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    HALOGEN FREE SYNTHESES OF AMINOSILANES BY CATALYTIC DEHYDROGENATIVE COUPLING
    4.
    发明申请
    HALOGEN FREE SYNTHESES OF AMINOSILANES BY CATALYTIC DEHYDROGENATIVE COUPLING 审中-公开
    通过催化脱氢偶联无卤素合成氨基硅烷

    公开(公告)号：WO2015048237A2

    公开(公告)日：2015-04-02

    申请号：PCT/US2014057377

    申请日：2014-09-25

    Applicant: SANCHEZ ANTONIO ,  ITOV GENNADILY ,  ZHANG PENG ,  STEPHENS MATTHEW DAMIEN

    Inventor： SANCHEZ ANTONIO ,  ITOV GENNADILY ,  ZHANG PENG ,  STEPHENS MATTHEW DAMIEN

    IPC: C07F7/10

    CPC classification number: C07F7/025 ,  C07F7/10 ,  H01L21/02219 ,  H01L21/02617

    Abstract: Compounds and method of preparation of Si-X and Ge-X compounds (X = N, P, As and Sb) via dehydrogenative coupling between the corresponding unsubstituted silanes and amines (including ammonia) or phosphines catalyzed by metallic catalysts is described. This new approach is based on the catalytic dehydrogenative coupling of a Si-H and a X-H moiety to form a Si-X containing compound and hydrogen gas (X = N, P, As and Sb). The process can be catalyzed by transition metal heterogenous catalysts such as Ru(0) on carbon, Pd(0) on MgO) as well as transition metal organometallic complexes that act as homogeneous catalysts. The -Si-X products produced by dehydrogenative coupling are inherently halogen free. Said compounds can be useful for the deposition of thin films by chemical vapor deposition or atomic layer deposition of Si - containing films.

    Abstract translation: 描述了通过金属催化剂催化的相应的未取代硅烷和胺（包括氨）或膦之间的脱氢偶联制备Si-X和Ge-X化合物（X = N，P，As和Sb）的化合物和方法。 这种新方法是基于Si-H和X-H部分的催化脱氢偶合形成含Si-X的化合物和氢气（X = N，P，As和Sb）。 该过程可以由过渡金属异质催化剂如碳上的Ru（0），MgO上的Pd（0））以及作为均相催化剂的过渡金属有机金属络合物催化。 由脱氢偶联产生的-Si-X产物固有地是无卤素的。 所述化合物可用于通过化学气相沉积或含Si膜的原子层沉积沉积薄膜。

    POLYMER COATED PARTICLES AND METHODS THEREOF
    5.
    发明申请
    POLYMER COATED PARTICLES AND METHODS THEREOF 审中-公开
    聚合物涂层颗粒及其方法

    公开(公告)号：WO2014205000A1

    公开(公告)日：2014-12-24

    申请号：PCT/US2014/042803

    申请日：2014-06-17

    Applicant: UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL

    Inventor： LAI, Samuel K. ,  YANG, Qi

    IPC: C08J3/12 ,  B01J13/02 ,  A61K9/48 ,  A61K47/30

    CPC classification number: C07F7/025 ,  A61K9/5146 ,  B01J13/02 ,  C08F112/08

    Abstract: Embodiments of the presently-disclosed subject matter include a composition that comprises a particle, a plurality of surface functional groups on a surface of the particle, and a plurality of coating polymers bound to the surface functional groups and forming a coating on the particle that includes a density ratio of about 0.1 to about 20.0, the density ratio being equal to a Flory radius of the plurality of coating polymers divided by a distance between adjacent surface functional groups. Embodiments of the presently-disclosed subject matter also include methods for making the present compositions as well as methods for using the present compositions to deliver a bioactive agent and treat a subject in need thereof.

    Abstract translation: 目前公开的主题的实施方案包括包含颗粒，颗粒表面上的多个表面官能团和与表面官能团结合并在颗粒上形成涂层的多个涂料聚合物的组合物，其包括 密度比为约0.1至约20.0，密度比等于多个涂层聚合物的光泽半径除以相邻表面官能团之间的距离。 目前公开的主题的实施方案还包括制备本发明组合物的方法以及使用本发明组合物递送生物活性剂并治疗有需要的受试者的方法。

    METHOD OF PRODUCING CYCLOHEXASILANE COMPOUNDS
    8.
    发明申请
    METHOD OF PRODUCING CYCLOHEXASILANE COMPOUNDS 审中-公开
    生产环己烷化合物的方法

    公开(公告)号：WO2011094191A1

    公开(公告)日：2011-08-04

    申请号：PCT/US2011/022360

    申请日：2011-01-25

    Applicant: NDSU RESEARCH FOUNDATION ,  ELANGOVAN, Arumugasamy ,  ANDERSON, Kenneth ,  BOUDJOUK, Philip, R. ,  SCHULZ, Douglas, L.

    Inventor： ELANGOVAN, Arumugasamy ,  ANDERSON, Kenneth ,  BOUDJOUK, Philip, R. ,  SCHULZ, Douglas, L.

    IPC: C01B33/00 ,  C01B33/08

    CPC classification number: C01B33/04 ,  C07F7/025 ,  C07F9/5442

    Abstract: A method of preparing a cyclohexasilane compound from trichlorosilane is provided. The method includes contacting trichlorosilane with a reagent composition to produce a compound containing a tetradecahalocyclohexasilane dianion, such as a tetradecachlorocyclohexasilane dianion. The reagent composition typically includes (a) tertiary polyamine ligand; and (b) a deprotonating reagent, such as a tertiary amine having a pKa of at least about 10.5. Methods of converting the tetradecahalocyclohexasilane dianion-containing compound to cyclohexasilane or a dodecaorganocyclohexasilane are also provided.

    Abstract translation: 提供了由三氯硅烷制备环己硅烷化合物的方法。 该方法包括使三氯硅烷与试剂组合物接触以产生含有十四氢环己烷硅烷二阴离子的化合物，例如十四氯环己烷硅烷二阴离子。 试剂组合物通常包括（a）叔胺配体; 和（b）去质子化试剂，例如pKa为至少约10.5的叔胺。 还提供了将十四氢环己烷硅烷二价阴离子化合物转化成环己硅烷或十二碳烯环己硅烷的方法。

    BICYCLIC ORGANOSILICON COMPOUNDS AS ELECTRON DONORS FOR POLYOLEFIN CATALYSTS
    9.
    发明申请
    BICYCLIC ORGANOSILICON COMPOUNDS AS ELECTRON DONORS FOR POLYOLEFIN CATALYSTS 审中-公开
    双金属有机硅化合物作为聚烯烃催化剂的电子助剂

    公开(公告)号：WO2010120794A1

    公开(公告)日：2010-10-21

    申请号：PCT/US2010/030910

    申请日：2010-04-13

    Applicant: FORMOSA PLASTICS CORPORATION, U.S.A. ,  FANG, Yiqun ,  LU, Honglan

    Inventor： FANG, Yiqun ,  LU, Honglan

    IPC: B01J37/00

    CPC classification number: C08F10/00 ,  C07F7/025 ,  C07F7/045 ,  C08F110/06 ,  C08F4/6495 ,  C08F4/6465 ,  C08F2500/04 ,  C08F2500/12

    Abstract: Cyclic organo silicon compounds that may be employed as an electron donor for polymerization catalyst systems, polymerization catalyst systems employing the cyclic organosilicon compounds as an electron donor, methods of making the polymerization catalyst systems, and polymerization processes to produce polyolefin are disclosed. The organosilicon compounds, which are useful as electron donors in polymerization catalyst systems for the production of polyolefins, are represented by the formula (I): where Q 1 , Q 2 , Q 3 , and Q 4 may be identical or different and are each hetero-atoms selected from the group consisting of N, O, S, Si, B, and P. R 1 , R 2 , R 3 , and R 4 may be identical or different and are each hydrocarbon-based substituents to Q 1 , Q 2 , Q 3 , and Q 4 , respectively. The subscripts i, j, m, and n are independently 0 to 3. R 5 and R 6 may be identical or different and are each a bridging group with a backbone chain length between the two hetero-atoms Q 1 and Q 3 , and Q 2 and Q 4 , respectively, being 1-8 atoms. The bridging group is selected from the group consisting of aliphatic, alicyclic, and aromatic bivalent radicals.

    Abstract translation: 公开了可用作聚合催化剂体系的电子供体的循环有机硅化合物，使用环状有机硅化合物作为电子给体的聚合催化剂体系，制备聚合催化剂体系的方法和聚合方法以制备聚烯烃。 在聚烯烃生产的聚合催化剂体系中可用作电子供体的有机硅化合物由式（I）表示：其中Q1，Q2，Q3和Q4可以相同或不同，并且各自是杂原子选择的 由N，O，S，Si，B和P组成的组中，R1，R2，R3和R4可以相同或不同，分别为Q1，Q2，Q3和Q4的烃基取代基。 下标i，j，m和n独立地为0至3.R 5和R 6可以相同或不同，并且各自为两个杂原子Q1和Q3之间的主链长度的桥连基团，以及Q2和Q4， 分别为1-8个原子。 桥连基团选自脂族，脂环族和芳族二价基团。

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