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    ORGANOIRIDIUM COMPOUND, PROCESS FOR PRODUCING THE SAME, AND PROCESS FOR PRODUCING FILM
    3.
    发明授权
    ORGANOIRIDIUM COMPOUND, PROCESS FOR PRODUCING THE SAME, AND PROCESS FOR PRODUCING FILM 有权
    铱有机化合物，制造方法，用于制造薄膜和方法

    公开(公告)号：EP1657245B1

    公开(公告)日：2012-07-25

    申请号：EP04771757.4

    申请日：2004-08-11

    申请人： TOSOH CORPORATION ,  SAGAMI CHEMICAL RESEARCH CENTER

    发明人： KAWANO, Kazuhisa ,  TAKAMORI, Mayumi ,  OSHIMA, Noriaki

    IPC分类号： C07F17/00 ,  C23C16/18

    CPC分类号： C07F17/02 ,  C23C16/18

    摘要： An organometallic compound which has a low melting point and excellent vaporization characteristics and can deposit a film on substrates at low temperatures; and a process for producing an iridium-containing film from the organometallic compound. A compound represented by the general formula [2] or the general formula [3]: [2] [3] is reacted with a compound represented by the general formula [4]: [4] to obtain an organoiridium compound represented by the general formula [1]: [1] [In the formulae, R1 represents hydrogen or lower alkyl; R2 represents lower alkyl; X represents halogeno; and M represents an alkali metal.] This compound is used as a raw material to produce an iridium-containing film.

    IMIDE COMPLEX, METHOD FOR PRODUCING THE SAME, METAL-CONTAINING THIN FILM AND METHOD FOR PRODUCING THE SAME
    5.
    发明公开
    IMIDE COMPLEX, METHOD FOR PRODUCING THE SAME, METAL-CONTAINING THIN FILM AND METHOD FOR PRODUCING THE SAME 有权
    IMIDKOMPLEX，方法ITS，金属薄膜和方法及其

    公开(公告)号：EP2058295A1

    公开(公告)日：2009-05-13

    申请号：EP07792748.1

    申请日：2007-08-20

    申请人： Tosoh Corporation ,  SAGAMI CHEMICAL RESEARCH CENTER

    发明人： TADA, Ken-ichi ,  FURUKAWA, Taishi ,  INABA, Koichiro ,  YOTSUYA, Tadahiro ,  CHIBA, Hirokazu ,  YAMAMOTO, Toshiki ,  YAMAKAWA, Tetsu ,  OSHIMA, Noriaki

    IPC分类号： C07C211/65 ,  C01G33/00 ,  C01G35/00 ,  C07C209/00 ,  C23C16/18 ,  C07F9/00

    CPC分类号： C23C16/18 ,  C01G33/00 ,  C01G35/00 ,  C01P2002/88 ,  C07C211/65 ,  C07C251/08 ,  C07F9/005 ,  C23C16/405

    摘要： Objects of the present invention are to provide a novel niobium or tantalum complex having good vapor pressure and becoming a raw material for producing a niobium- or tantalum-containing thin film by a method such as CVD method, ALD method or the like, a method for producing the same, a metal-containing thin film using the same, and a method for producing the same. The present invention relates to producing an imide complex represented by the general formula (1) by, for example, the reaction between M 1 (NR 1 )X 3 (L) r (2) and an alkali metal alkoxide (3):

    (wherein M 1 represents niobium atom or tantalum atom, R 1 represents an alkyl group having from 1 to 12 carbon atoms, R 2 represents an alkyl group having from 2 to 13 carbon atoms, X represents halogen atom, r is 1 when L is 1,2-dimethoxyethane ligand, r is 2 when L is pyridine ligand, and M 2 represents an alkali metal), and producing a niobium- or tantalum-containing thin film by using the imide complex (1) as a raw material.

    摘要翻译： 本发明的目的是提供一种具有良好蒸气压和成为原料用于生产铌或薄膜通过如下方法含钽的新颖铌或钽络合物：如CVD法，ALD法等，一种方法 其制造，含金属的薄膜使用相同的，和用于生产其的方法。 本发明涉及一种在由通式酰亚胺络合物的制造（1）由，例如，（NR 1）X 3（L）M 1之间的反应R（2）和碱金属醇盐（3）组成：（ worin M 1个darstellt铌原子或钽原子，R 1个darstellt烷基具有1至12个碳原子，R 2 darstellt烷基具有2至13个碳原子基团基团，X darstellt卤素原子，r为1时，L是1 1,2-二甲氧基乙烷配位体，配位体r为2时，L是吡啶和M 2 darstellt到碱金属），并且通过使用酰亚胺络合物（1）作为原料的铌或含钽薄膜。

    METHOD FOR PRODUCING 1-SUBSTITUTED-3-FLUOROALKYL PYRAZOLE-4-CARBOXYLATE
    6.
    发明公开
    METHOD FOR PRODUCING 1-SUBSTITUTED-3-FLUOROALKYL PYRAZOLE-4-CARBOXYLATE 有权
    VERFAHREN ZUR HERSTELLUNG VON 1-SUBSTITUIERTEM PYRAZOL-4-CARBONSUREURE-3-FLUORALKYLESTER

    公开(公告)号：EP1854788A1

    公开(公告)日：2007-11-14

    申请号：EP06714409.7

    申请日：2006-02-23

    申请人： SAGAMI CHEMICAL RESEARCH CENTER ,  Japan Finechem Company, Inc.

    发明人： AIHARA, Hidenori ,  YOKOTA, Wakako ,  YAMAKAWA, Tetsu ,  HIRAI, Kenji

    IPC分类号： C07D231/14

    CPC分类号： C07D231/14

    摘要： In a process for producing 1-substituted-3-fluoroalkyl-pyrazole-4-carboxylate (3) by a reaction of 2-alkoxymethylenefluoroacylacetate (1) and hydrazine (2), the reaction is conducted in the presence of a base and water, to produce 1-substituted-3-fluoroalkylpyrazole-4-carboxylate (3) with high selectivity and yield. This novel process enables to produce 1-substituted-3-fluoroalkylpyrazole-4-carboxylate (3), which is useful as an intermediate for pharmaceuticals and agrochemicals, with high selectivity and yield by simple and safe operations.

    摘要翻译： 在通过2-烷氧基甲基三氟酰基乙酸酯（1）和肼（2）的反应制备1-取代-3-氟烷基 - 吡唑-4-羧酸酯（3）的方法中，反应在碱和水的存在下进行， 以高选择性和产率制备1-取代-3-氟代烷基吡唑-4-羧酸酯（3）。 该新方法能够通过简单和安全的操作产生具有高选择性和产率的1-取代-3-氟烷基吡唑-4-羧酸酯（3），其可用作药物和农用化学品的中间体。

    PROCESS FOR PREPARATION OF 7-OXABICYCLO 2.2.1]HEPT-5-ENE-2-CARBOXYLIC ACID DERIVATIVES
    8.
    发明公开
    PROCESS FOR PREPARATION OF 7-OXABICYCLO 2.2.1]HEPT-5-ENE-2-CARBOXYLIC ACID DERIVATIVES 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON 7-OXABICYCLO¬2.2.1HEPT-5-EN-2-CARBONSÄURE-DERIVATEN

    公开(公告)号：EP1319662A1

    公开(公告)日：2003-06-18

    申请号：EP01965636.2

    申请日：2001-09-14

    申请人： Kuraray Co., Ltd. ,  SAGAMI CHEMICAL RESEARCH CENTER

    发明人： KUWAYAMA, Tomoya, c/o KURARAY CO., LTD ,  UJITA, Katsuji, c/o KURARAY CO., LTD ,  SHIMIZU, Kazuya, c/o KURARAY CO., LTD ,  TERASHIMA, Shiro

    IPC分类号： C07D493/08

    CPC分类号： C07D493/08

    摘要： The present invention provides a method of industrially advantageously producing 7-oxabicyclo[2.2.1]hept-5-ene-2-carboxylic acid derivatives under mild conditions in a high yield. The present invention relates to a production method of a 7-oxabicyclo[2.2.1]hept-5-ene-2-carboxylic acid derivative of the formula (III) or the formula (IV), which comprises reacting an α,β-unsaturated carboxylic acid of the formula (I) with a furan derivative of the formula (II) in the presence of a Lewis acid:
    wherein each symbol is as defined in the specification.

    摘要翻译： 本发明提供了一种工业上有利地以高产率在温和条件下生产7-氧杂双环-2,2-庚-5-烯-2-羧酸衍生物的方法。 本发明涉及式（III）或式（IV）的7-氧杂双环-2,2-庚-5-烯-2-羧酸衍生物的制备方法，其包括使α，β-不饱和羧酸 式（I）与式（II）的呋喃衍生物在路易斯酸：CHEM的存在下反应，其中每个符号如说明书中所定义.a

    PROCESS FOR THE PREPARATION OF 7-AZABICYCLO 4.1.0]-HEPT-3-ENE-3-CARBOXYLIC ACID ESTERS
    9.
    发明公开
    PROCESS FOR THE PREPARATION OF 7-AZABICYCLO 4.1.0]-HEPT-3-ENE-3-CARBOXYLIC ACID ESTERS 有权
    VERFAHREN ZUR HERSTELLUNG VON 7-AZABICYCLO（4.1.0）-HEPT-3-ENE-3-CARBONSÄUREESTERN

    公开(公告)号：EP1229022A1

    公开(公告)日：2002-08-07

    申请号：EP00970163.2

    申请日：2000-10-27

    申请人： SAGAMI CHEMICAL RESEARCH CENTER ,  Kuraray Co., Ltd.

    发明人： TERASHIMA, Shiro ,  UJITA, Katsuji ,  ISHIWATA, Akihiro

    IPC分类号： C07D203/02 ,  C07D203/26 ,  C07C227/08 ,  C07C229/48

    CPC分类号： C07C227/08 ,  C07C229/64 ,  C07D203/02 ,  C07D203/26 ,  C07C229/48

    摘要： The present invention provides a method of producing 7-azabicyclo[4.1.0]hept-3-ene-3-carboxylic acid ester (VII) economically, industrially advantageously and efficiently in a large amount. The present invention relates to a production method of compound (VII), which includes reacting epoxide (I) with amine (II) to give aminodiol (III), reacting the aminodiol (III) with a sulfonylating agent in the presence of a base to give azabicyclohept-2-ene (IV), reacting the azabicyclohept-2-ene (IV) with alcohol (V) in the presence of a Lewis acid to give azabicyclohept-3-ene (VI), and eliminating the 7-position substituent R 2 from the azabicyclohept-3-ene (VI).

    摘要翻译： 本发明提供了在工业上有效且有效地大量生产7-氮杂双环[4.1.1]庚-3-烯-3-羧酸酯（VII）的方法。 本发明涉及化合物（VII）的制备方法，其包括使环氧化物（I）与胺（II）反应得到氨基二醇（III），使氨基二醇（III）与磺酰化剂在碱的存在下反应， 给出氮杂双环庚烯-2-烯（IV），在路易斯酸存在下使氮杂双环庚烯-2-烯（IV）与醇（V）反应，得到氮杂双环庚烯-3-烯（VI），除去7-位取代基 R 2选自氮杂双环庚烯-3-烯（VI）。

    HUMAN PROTEINS HAVING SECRETORY SIGNAL SEQUENCES AND cDNAS ENCODING THESE PROTEINS
    10.
    发明公开
    HUMAN PROTEINS HAVING SECRETORY SIGNAL SEQUENCES AND cDNAS ENCODING THESE PROTEINS 审中-公开
    具有分泌与人体蛋白质编码的cDNA ENSURE

    公开(公告)号：EP1040188A2

    公开(公告)日：2000-10-04

    申请号：EP98945604.1

    申请日：1998-10-05

    申请人： SAGAMI CHEMICAL RESEARCH CENTER ,  Protegene Inc.

    发明人： KATO, Seishi ,  KIMURA, Tomoko ,  SEKINE, Shingo ,  KOBAYASHI, Midori

    IPC分类号： C12N15/12 ,  C07K14/47

    CPC分类号： C07K14/47

    摘要： The invention provides human proteins having secretory signal sequences and DNAs coding for these proteins as well as eucaryotic cells forming said proteins by secretory expression. All of the proteins are secreted outside the cells and exist in the extracellular liquid or on the cell membrane, so that they are considered to be proteins controlling the proliferation and the differentiation of the cells. Accordingly, the proteins can be employed as pharmaceuticals or as antigens for preparing antibodies against said proteins. Furthermore, said DNAs can be utilized for expression of said proteins in large amounts. Eucaryotic cells wherein expression vectors of said cDNAs are introduced can be utilized for secretory production of the proteins encoded by said cDNAs.