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91.发明公开BIMENTAL-EXCHANGEDZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USETHEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOx 审中-公开BIMETAL交换的β型沸石OFF有机模板干法合成及其用途在选择性催化NOx还原
公开(公告)号：EP3097054A1
公开(公告)日：2016-11-30
申请号：EP14877063.9
申请日：2014-12-30
Applicant: BASF SE , Tokyo Institute of Technology
Inventor： FEYEN, Mathias , MAURER, Stefan , MÜLLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , XIAO, Feng-Shou , YOKOI, Toshiyuki , YILMAZ, Bilge
Abstract: The present invention relates to a process for the production of a zeolitic material having a BEA-type framework structure comprising YO2 and X2O3, wherein said process comprises the steps of (1) preparing a mixture comprising one or more sources for YO2 and one or more sources for X2O3; (2) crystallizing the mixture obtained in step (1); (3) subjecting the zeolitic material having a BEA-type framework structure obtained in step (2) to an ion-exchange procedure with Cu; and (4) subjecting the Cu ion-exchanged zeolitic material obtained in step (3) to an ion-exchange procedure with Fe; wherein Y is a tetravalent element, and X is a trivalent element, wherein the mixture provided in step (1) and crystallized in step (2) further comprises seed crystals comprising one or more zeolitic materials having a BEA-type framework structure, and wherein the mixture provided in step (1) and crystallized in step (2) does not contain an organotemplate as a structure-directing agent, as well as to the zeolitic material having a BEA frame work structure per se, and to its use, in particular in a method for the treatment of NOx by selective catalytic reduction (SCR).
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92.发明授权ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING ALKENYLTRIALKYLAMMONIUM COMPOUNDS 有权沸石材料和生产方法采用ALKENYLTRIALKYLAMMONIUM CONNECTIONS
公开(公告)号：EP2841383B1
公开(公告)日：2016-11-09
申请号：EP13720843.5
申请日：2013-04-24
Applicant: BASF SE
Inventor： FEYEN, Mathias , MÜLLER, Ulrich , PARVULESCU, Andrei-Nicolae , SCHAACK, Bernd, Bastian , AHRENS, Sebastian , GERHARD, Dirk , SON, Sunghee , IFFLAND, Gabriele , SEELIG, Bianca
CPC classification number: B01J29/89 , B01J29/40 , B01J29/405 , B01J29/44 , B01J29/46 , B01J29/48 , B01J29/70 , B01J29/88 , B01J35/002 , C01B37/02 , C01B39/082 , C01B39/12 , C01B39/40
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公开(公告)号：EP3066086A1
公开(公告)日：2016-09-14
申请号：EP14795814.4
申请日：2014-11-05
Applicant: BASF SE
Inventor： VAUTRAVERS, Nicolas , TELES, Joaquim Henrique , PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich
IPC: C07D313/04
CPC classification number: C07D313/04 , B01J27/1806 , B01J29/7088 , B01J31/0209 , C07B41/12
Abstract: A process for the oxidation of an organic carbonyl compound comprising reacting the compound, optionally in the presence of a solvent, with hydrogen peroxide in the presence of a catalyst comprising a tin-containing zeolitic material and at least one potassium salt.
Abstract translation: 一种用于氧化有机羰基化合物的方法，包括任选地在溶剂存在下使化合物与过氧化氢在含锡的沸石材料和至少一种钾盐的催化剂存在下反应。
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94.发明公开
公开(公告)号：EP3060340A1
公开(公告)日：2016-08-31
申请号：EP14786927.5
申请日：2014-10-22
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , LÜTZEL, Hans-Jürgen , TELES, Joaquim Henrique , RIEDEL, Dominic , SEELIG, Bianca , URBANCZYK, Daniel , WEGERLE, Ulrike , HESSE, Michael , WALCH, Andreas , BENDIG, Volker , STEGMANN, Veit , ALTHÖFER, Henning , GASPAR, Boris , STALLMACH, Frank , PUSCH, Anne Kristin
IPC: B01J29/89 , B01J29/035 , B01J35/10 , B01J37/00 , C01B39/08 , B01J37/10 , B01J39/14 , B01J20/10 , B01J35/02
CPC classification number: B01J29/89 , B01J20/183 , B01J20/28011 , B01J20/2803 , B01J20/28042 , B01J20/28059 , B01J20/28061 , B01J20/28064 , B01J20/28071 , B01J20/28073 , B01J20/28076 , B01J20/3007 , B01J20/3014 , B01J20/3085 , B01J29/035 , B01J35/002 , B01J35/023 , B01J35/10 , B01J35/1014 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J37/0018 , B01J37/10 , B01J39/14 , B01J2229/183 , B01J2229/36 , B01J2229/40 , B01J2229/42 , C01B39/026 , C01B39/085 , C01B39/40
Abstract: The present invention relates to A process for the production of a molding, comprising (I) providing a zeolitic material; (II) mixing the zeolitic material provided in step (I) with one or more binders; (III) kneading of the mixture obtained in step (II); (IV) molding of the kneaded mixture obtained in step (III) to obtain one or more moldings; (V) drying of the one or more moldings obtained in step (IV); and (VI) calcining of the dried molding obtained in step (V); wherein the zeolitic material provided in step (I) displays a water adsorption ranging from 1 to 15 wt.-% when exposed to a relative humidity of 85%, as well as to a molding obtainable or obtained according to the inventive process in addition to a molding per se and to their respective use.
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公开(公告)号：EP2694458B1
公开(公告)日：2016-07-20
申请号：EP12768419.9
申请日：2012-04-03
Applicant: BASF SE , Tokyo Institute of Technology
Inventor： YILMAZ, Bilge , MÜLLER, Ulrich , ÖZKIRIM, Faruk , DE VOS, Dirk , XIAO, Feng-Shou , TATSUMI, Takashi , BAO, Xinhe , ZHANG, Weiping , GIES, Hermann , IMAI, Hiroyuki , TIJSEBAERT, Bart
IPC: C07C2/66 , C07C15/073 , C01B39/02 , B01J29/06
CPC classification number: C07C2/66 , C07C2529/70 , C07C15/073 , C07C15/02
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Patent Agency Ranking96.发明公开PROCESS FOR PREPARING A BORON CONTAINING ZEOLITIC MATERIAL HAVING MWW FRAMEWORK STRUCTURE 审中-公开用于生产含硼沸石MWW WITH的帧结构
公开(公告)号：EP2953897A1
公开(公告)日：2015-12-16
申请号：EP14703571.1
申请日：2014-02-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , LÜTZEL, Hans-Jürgen , UHL, Georg , BAYER, Robert , VOGELSANG, Regina , SCHLOSSER, Robert , RUSLIM, Franky , CZAJKA, Pawel
CPC classification number: C01B39/12 , B01J29/86 , B01J37/009 , B01J37/04 , B01J37/06 , B01J37/08 , B01J37/10 , C01B37/007 , C01B39/46 , C01B39/48 , C01P2002/70 , C01P2006/12 , C01P2006/90
Abstract: A process for preparing an aluminum-free boron containing zeolitic material comprising the framework structure MWW (BMWW), comprising (a) hydrothermally synthesizing the BMWW from a synthesis mixture containing water, a silicon source, a boron source, and an MWW template compound obtaining the BMWW in its mother liquor, the mother liquor having a pH above 9; (b) adjusting the pH of the mother liquor, obtained in (a) and containing the BMWW, to a value in the range of from 6 to 9; (c) separating the BMWW from the pH-adjusted mother liquor obtained in (b) by filtration in a filtration device.
Abstract translation: 一种用于无铝硼酸含沸石材料，其包括框架结构MWW（BMWW）包括制备方法（a）从水热合成混合物合成的BMWW含有水，硅源，硼源，并且在MWW模板化合物获得 所述BMWW在其母液，其pH高于9的母液; （B）调节所述母液的pH值，在（a）得到和含有BMWW，在6至9的范围内的值; （C）从在一过滤装置过滤的（b）中得到的pH调节的母液中分离的BMWW。
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97.发明公开PROCESS FOR THE PRODUCTION OF A ZEOLITIC MATERIAL EMPLOYING ELEMENTAL PRECURSORS 审中-公开用于生产有初等前体的沸石材料
公开(公告)号：EP2903934A1
公开(公告)日：2015-08-12
申请号：EP13770921.8
申请日：2013-10-01
Applicant: BASF SE
Inventor： MAURER, Stefan , RUETZ, Roger , PETRY, Julia , MÜLLER, Ulrich
CPC classification number: C01B39/04 , B01J20/18 , B01J29/035 , B01J29/40 , B01J29/86 , B01J29/89 , B01J35/002 , B01J35/023 , B01J2229/186 , B01J2229/42 , C01B37/02 , C01B39/06 , C01B39/12 , C01B39/40 , C07D301/12
Abstract: The present invention relates to a process for the production of a zeolitic material having a framework structure comprising YO2, wherein said process comprises: (1) preparing a mixture comprising one or more tetravalent elements Y in elemental form, one or more organic hydroxide salts, and one or more protic solvents; (2) reacting the mixture obtained in step (1) for converting at least part of the one or more tetravalent elements Y into an oxidic form thereof containing one or more Y—O single bonds and/or one or more Y═O double bonds; and (3) crystallizing a zeolitic material from the mixture obtained in step (2).
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98.发明公开ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING ALKENYLTRIALKYLAMMONIUM COMPOUNDS 有权沸石材料和生产方法采用ALKENYLTRIALKYLAMMONIUM CONNECTIONS
公开(公告)号：EP2841383A1
公开(公告)日：2015-03-04
申请号：EP13720843.5
申请日：2013-04-24
Applicant: BASF SE
Inventor： FEYEN, Mathias , MÜLLER, Ulrich , PARVULESCU, Andrei-Nicolae , SCHAACK, Bernd, Bastian , AHRENS, Sebastian , GERHARD, Dirk , SON, Sunghee , IFFLAND, Gabriele , SEELIG, Bianca
CPC classification number: B01J29/89 , B01J29/40 , B01J29/405 , B01J29/44 , B01J29/46 , B01J29/48 , B01J29/70 , B01J29/88 , B01J35/002 , C01B37/02 , C01B39/082 , C01B39/12 , C01B39/40
Abstract: The present invention relates to a process for the preparation of a zeolitic material comprising the steps of: (1) providing a mixture comprising one or more sources for YO
2 and one or more alkenyltrialkylammonium cation R
1 R
2 R
3 R
4 N
+ -containing compounds as structure directing agent; and (2) crystallizing the mixture obtained in step (1) to obtain a zeolitic material; wherein Y is a tetravalent element, and wherein R
1 , R
2 , and R
3 independently from one another stand for alkyl; and R
4 stands for alkenyl, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.-
99.发明公开
公开(公告)号：EP2812115A2
公开(公告)日：2014-12-17
申请号：EP13716733.4
申请日：2013-02-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , TELES, Joaquim Henrique , SEELIG, Bianca , KAMPE, Philip , WEBER, Markus , BAYER, Robert , SEIDEL, Karsten , RESCH, Peter
CPC classification number: B01J29/7088 , B01J29/7476 , B01J29/89 , B01J35/002 , B01J35/0026 , B01J35/023 , B01J37/0045 , B01J2229/186 , B01J2229/42 , C01B37/005 , C01B39/026 , C01B39/06 , C01B39/085 , C01B39/12 , C07D301/12 , Y02P20/52
Abstract: The present invention relates to a micropowder, wherein the particles of the micropowder have a Dv10 value of at least 2 micrometer and the micropowder comprises mesopores which have an average pore diameter in the range of from 2 to 50 nm and comprise, based on the weight of the micropowder, at least 95 weight-% of a microporous aluminum-free zeolitic material of structure type MWW containing titanium and zinc.
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100.发明公开ORGANOTEMPLATE-FREE SYNTHETIC PROCESS FOR THE PRODUCTION OF A ZEOLITIC MATERIAL OF THE CHA-TYPE STRUCTURE 审中-公开SYNTHENTISCHES过程而不有机模板剂制备具有CHA-施工沸石
公开(公告)号：EP2776369A1
公开(公告)日：2014-09-17
申请号：EP12847478.0
申请日：2012-11-09
Applicant: BASF SE
Inventor： MAURER, Stefan , JIN, Hanpeng , YANG, Jeff , MÜLLER, Ulrich
CPC classification number: B01J29/7015 , B01J2229/186 , C01B39/46
Abstract: The present invention relates to an organotemplate-free synthetic process for the production of a zeoiitic material having a CHA-type framework structure comprising YO2, X
2 O
3 , and optionally comprising Z
2 O
5 , wherein said process comprises the steps of: (1 ) providing a mixture comprising one or more sources for YO
2 , one or more sources for X
2 O
3 , and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO
2 , X
2 O
3 , and optionally comprises Z2O5; and (2) crystallizing the mixture obtained in step (1 ); wherein Y is a tetravaient element, X is a trivalent element, and Z is a pentavalent element, wherein optionally one or more sources for Z
2 O
5 are further provided in step (1 ), and wherein if the CHA framework of the seed crystals does not contain Z
2 O
5 , the seed crystals then have a Y0
2 : X
2 O
3 molar ratio of 5 or greater than 5.
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