的方法包括向化学反应物质供应适于承受高温和高压的反应室，施加微波加热以引发化学反应并达到所需温度，并将反应混合物冷却至 通过使用绝热冷却所需的较低温度。 本发明还涉及一种用于执行用于进行有机合成反应的方法和装置的方法和用途的装置。
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公开(公告)号：WO2004054705A1
公开(公告)日：2004-07-01
申请号：PCT/SE2003/001964
申请日：2003-12-17
IPC分类号： B01J19/12
CPC分类号： H05B6/666 , B01J19/126 , B01J2219/1218 , B01J2219/1275 , B01J2219/1281 , H05B6/686 , H05B6/70 , H05B6/705 , H05B6/806
摘要： Microwave heating system comprising a plurality of microwave applicators for heating loads arranged in said applicators, a control means, one microwave generator to generate microwave energy having a controllable frequency and power level, and a microwave switch arranged to connect said microwave generator to each of said applicators. Each microwave applicator is dedicated a heating time slot in a time frame, and that said time frame comprises time slots for applicators to be heated. During microwave heating, microwave energy is applied to the microwave applicators in its respective time slot, in consecutive time frames.
摘要翻译： 微波加热系统包括多个用于加热布置在所述施加器中的负载的微波加热器，控制装置，一个产生具有可控频率和功率电平的微波能量的微波发生器，以及布置成将所述微波发生器连接到每个所述微波发生器的微波开关 涂药。 每个微波施加器在时间框架中专用加热时隙，并且所述时间框架包括用于待加热的施加器的时隙。 在微波加热期间，微波能量在相应的时隙中以连续的时间帧施加到微波施加器。
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