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    VERFAHREN ZUR SYNTHESE VON N, N-DIMETHYL-1,3-DIAMINOPRAN (DMAPA)
    1.
    发明公开
    VERFAHREN ZUR SYNTHESE VON N, N-DIMETHYL-1,3-DIAMINOPRAN (DMAPA) 有权
    法合成的N，N-二甲基-1,3--DIAMINOPRAN（DMAPA）

    公开(公告)号：EP1945603A1

    公开(公告)日：2008-07-23

    申请号：EP06819191.5

    申请日：2006-10-31

    Applicant: BASF SE

    Inventor： ERNST, Martin ,  OEHLENSCHLÄGER, Steffen ,  KUHNKE, Frank ,  ROSS, Karl-Heinz ,  DEEG, Roland ,  MELDER, Johann-Peter

    IPC: C07C209/48 ,  C07C211/11 ,  B01J10/00 ,  B01D3/14

    CPC classification number: B01J8/20 ,  B01D3/14 ,  B01J2219/00006 ,  B01J2219/00029 ,  B01J2219/0004 ,  C07C209/48 ,  C07C211/11

    Abstract: The invention relates to a diamine industrially producing method from a corresponding alkenile-nitrile which contains at least one C-C double bond consisting (a) in reacting the alkenile-nitrile in a first reactor with a corresponding monoamine by exothermally adding a monoamine to said double bond in such a way that an aminoalkyle nitrile is obtained, wherein the monoamine and water are provided and the alkenile-nitrile is added, (b) in evaporating the unreacted alkenile-nitrile and aminoalkyle for enriching the aminoalkyle nitrile produces in the sump of the first reactor, (c) in transferring the aminoalkyle nitrile bottom product of the step (b) to a second reactor, (d) in batchwisely catalytically hydrogenating the aminoalkyle nitrile transferred at the step (c) in such a way that a diamine is produced in the second reactor, wherein for each batch, an appropriate catalyst and water for hydrogenating nitrils into amines, a desired diamine and a base are provided, the second reactor is supplied with hydrogen and the aminoalkyle nitrile transferred at the step (c) is proportioned therein, and (e) in extracting the diamine and in possibly repeating the steps from (a) to (e). A device for producing the diamine and the use of the devices are also disclosed. The preferred diamine is embodied in the form of a 3-dimethylaminopropylamine (DMAPA).

    VERFAHREN ZUR SYNTHESE VON N, N-DIMETHYL-1,3-DIAMINOPRAN (DMAPA)
    2.
    发明授权
    VERFAHREN ZUR SYNTHESE VON N, N-DIMETHYL-1,3-DIAMINOPRAN (DMAPA) 有权
    VERFAHREN ZUR SYNTHESON N，N-DIMETHYL-1,3-DIAMINOPRAN（DMAPA）

    公开(公告)号：EP1945603B1

    公开(公告)日：2012-05-30

    申请号：EP06819191.5

    申请日：2006-10-31

    Applicant: BASF SE

    Inventor： ERNST, Martin ,  OEHLENSCHLÄGER, Steffen ,  KUHNKE, Frank ,  ROSS, Karl-Heinz ,  DEEG, Roland ,  MELDER, Johann-Peter

    IPC: C07C209/48 ,  C07C211/11 ,  B01J10/00 ,  B01J8/20 ,  B01D3/14

    CPC classification number: B01J8/20 ,  B01D3/14 ,  B01J2219/00006 ,  B01J2219/00029 ,  B01J2219/0004 ,  C07C209/48 ,  C07C211/11

    Abstract: The invention relates to a diamine industrially producing method from a corresponding alkenile-nitrile which contains at least one C-C double bond consisting (a) in reacting the alkenile-nitrile in a first reactor with a corresponding monoamine by exothermally adding a monoamine to said double bond in such a way that an aminoalkyle nitrile is obtained, wherein the monoamine and water are provided and the alkenile-nitrile is added, (b) in evaporating the unreacted alkenile-nitrile and aminoalkyle for enriching the aminoalkyle nitrile produces in the sump of the first reactor, (c) in transferring the aminoalkyle nitrile bottom product of the step (b) to a second reactor, (d) in batchwisely catalytically hydrogenating the aminoalkyle nitrile transferred at the step (c) in such a way that a diamine is produced in the second reactor, wherein for each batch, an appropriate catalyst and water for hydrogenating nitrils into amines, a desired diamine and a base are provided, the second reactor is supplied with hydrogen and the aminoalkyle nitrile transferred at the step (c) is proportioned therein, and (e) in extracting the diamine and in possibly repeating the steps from (a) to (e). A device for producing the diamine and the use of the devices are also disclosed. The preferred diamine is embodied in the form of a 3-dimethylaminopropylamine (DMAPA).

    Abstract translation: 本发明涉及由含有至少一个CC双键的相应烯烃腈制备工业二胺的方法，其包括（a）通过将单胺向所述双键放热加成，使第一反应器中的烯烃腈与相应的单胺反应 从而获得氨基亚烷基腈，其中提供单胺和水并且加入烯烃腈，（b）蒸发未反应的烯烃腈和氨基烷烃以富集在第一槽的槽中产生的氨基亚烷基腈 （c）将步骤（b）的氨基亚烷基腈底部产物转移至第二反应器中，（d）分步催化氢化在步骤（c）中转移的氨基亚烷基腈，使得二胺在 第二反应器，其中对于每批次，提供用于将氮化合物氢化成胺的合适的催化剂和水，提供期望的二胺和碱，第二反应器 （c）中转移的氨基亚烷基腈在其中成比例，和（e）提取二胺，并且可能重复从（a）到（e）的步骤。 还公开了用于生产二胺的装置和这些装置的用途。 优选的二胺以3-二甲基氨基丙胺（DMAPA）的形式体现。

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